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A-7

Oxygen Analyzer

Appendix

Teledyne Analytical Instruments

Melting
Point
(°C)

328

360

A-4

Material Safety Data Sheet

Product Name:

Micro-Fuel Cells and Super Cells, all classes except A-2C, A-3,

and A-5.

Electrochemical Oxygen Sensors, all classes except R-19.
Micro-Fuel Cells, all classes.

Manufacturer:

Teledyne Analytical Instruments

Address:

16830 Chestnut Street, City of Industry, CA 91749

Phone:

(626) 934-1500

Customer Service:

Extension 222

Environmental Health
and Safety:

Extension 230

Date Prepared :

04/26/95

Section I – Product Identification

Section III – Physical/Chemical Characteristics

Section II – Hazardous Ingredients/Composition

Material or
Component

C.A.S. #

Quantity

OSHA PEL

ACGIH

TLV

Lead (Pb)

7439-92-1

3–20 gms

0.05 mg/m

0.15 mg/m

Potassium Hydroxide

1310-58-3

1–5 ml

None

2 mg/m

Solution 15% (KOH)

Specific
Gravity

11.34

2.04

Material
Appearance
or Compo-
nent

Lead

Potassium
Hydroxide

Density

Vapor
Pres-
sure

Boiling
Point (°C)

1744

1320

Odor

Solid, silver
gray, odorless

White or
slightly
yellow,
no odor

Solubility
in Water

Insoluble

Complete

Evap.
Rate

Содержание 3010TAC

Страница 1: ...OR GASES MAY BE PRESENT IN THIS MONITORING SYSTEM PERSONAL PROTECTIVE EQUIPMENT MAY BE REQUIRED WHEN SERVICING THIS SYSTEM HAZARDOUS VOLTAGES EXIST ON CERTAIN COMPONENTS INTERNALLY WHICH MAY PER SIST...

Страница 2: ...weight of any parts in so far as such alterations do not adversely affect our warranty ImportantNotice This instrument provides measurement readings to its user and serves as a tool by which valuable...

Страница 3: ...Analyzer TeledyneAnalyticalInstruments Table of Contents Specific Model Information iv Preface v Part I Control Unit Model TAC Part I 1 1 Part II Intrinsic Safe Barriers and Remote Probe Part II 1 1 A...

Страница 4: ...e box Model3010TACcomplieswithalloftherequirementsoftheCommon wealthofEurope CE forRadioFrequencyInterferenceandElectromagnetic Interference RFI EMI protection 19 Rack Mount The 19 Relay Rack Mount un...

Страница 5: ...ommonwealth of Europe CE for Radio Frequency Interference and Electromagnetic Interference RFI EMI protection and Low Voltage Directive LVD Part I of this manual covers the Model 3010TAC General Purpo...

Страница 6: ...ontrol Unit PN D 64596B or C and a 3010P Analysis Unit PN D 65479 3010TB NECtypeTraceOxygenAnalyzerwithbulkheadmount Control Unit Consists of 3010TB PB Control Unit PN D 66190A and a 3010T Analysis Un...

Страница 7: ...ased electronics 8 bit CMOS microprocessor with 32 kB RAM and 128 kB ROM Three user definable output ranges allow best match to users process and equipment 0 10 ppm through 0 250 000 ppm for trace ana...

Страница 8: ...or general purpose areas The probe is CENELEC approved certification code EEXIA IICT6 The following International Symbols are used throughout the Instruction Manual for your visual and immediate warni...

Страница 9: ...Part I i Part I Control Unit TeledyneAnalyticalInstruments OPERATING INSTRUCTIONS Model 3010TAC Oxygen Analyzer Part I Control Unit Flush Panel Mount Part Numbers D 66192A...

Страница 10: ...ting the Control Unit 3 1 3 3 Electrical Connections 3 3 3 3 1 Primary Input Power 3 4 3 3 2 50 Pin Interface Connector 3 4 3 3 3 RS 232 Port 3 9 3 3 4 Remote Probe Connection 3 10 3 4 Testing the Sys...

Страница 11: ...2 4 4 1 3 Cell Failure 4 13 4 4 2 Span Cal 4 13 4 4 2 1 Auto Mode Spanning 4 13 4 4 2 2 Manual Mode Spanning 4 14 4 4 3 Span Failure 4 16 4 5 The Alarms Function 4 16 4 6 The Range Function 4 18 4 6 1...

Страница 12: ...iv Part I Model 3010TAC Oxygen Analyzer TeledyneAnalyticalInstruments...

Страница 13: ...f this manual covers the Model 3010TAC General Purpose flush panel and or rack mount Control Unit The Remote Probe is covered in Part III of this manual The Control Unit is for indoor use in a nonhaza...

Страница 14: ...related tasks described in detail in chapter 4 Operation Span Span calibrate the analyzer Zero Zero calibrate the analyzer Alarms Set the alarm setpoints and attributes Range Set up the 3 user definab...

Страница 15: ...n operator and analyzer It displays values options and messages that give the operator immediate feedback Standby Button The Standby turns off the display and outputs but circuitry is still operating...

Страница 16: ...centration alarms and 1 system alarm RS 232 Port Serial digital concentration signal remote control valve Remote Valve Provides all electrical interconnect to the Analysis Unit or Remote Probe Remote...

Страница 17: ...Serial digital communications for local network access For future expansion Not implemented at this printing Note If you require highly accurate Auto Cal timing use external Auto Cal control where po...

Страница 18: ...1 6 Part I 1 Introduction Model 3010TAC Teledyne Analytical Instruments...

Страница 19: ...locations are illustrated in section 5 Maintenance Refer to Figure 2 1 Block Diagram of the 3010TAC Electronics In the presence of oxygen the sensor in the Analysis Unit generates a current A current...

Страница 20: ...2 2 Part I 2 Operational Theory Model 3010TAC Teledyne Analytical Instruments Figure 2 1 Block Diagram of the 3010TAC...

Страница 21: ...directed to the display alarms and communications port as well as to the gas control valves in the Analysis Unit The same digital information is also sent to a 12 bit digital to analog converter that...

Страница 22: ...2 4 Part I 2 Operational Theory Model 3010TAC Teledyne Analytical Instruments...

Страница 23: ...the system for operation Carefully unpack the Control Unit and inspect it for damage Immediately report any damage to the shipping agent 3 2 Mounting the Control Unit The Model 3010TAC Control Unit i...

Страница 24: ...it Figure 3 2 Single and Dual 19 Rack Mounts All operator controls are mounted on the control panel which is hinged on the left edge and doubles as a door to provide access to the internal components...

Страница 25: ...open in a 90 degree arc of radius 7 125 inches See Figure 3 3 Figure 3 3 Required Front Door Clearance 3 3 Electrical Connections Figure 3 4 shows the Control Unit rear panel Connections for power co...

Страница 26: ...lock are located in the same assembly Insert the power cord into the power cord receptacle The universal power supply requires a 85 250 V ac 47 63 Hz power source Fuse Installation The fuse block at t...

Страница 27: ...A floating 5 Range 4 20 mA floating 6 Range 4 20 mA floating 8 Range ID 0 1 V dc 23 Range ID 0 1 V dc negative ground 24 Range 0 1 V dc 7 Range 0 1 V dc negative ground Alarm Relays The nine alarm cir...

Страница 28: ...44 Threshold Alarm 2 moving contact 43 Threshold Alarm 2 normally open contact 36 System Alarm normally closed contact 20 System Alarm moving contact 37 System Alarm normally open contact Digital Remo...

Страница 29: ...analyzer is analyzing the Remote Cal Inputs are being polled and a zero or span command can be sent When the contact is CLOSED the analyzer is already calibrating It will ignore your request to calibr...

Страница 30: ...s reserved for the Air Cal Range 25 Table 3 4 lists the pin connections Table 3 4 Range ID Relay Connections Pin Function 21 Range 1 ID Contact 38 Range 1 ID Contact 22 Range 2 ID Contact 39 Range 2 I...

Страница 31: ...e obtainable voltage depending on the load impedance applied See Figure 3 6 Figure 3 6 FET Series Resistance 3 3 3 RS 232 Port The digital signal output is a standard full duplex RS 232 serial communi...

Страница 32: ...he 3010TAC implementation Table 3 6 Required RS 232 Options Parameter Setting Baud 2400 Byte 8 bits Parity none Stop Bits 1 Message Interval 2 seconds 3 3 4 Remote Probe Connection The Models 3010TAC...

Страница 33: ...oth installed and interconnected and the system gas and electrical connections are complete the system is ready to test Before plugging either of the units into their respective power sources Check th...

Страница 34: ...3 Installation Model 3010TAC 3 12 Part I Teledyne Analytical Instruments...

Страница 35: ...hoose autoranging or select a fixed range of analysis as required Set alarm setpoints and modes latching failsafe etc Before configuration these default values are in effect PARAMETER DEFAULT LO Range...

Страница 36: ...of oxygen and warns of any alarm conditions System The system function consists of six subfunctions that regulate the internal operations of the analyzer Auto Cal setup Passwordassignment Self Testini...

Страница 37: ...able of ASCII characters available Once a unique password is assigned and activated the operator MUST enter the UNIQUE password to gain access to set up functions which alter the instrument s operatio...

Страница 38: ...grity of the power supply output boards and amplifiers Version Displays Manufacturer Model and Software Version ofinstrument Show Negative The operator selects whether display can show negative oxygen...

Страница 39: ...in the second line of the TRAK HLD menu after the analyzer returns to the Analyze mode The factory default is three minutes but the delay time is program mable To adjust to delay time use the Left or...

Страница 40: ...en setting the following system parameters can be done only after the password is entered span and zero settings alarm setpoints analysis range definitions switching between autoranging and manual ove...

Страница 41: ...k and forth between letters and the arrow keys to change the letters to the proper password Press Enter to enter the password If the password is accepted the screen will indicate that the password res...

Страница 42: ...A B C D E F G H I J K L M N O P Q R S T U V W X Y Z _ a b c d e f g h i j k l m n o p q r s t u v w x y z 0 1 2 3 4 5 6 7 8 9 When you have finished typing the new password press Enter A verification...

Страница 43: ...the arrow keys to position the blinking over the Logout func tion and press Enter to Log out The screen will display the message ProtectedUntil Password Reentered 4 3 5 System Self Diagnostic Test Th...

Страница 44: ...o chapter 5 Maintenance for number code information The results screen alternates for a timewith Press Any Key ToContinue Then the analyzer returns to the initial System screen 4 3 6 Version Screen Mo...

Страница 45: ...rmance beyond published specification lim its The analyzer is calibrated using zero and span gases Any suitable oxygen free gas can be used for zero gas as long as it is known that it will not react a...

Страница 46: ...ion 4 4 1 3 4 4 1 1 AutoModeZeroing Press Zero to enter the zero function mode The screen allows you to select whether the zero calibration is to be performed automatically or manu ally Use the arrow...

Страница 47: ...e to display Wait about 10 seconds Then wait until Slope is sufficiently close to zero before pressing Enter to finish zeroing Slope is given in ppm s Generally you have a good zero when Slope is less...

Страница 48: ...he display Span Settling AUTO ENT For Next Press Enter to move to the next screen Calib Holdingtime Cal hold 5 min This menue allows the operator to set the time the analyzer should be held in the spa...

Страница 49: ...mode It does not affect anything in Manual Mode Just press Enter to continue SpanVal 000008 00 ENT Span UP Mod Press UP to permit modification Mod of span value Use the arrow keys to enter the oxygen...

Страница 50: ...It will not reset if the next span cycle is correct A trace cell is unlikely to fail span As explained before when the sensor reaches the end of its useful life the zero offset begins to rise until t...

Страница 51: ...the concentration alarms to operate in failsafe or nonfailsafe mode 3 Are either of the alarms to be latching In latching mode once the alarm or alarms trigger they will remain in the alarm mode even...

Страница 52: ...s to move the blinking over to the desired parameter Then use the arrow keys to change the parameter Once the parameters for alarm 1 have been set press Alarms again and repeat this procedure for alar...

Страница 53: ...automatic air calibration range is always 0 25 and is not pro grammable 4 6 1 Setting the Analog Output Ranges To set the ranges enter the range function mode by pressing the Range button on the fron...

Страница 54: ...the digital readout and the RS 232 output continue to read the true value of the oxygen concentration regardless of the analog output range 4 7 The Analyze Function When the Analyze function is active...

Страница 55: ...3 8 8 40 0 4 10 4 50 0 5 12 0 60 0 6 13 6 70 0 7 15 2 80 0 8 16 8 90 0 9 18 4 100 1 0 20 0 The analog output signal has a voltage which depends on the oxygen concentration AND the currently activated...

Страница 56: ...nd in most cases quickly saturate the cell with oxygen which can then require a quite long purge down time for the sensor when then exposed to low oxygen concen trations In the event that flow is to b...

Страница 57: ...cing Micro Fuel cells and replacing fuses in the Analysis Unit are covered in Part II Chapter 5 For recalibration see Part I section 4 4 Calibration WARNING SEE WARNINGS ON THE TITLE PAGE OF THIS MANU...

Страница 58: ...Test 1 Press the System button to enter the system mode 2 Use the arrow keys to move to More and press Enter 3 Use the arrow keys to move to Self Test and press Enter The following failure codes appl...

Страница 59: ...TED The 3010TA Control Units contain the following major components Power Supply Motherboard with Microprocessor RS 232 chip and PreamplifierPCB Front Panel Display Board and Displays 5 digit LED mete...

Страница 60: ...nstru ment from the power source Close and latch the front panel access door Clean outside surfaces with a soft cloth dampened slightly with plain clean water Do not use any harsh solvents such as pai...

Страница 61: ...PartII i Part II Analysis Unit TeledyneAnalyticalInstruments OPERATING INSTRUCTIONS Model 3010TAC Oxygen Analyzer Part II Intrinsic Safe Barriers and Remote Probe CENELEC Type Part Number C 67564...

Страница 62: ...rochemical Reactions 2 3 2 2 4 The Effect of Pressure 2 4 2 2 5 Calibration Characteristics 2 4 2 2 6 Micro Fuel Cell Class 2 5 2 2 6 1 Hydrogen and or Helium Service 2 5 2 2 6 2 Class L 2C B 2 Cell 2...

Страница 63: ...d are intended for applica tions where remote control of the sample analysis is desirable Safety barrier box isolate the BASEEFA approved probes from the control unit The intrinsically safe sensor pro...

Страница 64: ...barriers and barrier box as shown in drawings C67564 and D66193 1 4 Cell Housing Probe The cell housing probe provides an enclosure for the L 2 MFC O2 or B 2 with an adaptor sensor and temperature co...

Страница 65: ...sed in the remote Control Unit covered in Part I of this manual 2 2 Micro Fuel Cell Sensor 2 2 1 Principles of Operation The oxygen sensors used in the Model 3010TAC series are Micro Fuel Cells design...

Страница 66: ...idently in practically any environment or sample stream The cell is effectively sealed although one end is permeable to oxygen in the sample gas The other end of the cell is a contact plate consisting...

Страница 67: ...rear membrane beneath the anode is filled with electro lyte Cathode and anode are submerged in this common pool They each have a conductor connecting them to one of the external contact rings on the c...

Страница 68: ...rease The electron transfer and therefore the external current will increase even though the oxygen concentration of the sample has not changed It is therefore important that the sample pressure at th...

Страница 69: ...with its application This designation is its class 2 2 6 1 Hydrogen and or Helium Service If the sample gas contains 10 or more hydrogen and or helium only clamp cells are used These Micro Fuel cells...

Страница 70: ...2 6 Part II 2 Operational Theory Model 3010TAC Teledyne Analytical Instruments...

Страница 71: ...that is sheltered from the elements In areas where the ambient temperature is expected to drop below 0 C auxiliary heating must be provided Install the probe with a suitable sample system in an area...

Страница 72: ...the instrument has been idle for too long When the micro Fuel Cell needs to be installed or replaced follow the procedures in chapter 5 Maintenance for removing and installing cells 3 4 Testing the Sy...

Страница 73: ...els intrinsic safety barrier strips P N B367 are installed between the cell and the control unit The barrier strips are housed in an approved bulkhead mountable barrier box P N E324 Refer to drawing D...

Страница 74: ...0 1 V 13 Network 15 Zero Solenoid Return 16 Span Solenoid Return 17 Span Solenoid Hot 18 Range 3 Contact 19 Range 3 Contact 20 Alarm 3 C Contact 21 Range 1 Contact 22 Range 2 Contact 23 Range ID 0 1...

Страница 75: ...O Contact 48 Exhaust Solenoid Return 49 Zero Solenoid 50 Sample Solenoid Return 3 5 Remote Probe Connection The Models 3010TAC are split architecture dual chassis instru ments which have a Remote Prob...

Страница 76: ...3 Installation Model 3010TAC 3 6 Part II Teledyne Analytical Instruments...

Страница 77: ...HE TITLE PAGE OF THIS MANUAL 4 2 When to Replace a Cell The characteristics of the Micro Fuel Cell show an almost constant output throughout its useful life and then fall off sharply towards zero at t...

Страница 78: ...ck holder must align with the guide pin on the cell block Step 1 Remove power from instrument Step 2 Remove the old sensor if installed from the analyzer Step 3 Purge the analyzer at approximately 1 S...

Страница 79: ...effect the cell performance Consult TETAI for available options for either intermittent or continuous CO2 exposure If a cell was working satisfactorily but ceases to function before the warranty peri...

Страница 80: ...Model 3010TAC 4 4 Part II Teledyne Analytical Instruments 0 OK 1 DAC A 0 1 V Concentration 2 DAC B 0 1 V Range ID 3 Both Failed Preamp 0 OK 1 Zero too high 2 Amplifier output doesn t match test input...

Страница 81: ...A 1 Oxygen Analyzer Appendix TeledyneAnalyticalInstruments OPERATING INSTRUCTIONS Models 3010TAC Oxygen Analyzers Appendix Flush Mount Control Unit PN D66192A CENELEC Type Analysis Unit PN C66336...

Страница 82: ...2 Appendix Model 3010TAC TeledyneAnalyticalInstruments Contents A 1 Model 3010TAC Specifications A 3 A 2 Recommended 2 Year Spare Parts List A 5 A 3 Drawing List A 6 A 4 Material Safety Data Sheet A...

Страница 83: ...ell Cell Block BASEEFA Approved Remote Probe Ranges Threeuserdefinableranges 0 10 ppmto0 250 000 ppm Air calibration range 0 25 Autoranging with range ID output Alarms Onesystem failurealarm contactto...

Страница 84: ...meet EN 50081 1 EN 50082 2 LVD Accuracy 2 of full scale at constant temperature 5 of full scale over operating temperature range on factory default analysis ranges once thermal equilibrium has been ac...

Страница 85: ...2 B367 Intrinsic Safe Zenner Barrier 1 A68314 Backpanel Connector Kit _____________________ Order one type only US or European as appropriate A minimum charge is applicable to spare parts orders Note...

Страница 86: ...ing Control Unit Trace Oxygen D 66193 Sensor Block Interconnection Diagram C 66899 Sensor Block Outline Diagram Top 4 Probe C 67564 Safety Barrier Housing Assembly NOTE The MSDS on this material is av...

Страница 87: ...onmentalHealth and Safety Extension 230 Date Prepared 04 26 95 Section I Product Identification Section III Physical Chemical Characteristics Section II Hazardous Ingredients Composition Material or C...

Страница 88: ...f Entry Inhalation Highly unlikely Ingestion May be fatal if swallowed Skin The electrolyte potassium hydroxide is corrosive skin contact may cause irritation or chemical burns Eyes The electrolyte po...

Страница 89: ...and remove all contaminated clothing Get medical attention immedi ately If ingested give large amounts of water and DO NOT INDUCE VOMITING Obtain medical attention immedi ately If inhaled remove to f...

Страница 90: ...n RQ Hazardous Waste Solid N O S Lead Class 9 NA3077 PG III Follow all Federal State and Local regulations Section X References Material Safety Data Sheets from J T Baker Chemical Aldrich Malinckrodt...

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