Shodex ORpak CDBS-453 Скачать руководство пользователя страница 1

ver.211214E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

Operation Manual 

Shodex

 ORpak

 CDBS-453 

 

Please read this manual carefully to achieve the best and consistent column performance for a long time

 

 
 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

· Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 ORpak

 CDBS-453 is a chiral separation column 

filled with spherical porous particles of silica modified with 

β

-cyclodextrin group. Optical isomers are separated 

by 

β

-cyclodextrin’s host-guest inclusion capability. 

 

2. Column Components   
 
 

 
 
 

               

 

 

 
 
 
 
 
 
 
3. Column Specifications 

Product Code 

Product Name 

Column Size (mm) 

Particle 

Size (

μ

m) 

Theoretical Plate Number 

(Per Column) 

I.D. Length 

F7146003 

ORpak CDBS-453 

4.6 150 

 6,000   

 

Base Material 

: Spherical porous particles of silica modified with 

β

-cyclodextrin group

 

Column Housing  : SUS-316   
Screw Type 

: Internally-threaded type No.10-32 UNF 

Shipping Solvent : 0.05 % Acetic Acid + 0.2 M Sodium Chloride Solution/Acetonitrile = 95/5 

 
 
 
 
 
 
 

Содержание ORpak CDBS-453

Страница 1: ...outside of the column for any damage 2 Please check if product name and serial number written on the column package column name tag and enclosed Certificate of Analysis CoA are matching and correct 1 Introduction Thank you for purchasing the Shodex product Shodex ORpak CDBS 453 is a chiral separation column filled with spherical porous particles of silica modified with β cyclodextrin group Optical...

Страница 2: ...bottle Use HPLC grade organic solvent whenever possible Solvents left in an opened bottle for a long time should not be used The content may have been changed absorbed moisture or has been contaminated Always use freshly prepared solvents Solvents stored for a long time may have changed their compositions and may influence elution patterns and or damage the column Note Use of on line degasser is r...

Страница 3: ... start the system at less than 0 2 mL min A rapid increase in pressure can damage the column If the column was used at an elevated temperature lower the flow rate to less than 0 2 mL min at the end of analysis Then turn off the column oven and let the column temperature return to room temperature before stopping the pump If the pump was stopped while the eluent inside the column was still hot as t...

Страница 4: ...the flow direction Introduce 50 mL of acetonitrile or methanol at 0 5 mL min 8 Column Storage Remove the column from the system keeping the solvent used for the analysis Securely tighten the end caps and store the column at a location with stable temperature a cool and dark space is recommended Attention Never allow inside of the column to dry It can damage the column 9 Column Inspection Inspectio...

Страница 5: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

Отзывы: