49
Sample Preparation
Dissolving Solid Samples in Organics
•
Always work in a fume hood so that flammable and/or toxic solvents do not
concentrate in the work area.
•
Wear protective clothing and gloves. Some solvents are readily absorbed
through the skin.
When selecting a solvent, consider the following:
•
Is the solvent compatible with the equipment?
Aliphatic hydrocarbons, ketones and esters, alcohols, and xylene, are the most
frequently used solvents. Make sure that all equipment that will come into
contact with the solvent is compatible with the solvent, e.g., tubing, sample
cups, storage and waste containers, etc.
•
Is the solvent toxic?
Avoid solvents known to be health hazards, such as benzene or methyl isobutyl
ketone (MIBK).
Some solvents, such as the halogenated hydrocarbons, generate toxic gases
when heated.
Consult the data sheets provided by the manufacturer for information on health
hazards (see Reference 5 on page 55).
Dissolving Solid Samples Using Acids
Dissolving solid samples in aqueous solutions often requires the use of
concentrated acids.
Using Acids
When using acids, use the following precautions:
•
Always work in an acid-resistant fume hood.
•
Wear protective clothing, including gloves specifically designed to resist the
acid being used.
Содержание AVIO 500
Страница 1: ...AVIO 500 Customer Hardware and Service Guide ICP OPTICAL EMISSION ...
Страница 2: ......
Страница 3: ...Avio 500 Customer Hardware and Service Guide ...
Страница 12: ...Contents 10 ...
Страница 30: ...28 ...
Страница 31: ...C h a p t e r 1 ...
Страница 32: ......
Страница 33: ...Safety Practices 1 ...
Страница 58: ...56 Safety Practices ...
Страница 59: ...C h a p t e r 2 ...
Страница 60: ......
Страница 76: ...74 Preparing Your Laboratory ...
Страница 77: ...C h a p t e r 3 ...
Страница 78: ......
Страница 79: ...System Description 3 ...
Страница 94: ...92 System Description Figure 3 7 GemCone nebulizer and end cap N0680504 also shown in cross sectional view ...
Страница 115: ...C h a p t e r 4 ...
Страница 116: ......
Страница 137: ...135 Installing the Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 152: ...150 Installation Figure 4 22 Scott Spray Chamber Clip Assembly in Place ...
Страница 195: ...193 Shipping Lists 09290798 USB Cable Table 4 6 Spares Available Continued ...
Страница 196: ...194 Installation ...
Страница 197: ...C h a p t e r 5 ...
Страница 198: ......
Страница 209: ...207 Quick Change Adjustable Torch Module Figure 5 1 Quartz Torch Item Description 1 Plasma Induction Plates 2 Torch 2 1 ...
Страница 217: ...215 Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 316: ...314 Maintenance ...
Страница 317: ...C h a p t e r 6 ...
Страница 318: ......
Страница 339: ...337 RF Generator Sample Introduction System Troubleshooting Form Figure 6 2 Normal plasma at 3mm position ...
Страница 340: ...338 Troubleshooting Figure 6 3 Rounded Plasma due to sample or air getting around the outside typically subtle air leak ...
Страница 342: ...340 Troubleshooting Figure 6 5 Injector too far forward ...
Страница 343: ...341 RF Generator Sample Introduction System Troubleshooting Form Figure 6 6 No Aux Gas torch may be glowing ...
Страница 344: ...342 Troubleshooting Figure 6 7 Air leak or spray chamber temperature too high ...
Страница 345: ...343 RF Generator Sample Introduction System Troubleshooting Form Figure 6 8 Thin plasma due to leak in plasma gas line ...
Страница 346: ...344 Troubleshooting ...
Страница 354: ......