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API 4000 Site Planning Guide

System Requirements

15

Exhaust Requirements

Exhaust from the API 4000 instrument originates from the source exhaust and roughing
pump(s).

Source Exhaust Pump

During operation, solvent vapors and effluent are exhausted from the vent chamber under
the ion source housing by the source exhaust pump (venturi pump) to a 1.27 cm (0.50 in.)
barbed fitting. This effluent must be drained to a drain vessel and vented to a fume hood or
an outside port. It is the responsibility of the customer to provide the proper plumbing
from the drain vessel to the ventilation point.

Roughing Pump Exhaust

The customer will be provided with the installation kit that includes a smoke eliminator
(mist filter) for the roughing pump(s). The system includes fittings and tubing to connect
the roughing pump(s) to the fume hood or other vents.

Venting System Recommendations

The following are recommendations for a customer-supplied vent system that may be used
to vent the roughing pump(s) and the ion source exhaust.

The exhaust flow rate at the instrument (the ability to vent the system) is dependent on the
blower provided by the customer, the duct length, the material and the number of elbows
(or bends) used. If an excessively long duct system or a system with many bends is used, a
stronger blower may be necessary to provide sufficient exhaust volume at the instrument.

Smooth stainless steel tubing should be used instead of flexible stainless steel tubing
where flexibility is not required to reduce system friction loss or drag. A length of smooth
stainless steel ducting has 20 to 30% less friction loss than a comparable length of flexible
ducting. When smooth stainless steel tubing is used, elbows must be used to turn corners.
These elbows should turn at an angle of 45 degrees to reduce friction losses, and a
minimum number of elbows should be used.

Additional recommendations for the venting system include the following items:

The duct casing and venting system should be made of materials suitable for
temperatures as high as 70

°

C (158

°

F) and should meet local building standards.

The vent system should produce a static vacuum of approximately 2 cm (0.75 in) of
water.

The blower should be located as close to the discharge outlet as possible. All joints on
the discharge side should be airtight.

The outlet end of the system should be equipped with a backdraft damper and the
necessary precautions should be taken to keep the exhaust outlet away from open
windows or inlet vents. The exhaust outlet should extend above the roof for proper
dispersal.

The exhaust end of the system should be equipped with an exhaust stack to improve
the overall efficiency of the system.

Содержание SCIEX API 4000 LC/MS/MS

Страница 1: ...http www appliedbiosystems com API 4000 LC MS MS Site Planning Guide P N 1002198D May 2002...

Страница 2: ...tented and may contain parts whose names are registered as trademarks and or function as trademarks Any such usage is intended only to designate those manufacturers products as supplied by Applied Bio...

Страница 3: ...ections 7 System Requirements 8 Weights and Dimensions 8 Room Dimensions 9 Operating Environment 10 Electrical Requirements 11 Gas Requirements 12 Exhaust Requirements 15 Drain Vessel Considerations 1...

Страница 4: ...Table of Contents API Site Planning Guide iv...

Страница 5: ...ed descriptions of the requirements for laboratory layout and required customer supplies Within the scope of this manual the following conventions are used WARNING Indicates an operation that may caus...

Страница 6: ...cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which case you will be required to correct the interfer...

Страница 7: ...nderneath for the roughing pump s A bench for the data acquisition workstation located within 2 m 6 6 ft of the main console One liter 1 L quantities of HPLC or MS grade methanol acetonitrile and wate...

Страница 8: ...flow vent with sufficient tubing to loosely couple the vent to the source exhaust drain vessel supplied by Applied Biosystems MDS SCIEX Safety Requirements Gas cylinders mounted to meet local safety s...

Страница 9: ...will 1 Supply all fittings plugs tubing and cables required to connect the API system to the lab vents electrical receptacles and regulators provided they are within the maximum distances specified i...

Страница 10: ...provides connection panels for gas inputs and exhaust and electronic interfaces for the data acquisition system Introduction The API 4000 LC MS MS instrument is a Liquid Chromatography LC Mass Spectr...

Страница 11: ...nt closest to the ion source housing This panel contains the connections for the curtain gas supply Gas 1 Gas 2 supply source exhaust supply and source exhaust waste out See the Gas and Vacuum Panel f...

Страница 12: ...he recommended bench See the Suggested bench height figure The roughing pump weighs approximately 36 kg 79 lb and is 28 cm 11 in high by 16 5 cm 6 5 in wide by 50 8 cm 20 in long For API 4000 instrume...

Страница 13: ...he custom bench option is the recommended bench Use of wall mounted or fixed benches will require custom installation For purposes of soundproofing it is highly recommended that a softwall be located...

Страница 14: ...2 C in the range of 15 C and 30 C 59 F to 86 F with a relative humidity between 20 and 80 noncondensing An air conditioning unit with a capacity of 2550W 8700 Btu h is required for this API system in...

Страница 15: ...met If the line voltage fluctuates by more than 5 during a 24 hour period and falls out of specified values a power conditioner may be needed Refer to Appendix A In North America use 6 15R receptacle...

Страница 16: ...d Gas 2 The gas supply for the Gas 1 Gas 2 connection requires an input of zero air or UHP nitrogen with an input pressure of 100 psig to a maximum of 105 psig and flows up to 17 L min Nebulizer and s...

Страница 17: ...the API 4000 instrument requires that if house gases are being supplied each supply be separately regulated at the instrument The preferred gas line connections are compression fittings Liquid pipe s...

Страница 18: ...linders have a pressure relief device that releases the contents of the cylinder if the temperature exceeds 52 C 125 F When storing cylinders outside of a building the cylinders should be stored so th...

Страница 19: ...stem or a system with many bends is used a stronger blower may be necessary to provide sufficient exhaust volume at the instrument Smooth stainless steel tubing should be used instead of flexible stai...

Страница 20: ...e housing The drain vessel can be placed under a fume hood or a positive flow vent can be loosely coupled with the short vent hose on the vessel to remove the exhaust gases from the laboratory For loo...

Страница 21: ...rements Only computers supplied by Applied Biosystems MDS SCIEX are fully supported there is no guarantee that customer supplied computers can be made to work properly Applied Biosystems MDS SCIEX may...

Страница 22: ...e manufacturer Useful Part Numbers and Suppliers The following is a list of part numbers for non Applied Biosystems MDS SCIEX supplied products and their manufacturers All regulator fittings are 1 4 N...

Страница 23: ...bing and fixtures and ensure that all installations follow local bylaws and biohazard regulations Electrical The customer will supply the following electrical connections Two 207 242 VAC at 50 60 Hz s...

Страница 24: ...pump s and the source exhaust pump The maximum flow rate of these pumps is a volume less than 30 L min NOTE For installations where the optional installation kit has been purchased venting of the rou...

Страница 25: ...s The API 4000 instrument has line filter circuits that should eliminate the effects of brief transients Regulation The required line voltage regulation is specified in the Electrical Requirements sec...

Страница 26: ...Appendix A API 4000 Site Planning Guide 22...

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