Katanax K1 PRIME Скачать руководство пользователя страница 1 | Manualshive

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Automatic fluxer

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Содержание K1 PRIME

Страница 1: ...Automatic fluxer 1...

Страница 2: ......

Страница 3: ...his time saving instrument please read this manual thoroughly and keep it in a safe and handy place for future reference Should you have any question regarding the use maintenance or repair of your in...

Страница 4: ...How the unit works 13 Heating 13 Agitation and pouring of the melt 13 Cooling 13 Solution agitation 13 Using the K1 Prime basic 15 The main running screen 15 During a fusion 17 The right ingredients...

Страница 5: ...odic inspection 39 Warning 39 Inspection schedule table 39 Flux spillages 39 Visual integrity of heating elements 40 Element terminal connections 41 Thermocouple junction 41 Service operations 43 Warn...

Страница 6: ...find 1 solution agitation module 1 unbreakable Teflon beaker 1 magnetic stirring bars Location Vent hood Molten flux additives and some samples may produce vapors and gases that need to be extracted...

Страница 7: ...t in the lower range of voltages heat up times will be longer than in the recommended voltage range It is possible that the instrument show heating errors due to this because the microprocessor monito...

Страница 8: ...e mineralogy grain size or orientation effects and the result is perfectly homogenous In sample preparation by fusion the sample never actually melts It is merely dissolved into a solvent This solvent...

Страница 9: ...success Katanax has updated the concept making it sturdier and easier to use than ever The K1 Prime comes pre loaded with various fusion methods that can be used as is or can be customized All fusion...

Страница 10: ...le an appropriate flux and often other agents The crucible is inserted into the crucible heater and locked by the locking bar s crucible lid A removable spill protector is provided so that any pouring...

Страница 11: ...old holder that is not suitable for your mold please order as follows Part number For mold with nominal diameter KP0037A 30 mm KP0038A 32 mm KP0039A 35 mm KP0040A 40 mm A blower underneath will provid...

Страница 12: ...into an unbreakable beaker instead of a mold which contains a dilute acid that is automatically stirred by a magnetic system optional Some fusion types such as peroxide and pyrosulfate do not even re...

Страница 13: ...o 7 samples hour Simplicity Simple intelligent high performance heaters Easy installation Intuitive touch screen color LCD graphics interface Easy icon and menu navigation Low maintenance easy compone...

Страница 14: ...ements are powered at voltages below 24 V reasonable precautions must be taken Disconnect power cord before attempting any cleaning maintenance or repair operation Be careful that no liquid infiltrate...

Страница 15: ...ing this tilting motor rotates the crucible heater further forward to an adjustable pouring angle at an adjustable speed The melt pours naturally into the mold and the crucible heater is automatically...

Страница 16: ...rnatively powered magnetic coils produce a rotating magnetic field under the beaker By placing a laboratory type magnetic stirring bar in the acid before fusion the agitation will be automatically sta...

Страница 17: ...e following not all buttons icons will appear depending on the instruments settings Here is a short explanation of the various zones and buttons The graph zone shows the outline of the crucible temper...

Страница 18: ...mong existing programs Clicking on the program name itself will also allow you to rename it More details on this are given at page 31 Managing fusion methods The Copy button is useful to duplicate an...

Страница 19: ...ll parameters can now be freely changed More details are given at page 27 Programming the K1 Prime advanced Entering the password is also required to access the Global parameters screen Duringafusion...

Страница 20: ...step number in red See page 24 Description of the fusion steps for more information on this topic The Stop button as the name implies is used to halt an ongoing fusion process stopping all motors Thi...

Страница 21: ...or neutral flux 50 LiT 50 LiM Here is a list of common oxides along with the recommended flux Simple oxide Recommended flux K2O Na2O BaO SrO Li2O CaO Ag2O MnO MgO PbO CoO Lithium tetraborate Bi2O3 FeO...

Страница 22: ...ible on the analytical instrument one wishes to put as much sample as possible in the preparation However putting too much sample will over saturate the flux and leave undissolved sample particles in...

Страница 23: ...ich reacts at around 700 800 C and lithium nitrate LiNO3 which reacts at around 500 600 C Several minutes at the reaction temperature must be allowed before heating up further and temperature ramping...

Страница 24: ...ll cause the crucibles to pour the hot molten glass onto the instrument possibly damaging it Ageneral fusion Here are the steps required to perform a fusion on the K1 Prime fluxer 1 Turn the instrumen...

Страница 25: ...present Then the flux melts and dissolves the sample The mold is heated at the same time At the end the crucible is tilted to pour into the mold A blower cools the disk 12 At the end of the cycle care...

Страница 26: ...ty the connector pointing to the right and then slide it rightwards to connect it fully 9 5 Put the beaker on the agitator In the last steps of the fusion program the magnetic stirrer will automatical...

Страница 27: ...again with little or no agitation Heating 4 Typically used to melt the flux Heating 5 Typically used to dissolve the sample in the flux with a vigorous agitation Heating 6 Typically used to de gas th...

Страница 28: ...emperature with no rocking the rocking parameter must be set to 0 Most fusion programs will not use all heating steps Note that all heating steps 1 to 6 are identically structured and could be used in...

Страница 29: ...ange a parameter any user can check the current values and settings of the current program step by step This is done by pressing the Settings icon in the lower left corner of the main running screen T...

Страница 30: ...eps of the current program The small crucible with red thermometer icon is placed just besides a cell where the target crucible temperature is displayed The Minus and Plus buttons will be used to chan...

Страница 31: ...ft corner has now switched to a graph icon Pressing this button will bring you back to the main running screen If we scrolled fusion steps towards the right until we reach the pouring step we would ob...

Страница 32: ...scrolling to the next step will show us the available parameters for a cooling step And we now recognize the duration parameter as well as the crucible tilting angle and motion speed The two crucible...

Страница 33: ...n incorrect password on the numeric keypad Managing fusionmethods Fusion methods can be managed just like files on a computer In the main screen you can press the icon corresponding to Copy Delete and...

Страница 34: ...ly two temperature plateaus you could use Heating 1 and Heating 2 or Heating 1 and Heating 3 and so on without affecting anything For standardization purposes Katanax tends to use the last heating ste...

Страница 35: ...ssing on the plus and minus buttons to limit the heat up rate The other ramping values besides Fast are given in C minute Slow heat up rates are particularly useful with a solid oxidizer when we want...

Страница 36: ...thermal stresses would remain in the solid disk This can cause hazardous bursting of the produced disk in the next minutes hours or even days On the other hand and again there are exceptions if the b...

Страница 37: ...rim during Cooling 2 Solution programs To create a fusion dedicated to making solutions the best is to either directly use the Solutions program or create a copy of it if parameter edition is require...

Страница 38: ...can change the instrument s interface language by selecting your preferred language in the list Automatic shut offdelay When the instrument is idle for a certain period of time the heating will be aut...

Страница 39: ...cking Allow more time for the still air cooling i e before starting the cooling blower Diskcrystallizes Crystallization reaction cause the transparent melt in the mold to become milky opaque during co...

Страница 40: ...n flux and will also cause damage to platinumware Make sure to use the proper type and amount of oxidizer Oversaturation A fusion being a dissolution reaction it is perfectly possible to obtain an ove...

Страница 41: ...of death by electrocution those procedures shall be executed only by trained personnel Inspection scheduletable Frequency Checkpoint Description Action if problem found Page Every fusion Flux spillag...

Страница 42: ...tegrity ofheating elements IMPORTANT Always disconnect the instrument from the power outlet when working with panels removed Risk of electrocution In the K1 Prime heating elements build a surface oxid...

Страница 43: ...ermocouple cover 1 7 Locate the mold heater connector on the side of the round mold heater under the thermocouple cover 1 8 Visually inspect and verify that both terminal connectors are not overly oxi...

Страница 44: ...d 1 3 Visually inspect the thermocouple junction Verify that no mechanical shock has occurred which could have damaged the thermocouple junction 1 4 Now look inside the mold heater where the mold woul...

Страница 45: ...on The crucible heating element comprises a single wire wound in a spiral into ceramic insulators plates The resulting assembly is inserted into a soft thermal insulation shell Then a clear tube is in...

Страница 46: ...ir contact brackets You should have in your hand two screws two washers and two small contact brackets 4 3 Manually tilt the crucible heater back to the upright position 5 With the crucible in the upr...

Страница 47: ...From the instructions above the crucible heater is in a partially disassembled state You are ready to install the new heating element 1 Make sure the instrument is still disconnected from its power ou...

Страница 48: ...ater gently tilt the heater forward in the pouring position 7 Using thin pliers gently pull on the two element leads No need to pull hard the idea is to just relieve any compression stress which could...

Страница 49: ...n completely 2 Wear surgical style gloves They will protect you from the insulation fibers and will protect the heating element s clear tubes from your skin oil 3 Remove the mold and mold holder if ne...

Страница 50: ...the mold heater is in a partially disassembled state You are ready to install the new heating element 1 Make sure the instrument is still disconnected from its power outlet 2 Wear surgical style glove...

Страница 51: ...Ensure that the heater s cavity is completely clean before installing a new element 4 Carefully insert the new element into the connector and into the opening on the top of the heater s soft insulatio...

Страница 52: ...ed to fully oxidized material Metal Samples containing un oxidized material Applicable to metals that can be attacked by acids or bases This method has a low temperature oxidation period in which the...

Страница 53: ...rd and what data to upload The password is 111111 six times the digit one You may have to drag the dialog window to the left to show the keyboard and then type the password 4 Select Upload Project Fil...

Страница 54: ...will erase ALL fusion programs currently stored on your fluxer 8 Touch OK 9 Now choose where you want the data to be fetched By default you will have to double click on USBDISK then click on its sub...

Страница 55: ...ns Electrical Voltage 117 127 VAC or 220 240 VAC Frequency 50 60 Hz Electric power 1300 W max consumption Main fuse 115 VAC 12 A 230 VAC 10 A Physical Weight 30 kg 66 lbs Height 40 cm 16 in Width 28 c...

Страница 56: ...the written consent of Katanax Minor adjustments are not covered by warranty Katanax disclaims any responsibility for misuse misapplication negligence or improper installation and maintenance of equip...

Страница 57: ...x inc 2500 Jean Perrin suite 100 Quebec City QC Canada G2C 1X1 Tel 1 418 915 4848 E mail info katanax com Web www katanax com When contacting us kindly have the serial number of the instrument at hand...

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