manualshive.com logo in svg

J-KEM Scientific Gemini, Руководство пользователя

Поделиться
Скачать
J-KEM Scientific Gemini Скачать руководство пользователя страница 28

 

28

Appendix 

 

 
 

I.                   Using the Controller With an Oil Bath 

Application Note #1 

 
Using your 200-Series controller with oil baths rated for less than 120 volt operation is not recommended.   
J-KEM manufactures a 400-Series controller designed for use with oil baths rated for any voltage and is 
recommended for this application.   The 200-Series controller can be used with an oil bath rated for 120 
volt operation without any special setup.   Simply place the flask and the thermocouple directly in the oil, 
set the appropriate power setting and enter the reaction setpoint temperature..   
 
If you need to use an oil bath with you J-KEM controller, J-KEM recommends the Instatherm oil baths.   
The two largest baths, Catalog #’s INS-150 and INS-160 are both rated for use with 120vac controllers 
and provide good temperature regulation. 
 
 
If you frequently heat reactions using oil baths, we recommend J-KEM’s 400-Series oil bath controller. 
 
 

If the reason for using an oil bath is that a small volume is being heated, and you want to use your 

200-Series controller for the job, you have a second option.  J-KEM sells heating mantles for small 
volumes (5, 10, 25, 50 ml) which can be plugged directly into the temperature controller.   Your controller 
regulates volumes as small as 1 ml in a 5 ml flask using a 5 ml heating mantle.   If you need to heat even 
smaller volumes, your User’s Manual describes a technique for heating microliters (“Controlling the 
Heating Mantle Temperature Directly”; in Section 4).   The advantage of this option is that it eliminates 
the mess and safety hazards associated with oil baths.   Accessories for regulating the temperature of 
small volumes are available from J-KEM including small volume heating mantles and micro 
thermocouples. 
 
Call if you have any concerns or would like to discuss your application with a technical representative. 
 
 

Accessories for Heating Small Volumes Available From J-KEM 

 
 

Heating Mantles 

All sizes from 5 ml to 50 L. 

Teflon Coated Microscale Thermocouples 

See Catalog. 

Thermocouples hermetically sealed in 
various size hypodermic needles 

See Catalog 

 

Содержание Gemini

Страница 1: ...Temperature Control For Research and Industry Gemini User s Manual ...

Страница 2: ...POSE IN NO EVENT SHALL J KEM SCIENTIFIC INC BE LIABLE FOR CONSEQUENTIAL INCIDENTAL OR SPECIAL DAMAGES THE BUYER S SOLE REMEDY FOR ANY BREACH OF THIS AGREEMENT BY J KEM SCIENTIFIC INC OR ANY BREACH OF ANY WARRANTY BY J KEM SCIENTIFIC INC SHALL NOT EXCEED THE PURCHASE PRICE PAID BY THE PURCHASER TO J KEM SCIENTIFIC INC FOR THE UNIT OR UNITS OF EQUIPMENT DIRECTLY AFFECTED BY SUCH BREACH Service J KEM...

Страница 3: ...ing Profile 19 3 9 Do s and Don ts When Using Your Controller 20 3 10 Resetting the Controller for use With Heating Mantles 21 3 11 Changing the Temperature Display Resolution 21 3 12 Changing Between PID and ON OFF Operating Modes 22 3 13 Troubleshooting 23 4 APPLICATION NOTES 25 4 1 Theory of How the Controller Works Simply 25 4 2 Controlling a Heating Mantle Temperature Directly 26 4 3 Automati...

Страница 4: ... is heating too slowly or you need more power e g heating to high temperatures give the heater more power by turning the power level up one setting If the a solid state variac Volume ranges are printed above this switch as a guide to select the correct power level since it s easier to guess the volume being heated than the appropriate percent power to apply to a heater Heat Off turns off the heate...

Страница 5: ...nd Low Safety temperature alarms KEM Net is free of charge and can be downloaded from J KEM s web site 1 Go to J KEM s web site at http www jkem com then click on the Download Software link at the bottom of the home page From the list of software downloads click on KEM Net A popup window appears presenting the options of RUN SAVE and CANCEL Selecting the SAVE option brings up a Save File Dialog wi...

Страница 6: ...d the tuning parameters Every type of heater has its own unique set of tuning parameters For the controller to heat with stability it must have programmed with the tuning parameters for the heater currently being used Prior to shipment tuning parameters were programmed into the controller that maximize heating performance for laboratory heating mantles since these are the most common heaters used ...

Страница 7: ...e equipment up in the exact configuration it will be used For example to tune to a vacuum oven place the thermocouple in the room temperature oven and plug the oven into the controller If the oven or heater has its own thermostat or power control turn both as high as they ll go 2 Set the controller to the appropriate power level see Section 3 6 If tuning Channel 1 make sure the timer switch is set...

Страница 8: ...high as they ll go With this procedure it s not necessary for the equipment to start at room temperature This procedure can be performed at any time and any temperature 2 Set the controller to the appropriate power level see Section 3 6 If tuning Channel 1 make sure the timer switch is set so that heating is on see Section 3 5 Turn the controller and heater on then enter the desired set point temp...

Страница 9: ... tuning parameters have been changed or the controller has been autotuned and you want to go back to using heating mantles J KEM recommends that the tuning parameters for heating mantles be loaded manually i e don t autotune to the heating mantle by following the step by step instructions given in Procedure 4 of Section 3 10 2 4 Sensor Placement Placement of the sensor is basically common sense Th...

Страница 10: ...ing mode of the timer See Section 3 5 for timer operation instructions 8 Channel 1 Power Outlet Plug only 120 VAC devices into this outlet see Section 3 2 9 Channel 1 Temperature Sensor Input Use the same type of sensor probe as the sensor plug installed on the controller see Section 3 7 The correct sensor type will have the same color plug as the input 9 on the front of the controller 10 Channel ...

Страница 11: ...Soak Power Off The controller is shipped with the Ramp to Setpoint feature OFF the user must specifically turn Ramp to Setpoint ON When Ramp to Setpoint is OFF the controller heats to the entered setpoint at the fastest rate possible When Ramp to Setpoint is ON the controller heats at the user entered ramp rate The Ramp to Setpoint feature and its associated parameters are turned on and set in the...

Страница 12: ...g Programming the Ramp to Setpoint Feature 1 Press and hold in both the and keys on the front of the temperature meter until the word tunE appears in the display then release both keys 2 Press the key 8 times until the word SPrr appears in the display This is were you set the ramp rate in units of degrees hour First hold in the key then while holding in the key press the and keys until the desired...

Страница 13: ...key until SP2 A is showing in the display 5 Hold in the key while holding in the key press the key until nonE is showing in the display then let go of all the keys 6 Press the key until LEVL is showing in the display 7 Hold in the key while holding in the key press the key until 3 is showing in the display then let go of all the keys 8 Press the key until rEU d is showing in the display 9 Hold in ...

Страница 14: ...ts three normal states of On toFF and t on If the Power Reduction Circuit Section 3 6 is set to the Heat Off position the timer window always displays oFF The four states of the timer circuit are explained below In the off state no power is applied to the heater even if the temperature meter calls for power to be applied The controller always enters the off state when power is turned on or followi...

Страница 15: ...n the timer rolls over from 00 to 59 minutes when entering minutes or from 00 to 99 hours when entering hours Push knob for 1 4 second Push knob for 1 4 second Push knob for 1 4 second Push knob for 1 4 second Hold in knob for 1 second Enter Minutes Function Change Push knob for 1 4 second Function Change Program Change Function Change Function Change Function Change Hold in knob for 1 second Prog...

Страница 16: ...ber of minutes rotate the timer knob to the left Rotate knob to enter minutes Step 3 To change the number of hours in the display momentarily press the timer knob 1 4 second and the hours digits begin to blink To increase the number of hours rotate the timer knob to the right To decrease the number of hours rotate the timer knob to the left Rotate knob to enter hours Momentarily push knob to lock ...

Страница 17: ... for 1 second to enter the time and start the timer When the timer starts the LED under the label ON at Zero lights This indicates that power to the heater will turn ON when the timer counts down to zero Hold in timer knob for 1 second to store time and start timer At any time the timer program can be aborted by holding in the timer knob for 1 second When this is done the display changes to t on T...

Страница 18: ...ask 1 L heating mantle SP 80o C 10 100 ml 10 power When the heating mantle size is substantially larger 5X than the volume being heated i e the heating mantle has excess heating capacity for the volume being heated a lower power setting gives better control 150 ml toluene 250 ml flask 250 ml heating mantle SP 35o C 10 100 ml 10 power Even though the solvent volume isn t included in this power sett...

Страница 19: ...tory oven o Power Setting 50 500 ml Power Setting 2L Conditions Set point 45 C HPLC Column wrapped with heating tape Power Setting 50 500 ml o Temp C o Time min 20 30 40 50 60 70 80 0 10 20 30 40 50 60 70 Temp o C Time min Power Setting 10 100 ml i e 10 power Power Setting 50 500 ml i e 25 power Power Setting 300 ml 2 L i e 50 power Conditions Set point 70o C 50 ml Toluene 100 ml Round bottomed fl...

Страница 20: ... loop should not be broken at any point Don t remove either the thermocouple or heater from the solution without setting the power level to the Heat Off With the thermocouple or heater separated from the solution as the thermocouple cools the controller turns the heater on Since this heat is never fed back to the controller it heats continuously Don t use the controller to regulate an exothermic p...

Страница 21: ...n while holding in the key press the or key until the value 3 0 appears in the display then let go of all the keys 6 Press the key once and the word CyC t will appear in the display First hold in the key then while holding in the key press the or key until the value 30 appears in the display then let go of all the keys 7 Press and hold in both the or keys until the temperature appears in the displ...

Страница 22: ...ained precisely The advantage of PID mode is that it delivers stable temperature control with any heater from heat lamps to vacuum ovens The disadvantage is that the controller must be properly tuned to the heater being used whereas ON OFF mode requires no tuning Since both heating modes have their advantages simplicity vs accuracy instructions to change the controller to ON OFF mode are given bel...

Страница 23: ...er The controller comes on but does not heat The timer controls are set incorrectly Change the position of switch 18 or enter a time into the timer See Section 3 5 The heater is broken To verify that the controller is functioning properly place the power level switch on the 2L setting and enter a set point of 100o C Plug a light into the outlet of the controller then wait 1 minute If the light com...

Страница 24: ...mocouple Temperature display offset needed To enter a controller display offset 1 Turn on controller Allow to warm up for 30 minutes 2 Record displayed temperature 3 Press both the and keys on the front of the temperature meter for the channel you want to change until tunE appears then let go of the keys 4 Press the key until LEVL appears 5 First hold in the key then while holding in the key press...

Страница 25: ...a closed loop feedback system If the process temperature is below the set point the controller turns the heating mantle on and then monitors the temperature rise of the solution If a small rise results indicating a large volume is being heated the controller sets internal parameters appropriate for heating large volumes If a large rise in temperature results the controller responds by loading a se...

Страница 26: ...ing the latent heat of the burner to raise the water temperature from 60o to 80o C This calculation is done by the controller and is independent of the operator The next feature of the controller is directly under operator control and has a major impact on the amount of overshoot on initial warm up 2 Again referring to the range analogy you d obtain better control when heating small volumes if the...

Страница 27: ...r the routine is started and cleared by turning the controller off This procedure must be started every time you want to record temperatures Procedure to Start Temperature Logging 1 Press and hold in both the or keys on the front of the temperature meter for the channel you want to change until the word tunE appears in the display then release both keys 2 Press the key once and the word LEUL appea...

Страница 28: ...r using an oil bath is that a small volume is being heated and you want to use your 200 Series controller for the job you have a second option J KEM sells heating mantles for small volumes 5 10 25 50 ml which can be plugged directly into the temperature controller Your controller regulates volumes as small as 1 ml in a 5 ml flask using a 5 ml heating mantle If you need to heat even smaller volumes...

Страница 29: ...ompared to water since the coefficient of heat for hexane is 0 54 calories g o C and water is 1 0 calorie gram o C That means that 1000 watt seconds of input power will raise the temperature of 10 g of hexane 44o C while the same amount of power causes a 24o C rise in water In theory the tuning constants needed to heat hexane are different from those to heat water Fortunately your J KEM controller...

Страница 30: ...nd unit will appear in the display Next hold in the key then while holding in the key press the key until the value o C appears in the display Let go of all the keys 6 Press the key once and the word SP1 d appears in the display Next hold in the key then while holding in the key press the key until the value SSd appears in the display Let go of all the keys 7 Press in both the and keys until the t...

Страница 31: ...ll the keys 23 Press the key until ZEro appears in the display Next hold in the key then while holding in the key press the or key until the correct value see below appears in the display Let go of all the keys If the TOP meter is being reset enter the value ___________ If the BOTTOM meter is being reset enter the value ___________ 24 Press the key until the word LEVL appears in the display If you...

Отзывы:

Нет отзывов

Бренды по названию

Популярные бренды

Загрузить еще бренды