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INGOS Ltd. Laboratory Instruments division                                                                                                                       Page 6

 

 

3. STARTING OF OPERATION                         

 

3.1  Unpacking of the apparatus

 

Remove  the  instrument  from  the  transport  packing,  check  the  instrument  surface  and  all 

the items according to the delivery note. Please contact the manufacturer or your dealer in case of 

instrument damage or a missing part.

 

Notification: Coat the glass joints with silicone vaseline prior to assembly.

 

3.2  Apparatus assembly

 

1.

 

Screw the bar of the cooler's holder into the nut in the head with the rotating housing, 

insert the housing with the openings and grooved nuts and the cooler's holder itself. 

2.

 

Insert the pipe into the head with the rotating housing from the side of the heating 

bath until the pipe joint snaps behind the ring in the rotating housing. Insert the 

arresting rod into the opening in the rotating housing and tighten the nut of the 

housing. 

3.

 

There is a fixed housing with a nut on the opposite side of the head with the rotating 

housing. Unscrew nut (2), insert on the recessed part of the ball adapter (1) and insert 

securing ring (3) until it snaps behind the recessed part of the ball adapter. Check 

if Gufero packing (4) coated with silicone vaseline is placed by the open side outside 

the recess. Check if flat packing (5) is inserted in the housing and carefully insert 

the ball adapter with Gufer and the nut on glass pipe (7). Insert the ball adapter 

until the end stop and tighten it carefully with nut (2). The half-ball joint of the ball 

adapter points downward. 

4.

 

Rotation  blocking  knob,  which  is  placed  on  the  rotary  casing  head,  set  to  the  ”Lock”  position 

(marking by red point) (for easier locking try to turn the casing a little). Insert suck pipe in to the 

rotary casing until the sitting touches the plastic collar. Than tighten the nut on the rotating casing. 

Finally ”Unlock” the blocking knob (marking by green point). 

5.

 

Coat all the joints on the other glass parts finely with silicone vaseline. 

6.

 

Insert the cooler into the joint in the top part of the ball adapter and also into the 

cooler's holder. The top cooler's outlet serves for connecting the subpressure source, 

other outlets are for cooling water. 

7.

 

Attach the flask with the ball joint to the ball joint using the fixed clamp and tighten 

it. 

8.

 

Insert the round-bottomed flask on the pipe and secure with the flexible clamp. 

9.

 

Insert the inlet pipe with the cock (cock is closed) into the ball adapter. 

10.

 

Connect the bushing. 

11.

 

Pour water into the heating bath; adjust the end stop of the stand for the round- 

bottomed flask being immersed in the liquid. The maximum amount of the liquid is 

approximately 20 mm below the edge of the heating bath. 
Notification: A glass part with a visible crack or another defect must not be used!

 

 

 

Содержание RVO 004

Страница 1: ...INGOS Ltd Laboratory Instruments division Page 1 INGOS Ltd ROTARY VACUUM EVAPORATOR RVO 004 User manual PRAGUE July 2018...

Страница 2: ...e 2 Producer Laboratory Instruments division of INGOS Ltd Supplier and service INGOS Ltd Tel 420 225 983 400 K Nouzovu 2090 420 225 983 409 143 00 PRAGUE 4 Fax 420 244 403 051 CZECH REP e mail instrum...

Страница 3: ...INGOS Ltd Laboratory Instruments division Page 3...

Страница 4: ...dense in a vertical cooler and are collected in a flask This ensures that the evaporated solution cannot be damaged and therefore impaired RVO 004 is equiped by water bath with the electronic temperat...

Страница 5: ...lve flexible and fixed clamp For complete list of basic accessories see paragraph 7 1 1 Fitting Vacuum connection 8 Stand 2 Fitting Cooling water connection 9 Rotation controling 3 Condenser cooler 10...

Страница 6: ...ted in the housing and carefully insert the ball adapter with Gufer and the nut on glass pipe 7 Insert the ball adapter until the end stop and tighten it carefully with nut 2 The half ball joint of th...

Страница 7: ...INGOS Ltd Laboratory Instruments division Page 7 1 Ball adapter 5 Flat sealing 2 Nut 6 Housing 3 Bead type securing ring 7 Suck pipe 4 Gufero sealing 35 22 10 Fig 2a Ball adapter sealing...

Страница 8: ...al resistant 3 3 Apparatus control The instrument is put into operation by connecting the network switch The round bottomed flask starts rotation after turning on the switch The speed of rotation is c...

Страница 9: ...eplace also the flat sealing between the ball adapter and the head fitted with a rotary casing Perform the assembly according to the point 3 2 Apply a light layer of silicone Vaseline to the gufero se...

Страница 10: ...er increasing the concentration of the evaporated sample If the flask cannot be removed easily from the cone carry out further operation only after cooling the bath Caution If you are replacing the ro...

Страница 11: ...ving flask 500 ml joint KS35 20 4SKL0006 Receiving flask 1000 ml joint KS35 20 4SKL0034 Receiving flask 2000 ml joint KS35 20 4SKL0005 Vertical condenser 4SKL0033 Diagonal condenser 4SKL0020 Dry ice t...

Страница 12: ...4 Flat sealing 1TOO0010 Scraper ring 1TOO0008 Sealing PTFE Fig 2b RO1080 Fixed clip for KS32 20 RO1041 Elastic clip for NZ14 23 4SKL0026 Straight fitting GL 14 4SKL0027 Cap nut GL 14 90000013 Tubing c...

Страница 13: ...INGOS Ltd Laboratory Instruments division Page 13 Fig 3 Glass accessories overview...

Страница 14: ...it over to the buyer The instrument may be used only in the manner described in these instructions for use The instrument must not be used in a manner different from that indicated in these instructi...

Страница 15: ...10 5 1 Leak required pressure is not obtained 10 5 2 Other failures 10 6 SAFETY AND OPERATION CONDITIONS 11 6 1 Safe operation 11 6 2 Operating conditions 11 7 ACCESSORIES AND SPARE PARTS 11 7 1 Basic...

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