IKA ElektraSyn 2.0, Руководство пользователя

Страница: 18 / 21

Start-up 19
/// CV setup
ASSEMBLE REFERENCE ELECTRODE AND CV CELL
1
1.
Remove Ag wire and electrode head from glass tube.
2.
Fill tube to halfway point with electrolyte solution*
3.
Insert Ag wire and electrode head into glass tube, the rubber seal should fit
snugly
4.
Place assembled reference electrode in a tube containing the electrolyte solution
and let stand until glass frit is saturated
5.
Attach reference electrode into ElectraSyn vial lid
6.
Attach working electrode and counter electrode to ElectraSyn vial lid
(note, "W" and "C" on top of vial lid correspond to position working
electrode and counter electrode orientation)
7.
Attach lid onto vial
8.
Add CV sample to vial via top cap (note: solution level should be high enough in
the vial to submerge the working electrode and reference electrode tips by ~5 mm)
*A standard electrolyte solution is 3 M KCl
(aq.)
; however, other electrolytes and elect-
rolytes in organic solutions can also be used in the ElectraSyn reference electrode.