Hanna Instruments HI 4109 Скачать руководство пользователя страница 7

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        HI 4000-70.

Avoid large changes in temperature (thermal shock)
as it may damage the sensor.

      Gas bubbles may form from solution out-gassing due

to temperature change.  Gently tap body of sensor to
dislodge them from sensing membrane.

HI 4009

Remove protective cover from sensor tip.

Prepare HI 5315 reference electrode by filling electro-
lyte reservoir with HI 7072 fill solution.

Place sensor and reference electrodes into electrode
holder and connect cable connectors to meter.

HI 4109

Remove the protective plastic wrap that covers the
ceramic junction before assembling sensor for the first
time.

HI 7072 reference fill solution should be added daily
to electrolyte reservoir before electrode use.

During measurement always operate electrode with
the fill hole open.

During normal use, fill solution will slowly drain out
of the tapered cone junction at the lower portion of the
electrode. Excessive loss (>4 cm drop within 24 hours)
is not normal. If this occurs verify cap is tightened and
the interface between the internal cone and outer
body is free of debris.

Add fill solution daily to maintain a good head pres-
sure. For optimum response, this level should be main-
tained and not be allowed to drop more than 2-3 cm
(1-inch) below fill hole. It must cover the ceramic
found on the inner stem.

If an erratic measurement occurs, check to see if for-
eign matter is seen trapped near the internal cone.
Drain and refill with fresh fill solution.

Содержание HI 4109

Страница 1: ...1 HI 4009 HI 4009 HI 4009 HI 4009 HI 4009 HI 4109 HI 4109 HI 4109 HI 4109 HI 4109 Cyanide Ion Selective Electrode Instruction Manual Half cell Combination CYANIDE HI 4009 HI 4109 CYANIDE COMBINATION...

Страница 2: ...uires a separate reference The HI 4109 is a combination ion selective electrode II II II II II Specifications Specifications Specifications Specifications Specifications Type Solid State electrode wit...

Страница 3: ...te itselectrolyticcircuit TheHI4109incorporates areference electrode The silver halide pellet is practically insoluble in thetestsolutionsbeingmeasuredandproducesapotential change due to changes in th...

Страница 4: ...HI 4109 Design elements of the HI 4009 and HI 4109 Design elements of the HI 4009 and HI 4109 electrodes electrodes electrodes electrodes electrodes Upper Cap Spring O Ring Ceramic Junction on Inner S...

Страница 5: ...rements for Cyanide Measurements ISA 500 mL HI4001 00 User supplied standards Note Thesesolutions shouldonlybeusedformakingmore dilute standards The sensing surface will be damaged if submersed in thi...

Страница 6: ...by the corresponding dilution factor For high ionic strength samples use standard addi tion or titration methods Calibration standards and sample solutions should be at same temperature and at elevat...

Страница 7: ...nce fill solution should be added daily toelectrolytereservoirbeforeelectrodeuse During measurement always operate electrode with the fill hole open During normal use fill solution will slowly drain o...

Страница 8: ...lm seal found over ceramic junction on inner stem and discard This is only used for ship ping and long term storage 2 Rinseinnerstemwithdeionizedwatermakingcertain to wet the o ring found on the inner...

Страница 9: ...nd verify elec trodereturnstoitsoriginalposition Youmayneedto gently assist for this to occur 7 Tighten the electrode cap onto the body and fill elec trode body until fill solution volume is just belo...

Страница 10: ...Corrective action Corrective action Corrective action Corrective action Corrective action Verify protective cap has been removed HI 4009 Verify plastic film has been removed from inner stem HI4109 Ve...

Страница 11: ...brated with two or more freshly made standards that are in the linear measurement range of the unknowns One mL of ISA HI 4001 00 is added to each 100 mL volume of standard or sample More calibration s...

Страница 12: ...ix before taking measurements 3 Follow sectionVII GeneralGuidelinestooptimizetest set up 4 Duringcalibrationitisbesttostartwithlowerconcen tration samples first Wait for a stable measurement before re...

Страница 13: ...pH ISE mV meter which simplifies the method greatly The method is recommended for samples with higher ionic strengths Example Cyanide ion determination in samples with con centrations less than 5 X 1...

Страница 14: ...the Hanna Titrator HI 901 or titrated manually XIII XIII XIII XIII XIII pH pH pH pH pH The HI 4109 and HI 4009 electrodes may be used in solutions with pH values between 11 and 13 Samples that fall b...

Страница 15: ...Disposal of Cyanides Disposal of Cyanides Sodium Cyanide is a deadly poison and extreme care must be taken during use and in disposal after use Test solutions and standards may be neutralized before d...

Страница 16: ...r 6 monthsfromdateofpurchasewhenusedfortheirintended purpose and maintained according to instructions If they failtoworkwhenfirstusedcontactyourdealerimmediately Damageduetoaccidents misuse misapplica...

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