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Operational Guide

27

pH 
Calibration

Calibration 
Messages

• 

If  the  buff er  temperature  exceeds  the  temperature  limits  of  the  buff er, 
“WRONG BUFFER TEMPERATURE” will be displayed.

• 

Press 

CLR

  after  entering  calibration  to  clear  all  calibration  options. 

“CLEAR ALL” message will be displayed and the instrument will return to 
measurement mode displaying “CAL DUE” message.

pH Buff er Temperature Dependence

Temperature has an eff ect on pH. The calibration buff er solutions are aff ected by 
temperature changes also. During calibration the instrument will automatically 
calibrate to the pH value corresponding to the temperature. During calibration 
the instrument will display the pH buff er value at 25 ºC.

TEMP

pH BUFFERS

ºC

ºF

1.679

3.000

4.010

6.862

7.010

9.177

10.010

12.454

0

32

1.670

3.072

4.007

6.982

7.130

9.459

10.316

13.379

5

41

1.670

3.051

4.002

6.949

7.098

9.391

10.245

13.178

10

50

1.671

3.033

4.000

6.921

7.070

9.328

10.180

12.985

15

59

1.673

3.019

4.001

6.897

7.046

9.273

10.118

12.799

20

68

1.675

3.008

4.004

6.878

7.027

9.222

10.062

12.621

25

77

1.679

3.000

4.010

6.862

7.010

9.177

10.010

12.450

30

86

1.683

2.995

4.017

6.851

6.998

9.137

9.962

12.286

35

95

1.688

2.991

4.026

6.842

6.989

9.108

9.919

12.128

40

104

1.693

2.990

4.037

6.837

6.983

9.069

9.881

11.978

45

113

1.700

2.990

4.049

6.834

6.979

9.040

9.847

11.834

50

122

1.707

2.991

4.062

6.834

6.978

9.014

9.817

11.697

55

131

1.715

2.993

4.076

6.836

6.979

8.990

9.793

11.566

60

140

1.724

2.995

4.091

6.839

6.982

8.969

9.773

11.442

65

149

1.734

2.998

4.107

6.844

6.987

8.948

9.757

11.323

70

158

1.744

3.000

4.123

6.850

6.993

8.929

9.746

11.211

75

167

1.755

3.002

4.139

6.857

7.001

8.910

9.740

11.104

80

176

1.767

3.003

4.156

6.865

7.010

8.891

9.738

11.003

85

185

1.780

3.002

4.172

6.873

7.019

8.871

9.740

10.908

90

194

1.793

3.000

4.187

6.880

7.029

8.851

9.748

10.819

95

203

1.807

2.996

4.202

6.888

7.040

8.829

9.759

10.734

The  Calibration  Check™  feature  may  fl ag  diagnostic  messages  during  a 
calibration. As electrode aging is normally a slow process, substantial changes 
from  previous  calibrations  are  likely  due  to  a  temporary  problem  with  the 
electrode or buff ers that can be addressed easily. These messages are seen in 
Standard and Basic modes.

Wrong Buff er

This message appears when the diff erence between 
the  pH  reading  and  the  value  of  the  selected  buff er 
is too great. If this error message is displayed, check 
if you have selected the proper calibration buff er and 
have poured the desired buff er.

Содержание edge PHM4092

Страница 1: ...pH...

Страница 2: ...right owner Hanna Instruments Inc Woonsocket Rhode Island 02895 USA Included 3 Safety Measures 3 Description 4 Diagram 4 8 Product Diagram 4 5 Probe Diagram 6 Keypad Function 7 Guide to Indicators 8 S...

Страница 3: ...sing this product make sure that it is entirely suitable for your specific application and for the environment in which it is used Operation of this instrument may cause interference to other electron...

Страница 4: ...c operation mode that streamlines measurement configuration and is useful for many routine applications Every featureandmeasurementdetailisdesignedtogiveyouanedgeinmeasurement technology edgepH is ver...

Страница 5: ...2 Capacitive Touch Keypad 3 3 mm jack input for edgepH digital probes 4 Top mounted ON OFF button 5 Micro USB device connection for power or PC interface 6 Standard USB host connection for data transf...

Страница 6: ...sensor recognition Store calibration specific data from the last calibration Are built with materials suitable for use in chemical analysis Have integrated temperature measurement Incorporate a 3 mm...

Страница 7: ...TUP CLR Used to enter exit SETUP mode During calibration used to clear previous calibration data In log RCL used to clear log records 5 Used to scroll through SETUP menu Used to change selection when...

Страница 8: ...LCD line temperature measurement 12 Temperature units 13 Temp Compensation status 14 Measurement line 15 Measurement units 16 Stability Indicator The third line of the LCD 9 is a dedicated message lin...

Страница 9: ...d for the measurement you will be making 6 Calibrate the sensor probe You are now ready for measurements Bench Cradle Setup Insert electrode holder arm into the post on the pivoting base Connect the p...

Страница 10: ...t the top Plug the 5 VDC adapter into the power supply socket or by connecting directly to a PC Note edgepH is supplied with a rechargeable battery inside which provides about 8 hours of continuous us...

Страница 11: ...ON EDGE or EXPORT TO PC LOG ON EDGE Available Log Select log type to be used from 3 types of logging Manual log on demand Manual log on stability 3 types of stability criteria available Timed interva...

Страница 12: ...nly seen when log errors are present Permits formatting the flash drive On or Off OFF Available Message Transition User may choose how messages are displayed on third LCD line of display Word scroll m...

Страница 13: ...of records Each time an Interval log is initiated a new lot is created The maximum number of Interval lots that may be stored is 100 If a 101st lot is attempted MAX LOTS will be displayed Some lots wi...

Страница 14: ...ng lot information is displayed on the third LCD line The line indicates in which lot the data will be placed and keeps track of the number of logged records taken The LOG tag is continuously on durin...

Страница 15: ...ating how much log space is available The LOG tag will be displayed on all 4 screens PLEASE WAIT WAITING SAVED with the log record number FREE with the number of free spaces available All log records...

Страница 16: ...tag blinking Press the pq keys to select a different lot Press CFM The instrument will display PLEASE WAIT CLEAR DONE is displayed for a few seconds after the selected Interval lot is deleted Delete R...

Страница 17: ...will be numbered 101 150 The lots are allocated successively provided available memory space until 999 is reached After this it is necessary to delete all the LOT logs to start over the numbering Del...

Страница 18: ...followed by EXPORT Press CFM to export the selected record or lot If CFM is not pressed in 10 seconds the USB host will become inactive The meter will display the percentage of export The export perc...

Страница 19: ...uage are suggested settings Other files may be visible depending upon computer settings All files stored will appear in this folder Adjust Font or column width appropriately Adjust the decimal places...

Страница 20: ...d SETUP menu there are no decisions to make regarding the pH measurement itself The meter will display 0 01 pH resolution and permit a 3 point buffer calibration from the following pH buffers 4 01 6 8...

Страница 21: ...electrode calibration Off or value Off Not Available First Calibration Point Allows the user to choose how the first point in calibration will be made Offset or point Offset Not Available automatical...

Страница 22: ...r list that includes the custom buffers and the standard buffers pH 1 68 4 01 pH 3 00 6 86 7 01 9 18 10 01 and 12 45 The custom buffers allow the user to calibrate in a buffer solution different from...

Страница 23: ...data for the corresponding buffer or for any buffer in the proximity of 0 2 pH If current buffer has no previous data stored and the calibration is not full five buffers the current buffer is added to...

Страница 24: ...bration point will be added to the existing data GLP will reflect the latest calibration data Older calibration buffers will be seen as blinking buffers Note Each time a buffer is confirmed the new ca...

Страница 25: ...of the electrode s reference impedance which should be kept low If the reference junction becomes fouled from a precipitate or coating the impedance will rise and cause the pH measurement to drift Thi...

Страница 26: ...ntly If necessary press the ARROW keys to select a different buffer value The along with STIR tag will be displayed and WAIT will blink on the LCD until the reading is stable When the reading is stabl...

Страница 27: ...9 962 12 286 35 95 1 688 2 991 4 026 6 842 6 989 9 108 9 919 12 128 40 104 1 693 2 990 4 037 6 837 6 983 9 069 9 881 11 978 45 113 1 700 2 990 4 049 6 834 6 979 9 040 9 847 11 834 50 122 1 707 2 991 4...

Страница 28: ...Maintenance for details Repeat calibration after cleaning Check Electrode Check Buffer CHECK ELECTRODE CHECK BUFFER appears when electrode slope exceeds the highest accepted slope limit You should che...

Страница 29: ...ion information Use the qp keys to scroll the stored information This includes the buffers used temperature of the buffer time and date of the last calibration the sensor serial number and the calcula...

Страница 30: ...expired I E CAL EXPIRED 2 DAYS AGO The probe serial number together with the current reading If a buffer is not from the last calibration the buffer tag will be displayed blinking In Standard Mode Con...

Страница 31: ...thoroughly with deionized water or tap water and then with some of the next sample to prevent cross contamination The pH reading is affected by temperature The temperature effect is compensated for u...

Страница 32: ...the instrument is in RELATIVE mV measurement mode The CAL tag will appear and the Absolute mV is displayed on the primary LCD line and AbS message on the secondary LCD line The will be displayed and W...

Страница 33: ...nt displays a blinking NO CAL message The relative mV calibration offset is displayed on the third LCD display Pressing the qp keys the last calibration date yyyy mm dd togetherwiththecurrentreadingis...

Страница 34: ...Or if enabled the number of days until the calibration alarm CAL DUE will be displayed i e CAL EXPIRES IN 2 DAYS The number of days since the calibration expired i e CAL EXPIRED 2 DAYS AGO The probe s...

Страница 35: ...asurement If the mV or temperature exceeds the limits of the sensor the message ELECTRODE OUT OF SPEC will scroll on the third LCD line The temperature will continue to be displayed If temperature exc...

Страница 36: ...filling solution electrolyte is more than 2 cm 1 below the fill hole add HI 7082 or HI 8082 3 5M KCl Electrolyte Solution for double junction electrodes Unscrewthefillholecoverduringmeasurementssothe...

Страница 37: ...7073 or HI 8073 Protein Cleaning Solution for 15 minutes Inorganic Soak in Hanna HI 7074 Inorganic Cleaning Solution for 15 minutes Oil grease Rinse with Hanna HI 7077 or HI 8077 Oil and Fat Cleaning...

Страница 38: ...with sample See mV and pH to determine what treatment you should use Measurement Rinse the electrode tip with distilled water Submerse the tip 3 cm 1 in the sample and stir gently for a few seconds Fo...

Страница 39: ...ped off D Verify no bubbles inside pH membrane The meter does not measure temperature is displayed on second LCD line Broken temperature sensor Replace the probe The meter fails to calibrate or gives...

Страница 40: ...and 2 custom buffers Relative mV Calibration Single point calibration Temperature compensation Automatic 5 to 100 C 23 to 212 F using integral temperature sensor Log feature Up to 1000 records organi...

Страница 41: ...with conical tip pH temperature electrode HI 36180 Glass body double junction refillable ORP temperature probe HI 36200 Plastic body single junction gel filled non refillable ORP temperature probe pH...

Страница 42: ...ORP Test Solution 240mV 25 C 77 F 500 mL HI 7021M ORP Test Solution 240mV 25 C 77 F 230 mL HI 7022L ORP Test Solution 470mV 25 C 77 F 500 mL HI 7022M ORP Test Solution 470mV 25 C 77 F 230 mL ORP PRET...

Страница 43: ...ed maintenance is not covered If service is required contact your local Hanna Office If under warranty report the model number date of purchase serial number and the nature of the problem If the repai...

Страница 44: ...Hanna Instruments reserves the right to modify the design construction or appearance of its products without advance notice MANEDGEPH 12 14...

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