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Figure 3n: Method screen – Sample Heater tab

3.10.3 Sample Heater tab (Option)

– If this Option is installed <click> on the Sample

Heater tab. The screen will appear as shown in Figure 3n. This tab contains the
parameters for the operation of the sample sparge tube heater. The sample heater
comes on at desorb and through the bake cycle to reduce carryover from run to
run.

Sample Heater Type –

Select

and the heater will be active during the bake

cycle. Select

Off

and the heater will be inactive during the bake cycle.

Pre Purge Time (min) –

The amount of time that the sample is purged with

pressurization gas before the pre heat function begins.

Preheat Temperature (

C) –

The temperature applied to the sample in the sparge

tube prior to purge.

Preheat Time (min) –

The duration of time, in minutes, that heat will be applied

to the sample in the sparge tube prior to purge.

Purge Temperature (

C) –

The temperature applied to the sample in the sparge

tube during purge.

Bake Temperature (

C) –

The temperature applied to the sparge tube during

bake.

Содержание Encon Evolution

Страница 1: ...Encon Evolution User Manual Original Operating Instructions Rev 4 5 ...

Страница 2: ......

Страница 3: ...esearch Institute Arhem HP is a registered trademark of Hewlett Packard Company Perkin Elmer is a registered trademark of Perkin Elmer Inc Varian is a trademark of Varian Inc Swaglock is a registered trademark of the Crawford Fitting Co Teflon and Vespel are trademarks of E I DuPont de Nemours and Company Inc Windows XP is a registered trademark of the Microsoft Corp Chemrex is a trademark of Chem...

Страница 4: ...provision of this warranty is prohibited by any federal state or municipal law that cannot be preempted Federal Communications Commission advisory This equipment has not been tested or found to comply with the limits of Class A computing device pursuant to part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipment is operated...

Страница 5: ...tice until the indicated conditions are completely understood and met AVERTISSEMENT La mention AVERTISSEMENT signale un danger Il attire l attention sur une procédure ou une pratique exploitation ou le comme ça s il n est pas correctement effectuée ou respectée peut entraîner des blessures de la mort Ne pas aller au delà d une mention AVERTISSEMENT jusqu à ce que les conditions indiquées sont comp...

Страница 6: ... 2 5 1 Interface Connection 2 5 2 Monitor Connection 2 5 3 Mouse Connection 2 5 4 Gas Connection 2 5 5 Power Connection 2 5 6 System Power Up Chapter 3 Encon Evolution Operation 3 1 Powering on the Encon Evolution 3 2 Opening the Encon Evolution Application 3 3 Powering off the Encon Evolution 3 4 Main Screen 3 5 Diagnostics Screen 3 6 Home Login Screen 3 7 Exit Icon 3 8 Options Screen 3 9 Sequenc...

Страница 7: ...nical Support Contact Information 4 2 Cleaning the Encon Evolution 4 3 Trap and MoRT Replacement 4 4 Diagnostics Screen 4 4 1 Icons 4 4 2 Manual Heater Control 4 4 3 Manual Valve Control 4 4 4 Flow Pathway Drop Down Menu 4 4 5 Flow 4 4 6 Flow Calibration 4 4 7 Trap Bake 4 4 8 Calibration 4 4 9 Drain 4 4 10 Manual Injection 4 5 Fuse Replacement 4 6 Spare Parts Website Chapter 5 Flow Diagrams ...

Страница 8: ...User Manual Introduction Chapter 1 ...

Страница 9: ... Control Patent Pending can help provide superior chromatographic resolution There are many different parameters that can affect peak shape especially with the early eluting compounds The peak shape of these compounds can be greatly affected by flow rates and pressure changes within the trap One of the problems is that the trap pressure is often different than the GC column head pressure When the ...

Страница 10: ...uch Screen Interface High Temperature capability Precise Temperature control Siltek sample pathway Dimensions 17 H x 11 W x 16 D 43 2cm x 27 94cm x 40 6cm Weight 45lbs 20 4kg Indoor Use Up to 2000 m altitude 10 C to 25 C operating temperature 5 C to 85 C storage temperature 10 to 90 relative humidity Programmable Time Ranges 999 99 min for all timed events Programmable Temp Ranges Trap ambient to ...

Страница 11: ...ile Compact Flash 2GB nonvolatile memory 20 local method storage with battery backup Display Std mouse optional keyboard optional touch screen USB communication Trap 1000 C min heating rate Cool down rate less than 90 sec Optional Sparge Glass Heater Up to 150 C glassware bake Temperature Accuracy Stability 1 C for all heated zones PID monitored Water Elimination Trap Operates at ambient to 210 C ...

Страница 12: ...vice and or repair of the instrument EST Analytical will assume no responsibility for customers failing to comply with the safety precautions stated Use of the Encon Evolution for something other than the intended use of the instrument is prohibited The use of the Encon Evolution is for trained personnel only Personnel operating the Encon Evolution should wear safety glasses safety shoes and glove...

Страница 13: ...l évolution Encon doivent porter des lunettes de protection chaussures de sécurité et gants le cas échéant Le Encon Evolution n est pas destiné à être utilisé dans un environnement dangereux Installation de l évolution Encon exige que rien ne bloque les orifices de ventilation du système l installation de l Evolution Encon exige que l instrument est placé sur une surface non inflammable capable de...

Страница 14: ...act your local authorities to learn about recycling options European Union This symbol above means that according to local laws and regulations your product should be disposed of separately from household waste When this product reaches its end of life take it to a collection point designated by local authorities Some collection points accept products for free The separate collection and recycling...

Страница 15: ...User Manual Installation and Setup Chapter 2 ...

Страница 16: ...operator must be thoroughly familiar with setup and installation sections of this manual NOTE Failure to follow the installation instructions as set forth could result in damage to the product and nullify the warranty 2 2 Work Space Requirements Dimensions 17 H x 11 W x 16 D 43 2cm x 27 94cm x 40 6cm NOTE Allow for added space on all sides of the instrument for proper ventilation The Encon Evoluti...

Страница 17: ... 3 Cut the strapping and lift the top box cover off the box and put aside Lift the outer box shell off the Encon Evolution and put aside Remove the excess foam packing material from the box and put aside 4 Remove the box inside the main Encon Evolution body This box contains the installation kit monitor mouse I O cable and power cable 5 With the help of another person tilt the Encon Evolution gent...

Страница 18: ... appareil pour assurer le bon refroidissement des composants de l instrument et de veiller à ce que le cordon d alimentation peut être facilement déconnecté NOTE Please retain all shipping material 2 5 System Setup Please refer to Figure 2b for a view of the back panel of the Encon Evolution Figure 2b View of the Encon Evolution s back panel 2 5 1 Interface Connection Install the supplied interfac...

Страница 19: ...inlet WARNING The transfer line is heated and needs to be installed so as to keep a minimum of 10 inches between the transfer line and any adjacent cables or objects AVERTISSEMENT La ligne de transfert est chauffé et doit être installé de manière à maintenir un minimum de 25 4 cm entre la ligne de transfert et les câbles ou les objets adjacents 2 5 5 Power Connection Plug power cord into the power...

Страница 20: ...User Manual Operation Chapter 3 ...

Страница 21: ...and the Windows XPeTM operating system 3 2 Open the Encon EV Application 1 The user will control the operation of the Encon EV using the mouse provided or the touch screen 2 click Encon EV on the desktop 3 The EST Analytical screen will appear while the application is loading 4 When the application has loaded the user will need to input the password in order to log on The default password is ESTAn...

Страница 22: ... to allow the user to simply click on the icon to load another screen of the program Figure 3a Main screen 3 5 Diagnostics Screen Refer to Maintenance and Troubleshooting chapter 4 for the Diagnostic Screen functions 3 6 Home Log On This icon serves a dual purpose 1 On the Main screen it serves as the user logon icon The logon allows for multiple users with various levels of access to the Encon EV...

Страница 23: ...ed This screen contains three tabs Instrument System Setup and User Accounts Figure 3b Options screen Instrument tab Instrument tab click the Instrument tab the screen will appear as shown in Figure 3b This provides information specific to the Encon EV instrument Encon Evolution Listed in the Encon Evolution box is the instrument name serial number and software version This information is used in ...

Страница 24: ...odels The GC Ready pull down provides the various selections for ready output signals TTL Low TTL Low must be selected when interfacing with a GC which gives a high voltage output signal when ready and a low voltage output signal when not ready TTL High TTL High must be selected when interfacing with a GC which gives a low voltage output signal when ready and a high voltage output signal when not ...

Страница 25: ...nits of psi or kPa The pressure unit selections are available from the pull down menu Trap Name Using the pull down menu select the type of trap installed in the Encon EV The trap type will be displayed on the Run Status and Diagnostics screens Trap Ready Max C This is the maximum temperature value that will be accepted in an Encon EV method to generate a purge ready signal for the analytical trap...

Страница 26: ...as been installed click the Install Trap button to display the install date Save To save the trap setup parameters click the Save button Trap Back Pressure This system pressure is determined from calibrating the purge flow When the desired purge flow is established from the Diagnostics screen the pressure will be displayed in the pressure display pop up box This figure must be manually added to th...

Страница 27: ...the Sequence icon the screen will appear as shown in Figure 3e Figure 3e Sequence screen Line Ten sequence lines are available for sample analysis by different Encon EV methods Ten different methods can be linked together to create a sequence Description User supplied description names Method The drop down lets the user select from the available methods Number of samples The number of samples anal...

Страница 28: ...ry Encon EV Method screen will consist of two tabs Method Setup and Purge Trap Each additional option to the Encon EV will have its own specific tab Figure 3f Method screen Method Setup tab 3 10 1 Method Setup tab click the Method Setup tab the screen will appear as shown in figure 3f This tab contains the parameters for the operation of the concentrator Overfill OPTION Included with Foam Detector...

Страница 29: ...lus the GC cool down time and equilibration time The GC Cycle Time can be set to a value of 0 0 999 9 minutes using the up down selection arrows Note The GC cycle time is used when the GC run time is longer than the purge and trap cycle time or when utilizing the dual concentrator option of the Encon Evolution system Start Delay min This is the time in minutes that the Encon EV will wait until sen...

Страница 30: ...rge tube Transfer Line Temperature C This is the temperature of the transfer line which connects the Encon EV to the GC Inlet This parameter can be set to a temperature between 35 C and 350 C in 1 C increments using the up down selection arrows Valve Oven Temperature C This is the temperature of the oven which contains the 8 port rotary valve and sample pathway tubing This parameter can be set to ...

Страница 31: ...purge dry purge desorb and bake Trap Ready Temperature C This is the temperature the adsorbent trap must reach before going to purge ready status The adsorbent trap will continue to cool free fall after reaching the set point The adsorbent trap ready temperature can be programmed to a value of 25 C to the maximum set point in 1 C increments MoRT Ready Temperature C This is the temperature the MoRT...

Страница 32: ...l flow can be programmed from 0 to 500ml min in 1ml min increments Initial Hold Time min This is the time in minutes the initial flow is maintained The initial hold time can be programmed from 0 to 99 9 minutes in 0 1 minute increments Ramp Rate ml min min This is the rate programmed in ml min the purge flow will increase after the initial hold time has expired to the desired final flow set point ...

Страница 33: ... below ambient to eliminate the possibility of analyte migration within the trap prior to desorb Dry Purge Flow Rate ml min This is the rate the pressurization gas flows through the adsorbent trap during the dry purge process The Dry Purge Flow Rate can be programmed from 1 to 500ml min in 1ml min increments Programmable Dry Purge Flow Control click the Program button to enable this feature This f...

Страница 34: ...ry Purge Time 5 minutes Initial Flow 40ml min Initial Hold Time 0 5 minutes Ramp Rate 40ml min per minute Final Flow 200ml min The Final Hold time at 200ml min would be 0 5 minutes Explanation It takes 4 minutes to ramp from 40ml min to 200ml min at a rate of 40ml min per minute The final hold time is calculated to be 0 5 minutes 5 minutes 0 5 minutes 4 minutes 0 5 minutes Dry Purge Time min This ...

Страница 35: ... adsorbent trap during bake The trap bake temperature can be programmed from 35 C to the set point in 1 C degree increments Programmable Trap Bake Temperature click the Program button to enable this feature The screen as shown in Figure 3k will appear Check the Enable Ramp Control box to program the desired settings Initial Temperature C This is the beginning temperature programmed in C The temper...

Страница 36: ...perature Control MoRT Bake Temperature C This is the set point temperature of the MoRT tube during bake The MoRT bake temperature can be programmed from 35 C to the set point in 1 C increments Programmable MoRT Bake Temperature click the Program button to enable this feature The screen as shown in Figure 3l will appear Check the Enable Ramp Control box to program the desired settings Initial Tempe...

Страница 37: ...o be entered by the User The final hold time is the calculated difference of the final bake time taken from the sum of the initial time and the ramping time needed to achieve the final temperature For Example Total Bake Time 10 minutes Initial Temperature 200 C Initial Hold Time 2 minutes Ramp Rate 10 C min per minute Final Temperature 260 C Final Hold time 2 minutes Explanation Since it takes 6 m...

Страница 38: ...to 999 9 minutes Ramp Rate ml min min This is the rate programmed in ml min the bake flow will increase after the initial hold time has expired to the desired final flow set point The ramp rate can be programmed from 1 ml min per minute to 500 ml min 1 ml min increments Final Flow ml min This is the ending bake flow rate programmed in ml min The final flow can be programmed from 0 to 500ml min in ...

Страница 39: ... This can be programmed from 1 to 10 cycles After the first bake cycle is completed the trap and MoRT will cool to approximately 60 C before beginning to heat for the next bake cycle Printing the Method click on the Printer icon The method can be printed if the Encon EV is interfaced to a printer Saving the Method click on the Save icon and the method will be saved NOTE After saving a method it mu...

Страница 40: ... will be active during the bake cycle Select Off and the heater will be inactive during the bake cycle Pre Purge Time min The amount of time that the sample is purged with pressurization gas before the pre heat function begins Preheat Temperature C The temperature applied to the sample in the sparge tube prior to purge Preheat Time min The duration of time in minutes that heat will be applied to t...

Страница 41: ...igure 3o Figure 3o Run Status screen The Run Status screen displays the current Encon EV instrument settings for real time monitoring of the concentrator and contains the buttons necessary to apply the Step To Start Stop and Hold functions Step To The Step To button will display the following functions Standby Purge Ready Purge Dry Purge Desorb Ready Desorb Preheat Desorb Bake Step to Standby With...

Страница 42: ...The position of the 8 port valve is displayed and the corresponding flow pathway is shown GC Ready Not Ready In the upper left corner of the Status screen is an icon of a GC When the GC is outlined in green it is ready When the GC is outlined in red it is not ready Temperatures C Displayed on the Run Status screen are the actual temperatures of the absorbent trap MoRT tube transfer line 8 port val...

Страница 43: ...aved Opening a saved Run Log click the Open icon All previously saved Error logs are available to be viewed 3 13 Reports Page Printing the Error Log click the Printer icon The Error Log can be printed if the Encon EV is interfaced to a printer Saving the Error Log click the Save icon The Error Log can be saved Opening a saved Error Log click the Open icon All previously saved Error Logs are availa...

Страница 44: ...are Figure 3q Help Screen Encon Evolution User Manual By placing the cursor and clicking on ENCON EV User Manual the user can view a PDF version of the operation manual Encon Evolution Software Update By placing the cursor and clicking on HOW TO Encon Evolution Updates the user can view the instructions to update the Encon Evolution software Encon Evolution Printer Installation By placing the curs...

Страница 45: ...r and follow instructions for transfer of applicable update files to instrument 5 When transfer of update files are complete open My Computer right click on Removable Drive and select Eject 6 Remove memory stick from USB port on instrument Encon EV update is now complete EXE Archive 1 Transfer Encon EV update to USB memory stick from desktop or laptop computer 2 Remove memory stick from computer a...

Страница 46: ... Control On 5 0 Note Set to 1 to 2psi below the inlet head pressure no more than 10psi Desorb Flow Control Off Desorb Preheat Temperature 245o C Desorb Temperature 250o C Desorb Time 0 5 minutes Trap bake temperature 260o C MoRT Bake Temperature 210o C Trap Bake Flow 85ml min 5ml purge volume 30ml min 25ml purge volume Trap Bake Time 6 minutes Trap Bake Cycles 1 Purge Temperature option Off Sparge...

Страница 47: ...User Manual Maintenance and Troubleshooting Chapter 4 ...

Страница 48: ... containing liquids during maintenance ONLY use replacement parts provided by EST Analytical CAUTION Before Maintaining and Servicing any component of the Encon Evolution the instrument must be 1 Turned off Note Windows should be turned off properly 2 Disconnected from the Power Supply 3 Hot Surfaces should be given time to cool 4 After servicing instrument all covers need to be placed back on the...

Страница 49: ... a clean damp lint free cloth Cloth should be dampened with water only Avoid any cleaning agents that could cause a hazard as a result of a reaction with parts of the equipment of with the material contained in it 2 Use canned air to remove any dust or lint from the fans or inside the unit 4 3 Trap MoRT Replacement 1 CAUTION Make certain the instrument is not running and the trap is cool ATTENTION...

Страница 50: ...replacement Refer to the Operations Chapter for further instructions NOTE Be sure the analytical trap is installed properly with the markings and the pre swaged ferrule at the top 4 4 Diagnostics Screen click the Diagnostics screen icon The Diagnostics screen will be displayed as shown in Figure 4a The Diagnostics screen contains the settings and controls necessary to manually operate and trouble ...

Страница 51: ...ut a ready signal When the image is outlined in red the GC is sending a not ready signal Trap icon Displays the trap type installed click the Trap icon and the Options screen will open to the System Setup tab To return to the Diagnostic screen click the Diagnostic screen icon Sparge Vessel icon click the Sparge Vessel icon and the Pressurization Valve PID calibration screen will open as shown if F...

Страница 52: ...point C Enter the desired set point SP temperature Heat to SP click the Heat to SP button The selected zone will heat to the entered set point The temperature will be maintained as selected until it is manually changed again or a method is loaded CAUTION Heating the trap or MoRT tube without flow may damage the trap sorbent materials or the MoRT tube Silco treated surface ATTENTION Le chauffage du...

Страница 53: ...ick the Flow pressurization valve icon and the pressurization valve screen will be displayed as in shown in Figure 4d Figure 4d Pressurization Valve manual setpoint screen Current Flow ml min Displays the current flow Setpoint ml min Enter the desired flow Flow to SP click the Flow to SP button this will activate the flow to the set point The flow will be maintained as selected until it is manuall...

Страница 54: ...5 9 and 5 10 Leak Check click Leak Check and the process will begin 1 The concentrator will pressurize to 20psi and then hold for 30 seconds 2 If the concentrator maintains the pressure 0 5psi the leak check passes 3 If the concentrator fails to reach or maintain the set point the 8 port valve will actuate and the concentrator will begin a secondary leak check 4 Upon completion of the secondary le...

Страница 55: ...he unit 2 If the flow is within 2 0ml min of the purge flow click Yes and the flow check passes 3 If the flow is 2 0ml min of the purge flow click No and the next pop up will ask if the flow is 5 0 ml min of the set point 4 If the flow is within 5 0ml min of the purge flow click No and the flow check fails Check for leaks and or restrictions 5 If the flow is within 5 0ml min of the purge flow clic...

Страница 56: ...meter to the vent bulkhead Choose the calibration flow to be calibrated Adjust the up down output arrows so that the actual flow from the vent bulkhead is the same as the calibration flow point Save the calibration Repeat this process for every calibration flow point to be adjusted Exit Flow Calibration and Step to Standby 4 4 7 Trap bake This function enables a manual bake of the trap and or MoRT...

Страница 57: ...ke Temperature C Set the bake temperature from 35 C up to the method set point in 1 C degree increments Bake Gas Bypass Select Off and during bake the gas flow pathway will be through the sparge tube Select On and during bake the gas flow pathway will be diverted and not flow through the sparge tube Enable Ramp Control click the Enable Ramp Control button to program the desired settings NOTE Enabl...

Страница 58: ...tion Since it takes 5 minutes to ramp from 40ml min to 240ml min at a rate of 40ml min The final hold time is calculated to be 3 minutes 10 minutes 2 minutes 5 minutes 3 minutes Start click Start to begin the manual bake Exit click Exit to return to the Diagnostics screen NOTE The remaining bake time and bake cycles will be displayed on the Status screen and not on the Diagnostics screen 4 4 8 Cal...

Страница 59: ...lowing options will be displayed Drain and Drain w Bake Here you can choose to manually drain the sparge vessel or to drain the sparge vessel and also bake the traps 4 4 10 Manual Injection This function allows you to manually inject your sample directly onto the trap of the Encon Evolution click the Manual Injection button and the software will instruct you on how to do the manual injection ...

Страница 60: ...E F14 F16 2A 250V SLO BLO TR5 TYPE F18 10A 250V SLO BLO 3AG TYPE DIO Board EST Part Number Z1838FP003 Fuse Number Description Type F1 F25 1A 250V SLO BLO TR5 TYPE F26 10A 250V SLO BLO TR5 TYPE IO Board EST Part Number Z1838FP002 Fuse Number Description Type F1 5A 250V SLO BLO TR5 TYPE F2 F3 6 3A 250V SLO BLO TR5 TYPE IO Board EST Part Number Z1838FP004 Fuse Number Description Type F1 2A 250V SLO B...

Страница 61: ...User Manual Flow Diagrams Chapter 5 ...

Страница 62: ...Figure 5 1 Standby Dry Purge Flow Diagram ...

Страница 63: ...Figure 5 2 Purge Flow Diagram ...

Страница 64: ...Figure 5 3 Desorb Ready Flow Diagram ...

Страница 65: ...Figure 5 4 Desorb Flow Control Flow Diagram ...

Страница 66: ...Figure 5 5 Desorb Auto Drain Flow Diagram ...

Страница 67: ...Figure 5 6 Desorb Flow Diagram ...

Страница 68: ...Figure 5 7 Bake with Bake Gas Bypass Flow On Flow Diagram ...

Страница 69: ...Figure 5 8 Bake with Bake Gas Bypass Flow Off Flow Diagram ...

Страница 70: ...Figure 5 9 Leak Check Flow Diagram 1 ...

Страница 71: ...Figure 5 10 Leak Check Flow Diagram 2 ...

Страница 72: ......

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