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Manual Microwave Peptide Synthesizer
600423 • Revision 2 • August 2017
15
Using the 4 mL Vessel for Smaller Scale
The 4 mL reaction vessel is used for small scale synthesis (below 0.1 mmol scale).
The 4 mL vessel does not have
a sprayhead. All additions and washes must be added manually by opening the top of the reaction vessel.
Connecting the 4 mL Vessel
1. Place a yellow ferrule and nut on the end of the thermowell. Insert the thermowell into the center
port of the reaction vessel top so that the bottom of the thermowell is on the bottom of the vessel.
Secure the thermowell with the nut.
2. Connect the RV Vent line to the side port of the reaction vessel top.
3. Connect the RV Drain line to the port on the bottom of the vessel.