15
Unload a Purification
Warning
»
Never flush or purge the system without a column mounted
or the column inlet and outlet tubing coupled together.
Flush the Column with Air
Empty the column of remaining solvents using the air flush
feature; see page 21.
Purge the System
Any pressure remaining after a purification can be released
using the purge feature; see page 21.
Unload the Run
When the purification is finished, unload the column and
rack(s). To avoid leakage, plug the column inlet and outlet
fittings and couple the column inlet and outlet tubes together
(see Figure 34).
Remove Racks in the Software
Unless the system has RFID
R
, racks that are unloaded have to
be removed manually in the software by selecting
None
in the
corresponding
Select Rack
drop-down list in the expanded
Rack
panel.
Figure 34.
When a run is finished, couple the column inlet and outlet
tubes together.
Unload a Purification
Flush the System
If the last purification of the day is performed with a
halogenated solvent (e.g. DCM), we recommend that you
assign methanol or a similar solvent to the inlet line used with
the halogenated solvent (see page 5) and flush with at least
30 mL (see page 20).
Shut Down the System
Warning
»
Failure to perform an orderly system shutdown may result in
user data corruption and/or remaining pressure.
An orderly system shutdown helps prevent data corruption.
For critical applications, the use of a suitable Uninterruptable
Power Supply (UPS) may help avoid data loss during a power
outage.
1. When the system is not processing, press
Menu,
Shut Down
,
and then
Yes
to confirm.
2. When the message saying it is safe to turn off the
system appears on the touch screen, turn off the system.
The power switch is located on the left side of the system;
see Figure 35.
3. If desired, unplug the power cord from the power outlet.
Figure 35.
The power switch is located on the left side of the system.
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