Beckman Coulter SA 3100 Скачать руководство пользователя страница 57

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PN 4237215AA (October 2011)

5-5

Figure 5.4 Analysis Screen

Analysis

Outgas

Figure 5.5 Outgas Screen

Outgas

Sample Information

screen

Содержание SA 3100

Страница 1: ......

Страница 2: ...WARNINGS CAUTIONS and IMPORTANTS alert you as follows WARNING Might cause injury CAUTION Might cause damage to the instrument IMPORTANT Might cause misleading results ...

Страница 3: ...ber 2011 iii Updated trademark information Updated all instances of Coulter Corporation or Coulter Electronics to Beckman Coulter Inc Revised the address to the Beckman Coulter address Deleted the Coulter Care Symbol CC ...

Страница 4: ...PN 4237215AA October 2011 ...

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Страница 16: ...PN 4237215AA October 2011 ...

Страница 17: ...PN 4237215AA October 2011 1 1 Screens Analysis Outgas Profiles Analysis ...

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Страница 23: ...PN 4237215AA October 2011 3 1 ...

Страница 24: ...3 2 PN 4237215AA October 2011 ...

Страница 25: ...PN 4237215AA October 2011 3 3 Figure 3 1 Shipping lnsert ...

Страница 26: ...3 4 PN 4237215AA October 2011 Vacuum Pump CAUTION Use only Balzers P3 pump oil in the vacuum pump Use of other oil may damage the pump and will void the pump warranty ...

Страница 27: ...PN 4237215AA October 2011 3 5 Figure 3 3 lnstalling Oil Mist Filter CAUTION Do not attach the vacuum line to the oil mist filter connector Doing so may damage the pump and the SA 3100 analyzer ...

Страница 28: ...3 6 PN 4237215AA October 2011 Figure 3 4 Connecting Vacuum Line to the Vacuum Pump ...

Страница 29: ...PN 4237215AA October 2011 3 7 ...

Страница 30: ...3 8 PN 4237215AA October 2011 Figure 3 6 Placing Vacuum Pump into Pump Shelf ...

Страница 31: ...tion WARNING The regulator supplied is designed for only nitrogen helium and other inert gases The regulator must not be used for any corrosive or hazardous gas WARNING To prevent valve damage and potential personal injury never use a nonstandard wrench or tool on any cylinder valve ...

Страница 32: ...onal injury do not force the regulator cylinder connection If the regulator does not screw into the cylinder valve outlet easily check for cross threading or contamination CAUTION Never use oil grease orTeflon7 tape on any cylinder or regulator valve or connection threads ...

Страница 33: ...PN 4237215AA October 2011 3 11 IMPORTANT The cylinder pressure must be at least 100 psig ...

Страница 34: ...3 12 PN 4237215AA October 2011 Figure 3 8 Gas Line Connections to the Analyzer ...

Страница 35: ...PN 4237215AA October 2011 3 13 IMPORTANT The cylinder pressure must be at least 100 psig ...

Страница 36: ...e to ports or fittings do not use any tools to remove or install port fittings Fittings are designed to seal when finger tight Figure 3 9 Port Fittings IMPORTANT Excess grease on O rings will be deposited on sample tubes causing weighing and analysis errors ...

Страница 37: ...PN 4237215AA October 2011 3 15 Figure 3 1 0 Seating the O ring ...

Страница 38: ...A October 2011 CAUTION Do not use any tools to remove or install saturation port adsorption port or outgas port fittings Fittings are designed to seal when finger tight Figure 3 1 1 Saturation Tube lnsert and Heat Sink ...

Страница 39: ...PN 4237215AA October 2011 3 17 Figure 3 1 2 Saturation Tube Installation 7 Analysis ...

Страница 40: ...3 18 PN 4237215AA October 2011 Figure 3 1 3 Analyzer Power up Figure 3 1 4 Analysis Screen ...

Страница 41: ...PN 4237215AA October 2011 3 19 Analysis Setup and Print Analysis ...

Страница 42: ...3 20 PN 4237215AA October 2011 Figure 3 1 5 Printer Installation Analysis Setup Configuration Configuration Printers Configuration Analysis Advanced Setup ...

Страница 43: ...PN 4237215AA October 2011 4 1 J ...

Страница 44: ...4 2 PN 4237215AA October 2011 ...

Страница 45: ...PN 4237215AA October 2011 4 3 Figure 4 1 SA 31 00 Analyzer Front View ...

Страница 46: ...4 4 PN 4237215AA October 2011 Figure 4 2 SA 3100 Analyzer Back View ...

Страница 47: ...PN 4237215AA October 2011 4 5 ...

Страница 48: ...4 6 PN 4237215AA October 2011 Figure 4 3 Analysis Screen Analysis ...

Страница 49: ...PN 4237215AA October 2011 4 7 Figure 4 4 Example of Nurneric Keypad on the Touch Screen Figure 4 5 Example of Alphanumeric QWERTY Keypad on the Touch Screen ...

Страница 50: ...4 8 PN 4237215AA October 2011 Analysis Analysis Analysis Analysis ...

Страница 51: ...PN 4237215AA October 2011 4 9 Outgas Figure 4 6 Outgas Screen Outgas Outgas Analysis Analysis ...

Страница 52: ...4 10 PN 4237215AA October 2011 Profile Figure 4 7 Profile Screen Sample Information ...

Страница 53: ...PN 4237215AA October 2011 5 1 ...

Страница 54: ...5 2 PN 4237215AA October 2011 Figure 5 1 Sample Tube Assembly ...

Страница 55: ...PN 4237215AA October 2011 5 3 Figure 5 2 Weighing the Sample Tube Assembly ...

Страница 56: ...5 4 PN 4237215AA October 2011 Figure 5 3 Adding Sarnple to the Sarnple Tube Analysis Outgas Outgas Outgas ...

Страница 57: ...PN 4237215AA October 2011 5 5 Figure 5 4 Analysis Screen Analysis Outgas Figure 5 5 Outgas Screen Outgas Outgas Sample Information Sample Information screen ...

Страница 58: ...5 6 PN 4237215AA October 2011 Profiles Figure 5 6 Sample lnformation Screen ...

Страница 59: ...October 2011 5 7 CAUTION Do not use any tools to remove or install saturation tube or adsorption tube fittings Fittings are designed to seal when finger tight Figure 5 7 Connecting the Sample Tube to an Outgas Port ...

Страница 60: ...5 8 PN 4237215AA October 2011 Outgas Outgas Outgas Outgas 1 Outgas ...

Страница 61: ...Sample Tube Assembly with Sample after Outgassing IMPORTANT Do not load the sample tube onto the analysis port until instructed to do so by a message on the touch screen Doing so may compromise analysis results Analysis Outgassed Samples Sample Information ...

Страница 62: ...5 10 PN 4237215AA October 2011 Figure 5 9 Outgassed Samples Screen Sample Information Analysis ...

Страница 63: ...oper safety equipment when handling liquid nitrogen including but not limited to safety glasses and low temperature thermal gloves WARNING Always temper new dewars by adding a small quantity of cryogen and swirling the liquid in the dewar before filling This reduces the risk of implosion and injury ...

Страница 64: ... Figure 5 1 1 Adding Liquid Nitrogen to Dewar IMPORTANT Do not load dewar into the dewer rack until instructed to do so by a message on the touchscreen Doing so will condense nitrogen onto the sample causing low surface area results ...

Страница 65: ...ctober 2011 5 13 CAUTION To avoid breaking glassware do not force a dewar into the dewar rack if it is difficult to install Make sure the top of the dewar is free of ice and try again Figure 5 12 lnstalling the Dewar ...

Страница 66: ...October 2011 IMPORTANT Do not fill the dewar above 2 cm from the top Doing so will cause temperature changes due to rapid evaporation and may cause inaccurate results Figure 5 13 Filling the Dewar Using the Dewar Funnel ...

Страница 67: ...PN 4237215AA October 2011 5 15 Figure 5 14 lnstalling Dewar Lid ...

Страница 68: ...nstructed to do so by a message on the touch screen Doing so may cause explosive pressures to develop in the sample tube CAUTION Do not remove the sample tube until instructed to do so by a message on the touch screen Doing so may reduce the lifetime of the vacuum system ...

Страница 69: ...PN 4237215AA October 2011 5 17 Figure 5 1 5 Specific Surface Area Result Screen ...

Страница 70: ...5 18 PN 4237215AA October 2011 ...

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Страница 72: ...6 PN 4237215AA October 2011 ...

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Страница 79: ...PN 4237215AA October 2011 6 Figure 6 1 ldealized V T Plots ...

Страница 80: ...6 PN 4237215AA October 2011 ...

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Страница 82: ...6 PN 4237215AA October 2011 ...

Страница 83: ...PN 4237215AA October 2011 7 1 ...

Страница 84: ...7 2 PN 4237215AA October 2011 ...

Страница 85: ...PN 4237215AA October 2011 7 3 ...

Страница 86: ...7 4 PN 4237215AA October 2011 Analysis Outgas Setup and Print Figure 7 1 Setup and Print Screen Configuration Figure 7 2 Configuration Screen Key Click ...

Страница 87: ...PN 4237215AA October 2011 7 5 Printer Setup and Print Analysis Profile New Profile ...

Страница 88: ...7 6 PN 4237215AA October 2011 ...

Страница 89: ...PN 4237215AA October 2011 7 7 ...

Страница 90: ...7 8 PN 4237215AA October 2011 ...

Страница 91: ...PN 4237215AA October 2011 7 9 Profile Analysis Outgas Setup and Print Profile Outgas Analysis Figure 7 3 Profile Screen ...

Страница 92: ...7 10 PN 4237215AA October 2011 Profiles Figure 7 4 Profiles Screen Profile Outgas Analysis Profiles Profiles Profiles New Profile ...

Страница 93: ...PN 4237215AA October 2011 7 11 Figure 7 5 New Profile Screen Profiles Profiles Setup and Print Outgas Analysis Profiles Setup Outgas Analysis Profile New Profile ...

Страница 94: ...7 12 PN 4237215AA October 2011 Profile New Profile Profile Profiles New Profile Adsorbate Sensitivity Category ...

Страница 95: ...PN 4237215AA October 2011 7 13 Figure 7 6 Category Screen Printer Output Calculations Calculation ...

Страница 96: ...7 14 PN 4237215AA October 2011 Figure 7 7 Calculations Screen Calculation Calculations Calculation Figure 7 8 BET Calculation Screen ...

Страница 97: ...PN 4237215AA October 2011 7 15 Calculation Calculations Calculation Figure 7 9 BJH Calculations Screen Calculation Calculations Calculation Calculation ...

Страница 98: ...7 16 PN 4237215AA October 2011 Calculations Calculation Calculation Calculations Calculation ...

Страница 99: ... Table 7 1 Optimal Sample Quantity Estimated Specific Surface Area Mass of Sample for Analysis 30 m 2 g 0 1 g 0 2 g 10 m 2 g 30 m 2 g 0 3 g 3 m 2 g 9 9 m 2 g 1 g 2 m 2 g 2 9 m 2 g 1 5 g 1 5 m 2 g 1 9 m 2 g 2 g 1 m 2 g 1 4 m 2 g 3 g ...

Страница 100: ...7 18 PN 4237215AA October 2011 ...

Страница 101: ...PN 4237215AA October 2011 7 19 Figure 7 1 1 Sample Tube Assembly ...

Страница 102: ...7 20 PN 4237215AA October 2011 Figure 7 12 Weighing the Sample Tube Assembly Using an Analytical Balance ...

Страница 103: ...PN 4237215AA October 2011 7 21 Figure 7 1 3 Adding Sample to the Sample Tube ...

Страница 104: ...7 22 PN 4237215AA October 2011 Sample Information Outgassed Samples Sample Information ...

Страница 105: ...PN 4237215AA October 2011 7 23 Profile List Outgas Outgas Analysis Outgas Outgas Outgas Figure 7 14 Outgas Screen Outgas Sample Information ...

Страница 106: ...7 24 PN 4237215AA October 2011 Figure 7 1 5 Sample lnformation Screen Sample Information Profile List Outgas ...

Страница 107: ...PN 4237215AA October 2011 7 25 CAUTION Do not use any tools to remove or install port fittings Fittings are designed to seal when finger tight ...

Страница 108: ...7 26 PN 4237215AA October 2011 Figure 7 16 Connecting the Sample Tube to an Outgas Port Outgas Analysis Outgas Outgas ...

Страница 109: ...PN 4237215AA October 2011 7 27 Outgas ...

Страница 110: ...7 28 PN 4237215AA October 2011 Figure 7 17 Weighing the Sample Tube Assembly and Sample after Outgassing ...

Страница 111: ... IMPORTANT Do not load the sample tube onto the analysis port until instructed to do so by a message on the touch screen Doing so may compromise analysis results Outgassed Samples Outgas Analysis Figure 7 18 Outgassed Samples Screen Outgassed Samples ...

Страница 112: ...11 Sample Information New Sample New Sample Sample Information Outgassed Samples Sample Information Analysis Analysis CAUTION Do not use any tools to remove or install port fittings Fittings are designed to seal when finger tight ...

Страница 113: ...PN 4237215AA October 2011 7 31 Figure 7 19 Connecting the Sample Tube to the Analysis Port ...

Страница 114: ...emper new dewars by adding a small quantity of liquid nitrogen and swirling the liquid in the dewar before filling This reduces the risk of implosion and injury IMPORTANT Do not load the dewar onto the dewar rack until instructed to do so by a message on the touch screen Doing so will condense nitrogen on the sample causing low surface area results Figure 7 20 Adding Liquid Nitrogen to Dewar ...

Страница 115: ...PN 4237215AA October 2011 7 33 Figure 7 21 Loading the Dewar into Dewar Rack ...

Страница 116: ...October 2011 IMPORTANT Do not fill the dewar above 2 cm from the top Doing so will cause temperature changes due to rapid evaporation and may cause inaccurate results Figure 7 22 Using the Dewar Funnel to Fill the Dewar ...

Страница 117: ...re 7 23 Installing Dewar Lid Analysis Analysis Screen Outputs Screen Outputs WARNING Do not remove the dewar until instructed to do so by a message on the touch screen Doing so may cause explosive pressures to develop in the sample tube ...

Страница 118: ...7 36 PN 4237215AA October 2011 CAUTION Do not remove the sample tube until instructed to do so by a message on the touch screen Doing so may reduce the lifetime of the vacuum system ...

Страница 119: ...PN 4237215AA October 2011 7 37 Screen Outputs Analysis Outgas Setup and Print ...

Страница 120: ...7 38 PN 4237215AA October 2011 Setup Advanced Setup Advanced Setup ...

Страница 121: ...PN 4237215AA October 2011 7 39 Setup and Print ...

Страница 122: ...7 40 PN 4237215AA October 2011 Analysis Figure 7 24 Advanced Setup Screen CAUTION Do not press the key Changes should be made only by or when directed by Beckman Coulter personnel Analysis ...

Страница 123: ...PN 4237215AA October 2011 ...

Страница 124: ...PN 4237215AA October 2011 CAUTION Do not use any tools to remove or install port fittings Fittings are designed to seal when finger tight ...

Страница 125: ...PN 4237215AA October 2011 Figure 8 1 Port Fittings IMPORTANT Excess grease on O rings will be deposited on sample tubes causing weighing and analysis errors ...

Страница 126: ...PN 4237215AA October 2011 Figure 8 2 Seating the O ring ...

Страница 127: ...PN 4237215AA October 2011 CAUTION Use only Balzers P3 pump oil in the vacuum pump Use of other oil may damage the pump and will void the pump warranty ...

Страница 128: ...PN 4237215AA October 2011 Figure 8 4 Draining Vacuum Pump Oil ...

Страница 129: ...PN 4237215AA October 2011 CAUTION Use only Balzers P3 pump oil in the vacuum pump Use of other oil may damage the pump and will void the pump warranty ...

Страница 130: ...PN 4237215AA October 2011 Figure 8 5 Rinsing the Fan Filter ...

Страница 131: ...PN 4237215AA October 2011 Figure 8 6 Oil Mist Filter Installation ...

Страница 132: ...PN 4237215AA October 2011 WARNING This procedure is NOT to be used for replacement or installation of gas cylinders containing corrosive or hazardous gases Figure 8 7 Gas Cylinder and Pressure Regulator ...

Страница 133: ...gulator cylinder connection If the regulator does not screw into the cylinder valve outlet easily check for cross threading or contamination CAUTION Never use oil grease or Teflon tape on any cylinder or regulator valve or connection threads IMPORTANT The cylinder pressure must be at least 100 psig ...

Страница 134: ...PN 4237215AA October 2011 Setup and Print Analysis ...

Страница 135: ...PN 4237215AA October 2011 ...

Страница 136: ...PN 4237215AA October 2011 ...

Страница 137: ...PN 4237215AA October 2011 ...

Страница 138: ...PN 4237215AA October 2011 ...

Страница 139: ...PN 4237215AA October 2011 A 1 ...

Страница 140: ...A 2 PN 4237215AA October 2011 Figure A l SA VIEW Program Window ...

Страница 141: ...PN 4237215AA October 2011 A 3 ...

Страница 142: ...A 4 PN 4237215AA October 2011 ...

Страница 143: ...PN 4237215AA October 2011 A 5 ...

Страница 144: ...A 6 PN 4237215AA October 2011 Sample Information ...

Страница 145: ...PN 4237215AA October 2011 A 7 Figure A 2 Open Report File Dialog Box Figure A 3 Analysis Log Dialog Box ...

Страница 146: ...A 8 PN 4237215AA October 2011 ...

Страница 147: ...PN 4237215AA October 2011 A 9 Figure A 4 Overlayed Results Dialog Box ...

Страница 148: ...A 10 PN 4237215AA October 2011 ...

Страница 149: ...PN 4237215AA October 2011 A 11 Figure A 5 Print Preview Screen ...

Страница 150: ...A 12 PN 4237215AA October 2011 ...

Страница 151: ...PN 4237215AA October 2011 A 13 ...

Страница 152: ...A 14 PN 4237215AA October 2011 Figure A 6 SA VIEW Program Copyright Dialog Box ...

Страница 153: ...ctober 2011 CAUTION If a sample is melted it will probably sublime within the instrument and vacuum pump This will cause severe operational problems if this happens contact your Beckman Coulter Service Representative ...

Страница 154: ...PN 4237215AA October 2011 Outgas ...

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Страница 157: ...PN 4237215AA October 2011 INDEX 1 A B C D ...

Страница 158: ...PN 4237215AA October 2011 E F G H I K L M N ...

Страница 159: ...PN 4237215AA October 2011 O P R ...

Страница 160: ...PN 4237215AA October 2011 S T U ...

Страница 161: ...PN 4237215AA October 2011 V W ...

Страница 162: ...PN 4237215AA October 2011 ...

Страница 163: ...PN 4237215AA October 2011 REFERENCES 1 ...

Страница 164: ...PN 4237215AA October 2011 ...

Страница 165: ... stylized logo and COULTER are trademarks of Beckman Coulter Inc and are registered in the USPTO All other trademarks service marks products or services are trademarks or registered trademarks of their respective holders ...

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