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Anatel A643a - Calibration and Validation

89 of 220

S -

- E

n 1

Anatel

Operator Manual

12)

Press

Enter

to view the average of the blank replicates, which establishes the

reference for the validation, then press it again to continue. Note that only one blank is
analyzed, not one blank per validation level.

13)

Remove the blank bottle and insert the requested standard vial. Press

Enter

and its

contents are sampled, analyzed and reported.

14)

Repeat

step 12

for each of the selected validation standard levels. The blank average

is is analyzed only once during the validation process and is subtracted from each
replicate average. The results for each are displayed once all analyses have been
completed.

Rep #1 = xxx ppb

Rep #2 = xxx ppb

Rep #3 = xxx ppb

Press Enter

Fig 6-11 :

Analysis Replicates

Blank ave=xxx

Press Enter

Fig 6-12 :

Blank Average

xxx ppb std

response=XXX ppb

deviation=XX%

Press Enter

Fig 6-13 :

Analysis Results

Fig 6-14 :

TOC Validation Results

Содержание A643

Страница 1: ...Operator Manual ANATEL A643a TOC ANALYZER...

Страница 2: ......

Страница 3: ...are Setup 22 2 3 Hardware Installation 26 2 3 1 Mounting 26 2 3 2 Plumbing Connections 29 2 3 3 Communications Connections 33 2 3 4 Power Connections 36 2 4 Analyzer Initialization 36 3 Network Instal...

Страница 4: ...rab Samples 76 5 7 2 On Line Samples 78 6 Calibration and Validation 6 1 General Information 81 6 2 TOC Calibration 82 6 3 TOC Validation 87 6 4 Conductivity Calibration 91 6 5 System Suitability 95 6...

Страница 5: ...11 12 VDC Bias Output 11 1 General Information 145 11 2 Hardware Setup 145 12 Serial Communications 12 1 General Information 147 12 2 Hardware Setup 147 12 3 Anatel A643a Command Set 149 12 3 1 Mode...

Страница 6: ...l Tests184 14 4 3 I O Tests 185 Appendix A Service Procedures A 1 Return Procedures 189 A 2 Technical Support Information 189 Appendix B Specifications and Accessories B 1 Performance Specifications 1...

Страница 7: ...hich if not met could cause serious personal injury and or death Do not move beyond a warning until all conditions have been met CAUTION A caution is used to indicate a condition which if not met coul...

Страница 8: ...e electronics and or hydraulics may result in personal injury and damage to the A643a A643a TOC Analyzer Warnings and Cautions CAUTION It is extremely important that the A643a TOC Analyzer be plumbed...

Страница 9: ...cerning the collection retention access and retrieval of data as electronic records The instrument uses no electronic signature s thus those parts of the rule referring to electronic signature s are n...

Страница 10: ...or other adverse environmental elements WARNING The calibration and validation processes employed by the Anatel A643a use chemicals and a photooxidation technology which produces hazardous waste bypr...

Страница 11: ...are This warranty shall not apply to damage resulting from attempts by personnel other than Hach Ultra representatives or factory authorized and trained personnel to install repair or service the inst...

Страница 12: ...gust 1999 Anatel Corporation Edition 5 April 2000 Anatel Corporation Edition 6 August 1997 Anatel Corporation Edition 7 July 2001 Anatel Corporation Edition 8 November 2001 Anatel Corporation Edition...

Страница 13: ...A643a applications include on line organic contamination detection in pharmaceutical water systems as well as the convenience of being able to perform TOC analyses in the laboratory The Anatel A643a...

Страница 14: ...surements in addition to providing local printouts as the data are reported C80 Controller The C80 Controller is the control display device for the Anatel A643a Analyzer The C80 allows operational and...

Страница 15: ...on and instrument performance can be validated on line using Anatel s Validation Kit USPCompliancefor Conductivity and System Suitability The Anatel A643a s limit response and response efficiency are...

Страница 16: ...her examining the exact TOC values on a printout the user can determine if the trend is critical and respond accordingly UV Detect Technology UV Detect is an optional feature Analyzers with UV Detect...

Страница 17: ...Anatel A643a Introduction 17 of 220 RPS June 2007 Edition 12 Anatel Operator Manual Fig 1 3 Anatel A643a P TOC Analyzer Components...

Страница 18: ...18 of 220 Introduction Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 19: ...llation of the Anatel A643a System Each Analyzer is furnished with an Installation Kit Anatel A643a S P N FG2041101 Anatel A643a P P N FG2041201 and must consider these preparatory and installation is...

Страница 20: ...the components Carefully remove the equipment verify the enclosed packing list and check once again for obvious damage Each Anatel A643a Installation Kit contains Power Cord Network Tee Terminator 15...

Страница 21: ...ator on the open couplings at each end of the configuration Proper termination is crucial for reliable communications 5 Plug both components into an AC power source A power cord is integral to Anatel...

Страница 22: ...The same programming should be performed on stand alone Anatel A643a P Analyzers to assure that they are operating properly 2 2 3 1 System Time Each Analyzer s onboard clock is set at the factory duri...

Страница 23: ...and Down Keys to move the flashing cursor left or right respectively to highlight the division of the Date Time display that is to be changed such as the day 6 Press Enter to enable the Controller s...

Страница 24: ...er so that its report functions are now synchronized to the clock calendar setting 2 2 3 2 Analyzer Name Note Default Serial Number The first step in setting up an Anatel A643a Analyzer is to name it...

Страница 25: ...Channel ID Number The second line presents its default name its Serial Number with the block cursor flashing on the first character 3 Use the Up and Down Keys to move the cursor and highlight the char...

Страница 26: ...one Analyzer to have the same Name Duplicate Sensor Names may cause confusion when reviewing printed reports 2 3 Hardware Installation Once the Anatel A643a hardware components have been checked and i...

Страница 27: ...The air is filtered through an intake located on the bottom of the Analyzer Do not allow the air flow through the intake or outlet filters on the bottom of the instrument to be obstructed or to get we...

Страница 28: ...ent in conjunction with two 1 4 tie down tabs positioned along its bottom The mounting dimensions for the Analyzer are shown below Anatel A643a S Analyzers combine the measurement cell requisite elect...

Страница 29: ...lts The following plumbing communications and power connections are identical for the Anatel A643a S and Anatel A643a P Analyzers Note The terms Anatel A643a and Analyzer in th following instructions...

Страница 30: ...the Analyzer 2 3 2 2 Water I O Tubing A length of 1 4 PFA perfluoroalkoxy resin sample tubing and a length of 1 8 OD polypropylene drain tubing are supplied with each Anatel A643a Analyzer The suitab...

Страница 31: ...olation valve by opening and closing it fully several times before connecting the Analyzer in order to avoid introducing debris through the inlet plumbing 2 Noting its flow direction connect the 15 mi...

Страница 32: ...be adversely affected 8 Make sure the sample vessel is installed and securely tightened on the calibration assembly 9 Leak test the connections by slowly opening the upstream isolation valve to intro...

Страница 33: ...unications between the C80 Controller and Anatel A643a Analyzer 1 Grasp the end of the 3 foot local cable attached to the C80 Controller and noting the alignment of its internal pins gently push it on...

Страница 34: ...m its power source 2 Remove the I O Connector Block from the bottom of the Anatel A643a analyzer by loosening the four retaining screws A medium flat blade screwdriver may be required 3 Loosen and rem...

Страница 35: ...al to the Analyzer s TOC reading for external analog devices INPUTS is a digital connection allowing limited supervisory control of the Analyzer by a remote device or switch Connecting to the IN1 term...

Страница 36: ...he ground pin 2 4 Analyzer Initialization With the plumbing communications and power connections properly established the Anatel A643a Analyzer can be initialized and placed into operation Because the...

Страница 37: ...Manual Menu 4 Select Modes then press Enter to access its submenu 5 Specify Special Modes and press Enter to display the available options 6 Use the Up and Down Keys to specify Clean 7 Press Enter to...

Страница 38: ...nstrument to complete several analyses before accepting the reported data as valid 10 Specify Auto TOC and press Enter to initiate automatic analysis based on the factory default parameter settings 11...

Страница 39: ...associated Controller C80 Controllers are assigned Network addresses It is recommended these assignments be made during Operational Verification as described in Operational Verification on page 20 bef...

Страница 40: ...ign other Channel IDs as necessary The Up and Down Keys are used to access other Channel IDs that are not presently visible in the display 8 With all of the Channel ID Serial Number crossreference ass...

Страница 41: ...onent connected through an individual tee connector using a local cable no longer than 3 feet The A Net trunk line can extend a total of 3000 feet not including these local cable lengths If the trunk...

Страница 42: ...ve termination In these installations an AC powered terminator P N FG2006501 120 VAC 60 Hz FG2006601 230 VAC 50 Hz must be connected to the open coupling at each end of the Network and then plugged in...

Страница 43: ...FF and disconnect the power cord from its source 2 Remove the I O Connector Block from the bottom of the Sensor by loosening the four thumbscrews 3 Loosen and remove the two Phillips head screws that...

Страница 44: ...ain relief plate 7 Replace the I O Connector Block on the bottom of the Sensor taking care not to pinch any wires and secure it in place by tightening the thumbscrews 8 Reconnect the power cord and tu...

Страница 45: ...oller display simultaneously provides data from multiple Analyzers The Controller s faceplate also contains a set of Channel ID LEDs which reflect the operational status of each connected Analyzer and...

Страница 46: ...r or character While an Edit Mode is employed to change Anatel A643a parameter values there is no temporary screen All parameter changes are made in real time and the displayed values are those that a...

Страница 47: ...Enter to access its submenu 4 Specify Contrast Adj and press Enter once again to display its parameter screen 5 Use the Up and Down Keys to lighten or darken the display as necessary 6 With the contra...

Страница 48: ...Analyzer through another Controller the conflict is reported and access is denied to the second device Press the Esc Key to return to the original menu 4 5 1 The Single Channel Detailed analysis data...

Страница 49: ...on its running average over the last hour This trend indication initially appears at the conclusion of the instrument s second analysis cycle If no direction is denoted the TOC level has not changed...

Страница 50: ...ted instruments simply by pressing the Up and Down Keys once the Channel display is presented Pressing the Chnl Key twice displays the checksum value of the instrument s controlling EPROM as well as i...

Страница 51: ...they have been installed and powered up A list of the Analyzer s current parameter settings is available through the Print Setup menu selection see Printouts on page 117 The Anatel A643a s factory def...

Страница 52: ...alibrations which are not affected Outputs mA Range 4 to 20mA TOC Zero Scale 0 ppb TOC Full Scale 1000 ppb Conductivity Zero Scale 0 S cm U Conductivity Full Scale 20 S cm U Temperature Zero Scale 5 C...

Страница 53: ...Analysis Setup and press Enter 5 Specify More Setup press Enter to access its submenu and select Sampl Defalt 6 Use the Up and Down Keys to specify Factory Defalt 7 Press Enter to display the Factory...

Страница 54: ...ically output to the printer assuming one is attached These records include the time the parameter and the date of the change in addition to identifying the person authorized to make the modification...

Страница 55: ...ication is five alphanumeric characters and case sensitive 9 Press Enter to advance to the next character and similarly select it 10 Repeat the selection procedure to define the other characters 11 Wi...

Страница 56: ...its default setting of 00000 18 Press Enter and the flashing block cursor cursor becomes a flashing underscore 19 Use the Up and Down Keys to select the initial character in the password 20 Press Ente...

Страница 57: ...nsated values are displayed as if the solution was being measured at 25 C Compensated conductivities are displayed as S C This calculation provides consistency from one analysis reading to the next re...

Страница 58: ...esistivity Output on page 134 Note Uncompensated Resistivity may be chosen but this selection is for display only and does not generate an alarm as the USP limits are not checked in this case 7 Use th...

Страница 59: ...and reporting continues until manually interrupted by the user or until a critical fault is encountered To select the Auto TOC Mode 1 With the desired Analyzer selected in any View press Manual to di...

Страница 60: ...oxidation begins This interval varies depending on the organic content of the water The nature of the oxidation curve determines the sample to be one of the following Profile Types Conductivity is alw...

Страница 61: ...ry large organics with a high molecular weight or organics that contain some element which resists oxidation As TOC levels vary the location of this transition shifts but the accuracy of the measureme...

Страница 62: ...1 Auto TOC Software Setup There are several parameters which define Anatel A643a operation in the Auto TOC Mode These variables include setting the Sample and Cycle Times as well as the instrument s S...

Страница 63: ...asure sample resistivity Even minute amounts of residual oxidation products will increase the conductivity of a high purity water sample considerably The Anatel A643a compensates the reported conducti...

Страница 64: ...Time 2 Press Enter to access its parameter screen The current Sample Timeis displayed in an hour minute second format and represents duration not clock time The flashing block cursor highlights the h...

Страница 65: ...xt analysis begins immediately To set the instrument s Cycle Time 1 With the Times Cycle Menu displayed use the Up and Down Keys to specify Cycle Time 2 Press Enter to access its parameter screen The...

Страница 66: ...ling Mode setting determines the state of the Analyzer s internal valves during oxidations and the Idle Time interval if any that occurs between the completion of a TOC analysis and the initiation of...

Страница 67: ...the instrument s Sample Vessel 9 With the desired Sampling Mode setting indicated press Enter to enable it 10 Press Esc repeatedly to exit this function and return to the normal display 5 5 1 4 Cycle...

Страница 68: ...d setting TOC Idle displays the data from the last TOC analysis during the Cycle Time Idle interval TOC Purge displays conductivity or resistivity and temperature data during the instrument s Idle Tim...

Страница 69: ...Sensor The Model Number of the instrument SN The Serial Number of the instrument ID Its Channel ID Number Name The user entered name of the instrument TOC LIMIT The instrument s set TOC alarm limit S...

Страница 70: ...ey to display its submenu 2 Use the Up and Down Keys to specify Sensor Setup 3 Press Enter to access it submenu 4 Specify Display Print and press Enter 5 Select Printer Setup from the Display Print me...

Страница 71: ...repeatedly to exit this function and return to the normal display 5 6 The Purge Mode In the Purge Mode the Anatel A643a s internal sample valve is open to permit sample water to continuously flow thro...

Страница 72: ...nductivity or resistivity level exceeds a userdefined percentage in two successive analyses The Purge Printout reports the following values Fig 5 37 Selecting the Purge Mode Table 5 3 Purge Printout R...

Страница 73: ...up Key to display its submenu 2 Use the Up and Down Keys to specify Sensor Setup 3 Press Enter to access its submenu 4 Specify Display Print from among the available selections and press Enter to disp...

Страница 74: ...to select the specified format A flashing cursor highlights the current value Timed Purge Print If Timed Purge Print is selected a flashing block cursor highlights the minutes division 9 Use the Up a...

Страница 75: ...s desirable The Manual Samples menu selection allows the user to conduct a single sample analysis when necessary The Manual Mode is used to interrupt the current analysis in order to start a new analy...

Страница 76: ...l grab sample measurement 1 With the desired Analyzer selected in any View press the Manual Key to access its menu selections 2 Use the Up and Down Keys to specify Manual Samples 3 Press Enter to disp...

Страница 77: ...activated and the measurement cell is flushed with the sample solution before it is analyzed The results are displayed at the conclusion of the analysis cycle 10 Press Enter and the average TOC readi...

Страница 78: ...line sample measurement 1 With the desired Analyzer selected in any View press the Manual Key to access its menu selections 2 Use the Up and Down Keys to specify Manual Samples 3 Press Enter to displa...

Страница 79: ...o return to the Online Samples Menu 8 Use the Up and Down Keys to specify Manual 9 Press Enter to access its parameters and initiate a single analysis The Duration of the sampling period is reported d...

Страница 80: ...80 of 220 Anatel A643a Setup Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 81: ...standards and blanks in order to determine instrumental response Each procedure is prompted by a series of menus and all analyses are performed automatically The necessary materials are available thr...

Страница 82: ...the percent slope change SC of the new calibration is 15 of the factory calibration the instrument indicates that the new calibration has passed If the result is 15 of the factory calibration the Ana...

Страница 83: ...to the analyzer using a container closure system that includes a 50 mL glass vial VWR cat 16171341 a 20 mm teflon coated stopper VWR cat 16171561 and a 20 mm crimp top aluminum seal VWR cat 16171829 T...

Страница 84: ...nce they are properly entered press Enter to continue 11 If any changes must be made to the standard concentrations or the number of replicates press Esc followed by Enter to abort the procedure Immed...

Страница 85: ...d standard 250 500 or 750 ppb Press Enter and its contents are sampled analyzed and reported 15 Repeat step 14 for each of the selected standard levels The blank average is subtracted from each replic...

Страница 86: ...ibration is deemed unacceptable A opportunity to repeat the calibration procedure using new sucrose standards will be given 18 Once the calibration procedure is complete remove the standard vial and r...

Страница 87: ...page 39 it is important to confirm the instrument s Serial Number before proceeding Operation of the wrong Analyzer could result in water leakage from the sample vessel when it is removed during this...

Страница 88: ...te the validation results 9 Press Enter The analyzer will asked if the C of A values have been entered If not press Esc to enter the C of A values once they are properly entered press Enter to continu...

Страница 89: ...vial Press Enter and its contents are sampled analyzed and reported 14 Repeat step 12 for each of the selected validation standard levels The blank average is is analyzed only once during the validati...

Страница 90: ...test results and initiate a printout of the data If the response deviation exceeds 15 the corresponding results are displayed and the validation is deemed unacceptable The opportunity to repeat the va...

Страница 91: ...conductivity solution measurement must be within 2 of the reported label concentration Note Refer to Standard Operating Procedure SOP 643 3 for complete instructions on performing this procedure To pe...

Страница 92: ...is drained 7 Remove the shroud protecting the sample vessel by loosening the two screws that secure it 8 Insert the calibration resistor into the receptacle provided in the end lid until it firmly co...

Страница 93: ...ntact with the exposed needle could cause serious injury 12 Three replicates are run and the results are reported in S cm The results are displayed once all analyses have been completed The instrument...

Страница 94: ...tion is unacceptable The opportunity to repeat the procedure using a new conductivity standard will be given 14 Once the conductivity calibration procedure is complete remove the standard vial and rei...

Страница 95: ...to display its submenu 4 Use the Up and Down Keys to specify Suitability If the chosen Analyzer is connected to an A Net network on which other instruments reside the analyzer will prompt to confirm t...

Страница 96: ...r 10 Press Enter to confirm both Certificate of Analysis values have been properly entered 11 Remove the empty sample vessel and insert the blank vial Press Enter and its contents are sampled and anal...

Страница 97: ...standard The 1 4 benzoquinone replicates are displayed once all analyses have been completed Press Enter to view the average of the 1 4 benzoquinone replicates 16 Press Enter and the results of the s...

Страница 98: ...ed limit response Press the appropriate key to continue 18 Once the system suitability procedure is complete remove the standard vial and reinstall the sample vessel before proceeding A printout or di...

Страница 99: ...Calibrations 3 Press Enter to display its submenu 4 Use the Up and Down Keys to specify Data History and press Enter 5 Choose the desired test category Validation System Suitability TOC Calibration o...

Страница 100: ...test data for the most recent or all up to five tests will be given The last five test results for each test category are retained in the Anatel A643a s Data History regardless of whether they passed...

Страница 101: ...tible device see Digital Outputs on page 142 The Anatel A643a alarm reporting facility also is used to report any detected Analyzer problems such as a defective UV lamp or an excessively low sample te...

Страница 102: ...Press Enter to display the Sensor Setup Menu 4 Similarly specify and select Analysis Setup 5 Specify and select More Setup 6 Specify and select Alarm Setup to display its submenu X Sensor Setup System...

Страница 103: ...ctivity Alarms on page 106 Enabling the TOC Alarm type causes the corresponding TOC Alarm Limit to be displayed 9 Use the Up and Down Keys to specify which digit is to be changed 10 Press Enter to ena...

Страница 104: ...d return to the normal display 7 2 2 Beeper Setup Note Default Enabled The Beeper Setup is a global parameter for sounding the Controller s audible alarm in the event of a TOC limit excursion by one o...

Страница 105: ...rted The associated Controller s LCD display flashes The Analyzer s Channel LED flashes red If enabled the Controller beeps an audible alarm If connected to a printer a printout is generated documenti...

Страница 106: ...and Uncompensated be selected in the Display Units Menu The actual uncompensated conductivity limits are in accordance with the specifications set forth in the method 645 Water Conductivity of the USP...

Страница 107: ...and select Alarm Setup to display its submenu Note The Cond Alarm parameter does not appear unless the display was set to both Conductv and Uncomp see Display Units on page 56 7 Use the Down Key to se...

Страница 108: ...the specified limit In that case a new alarm report is output to ensure that each limit excursion is recorded The Sensor s Digital Output 2 is asserted to allow alarm annunciation to an external devi...

Страница 109: ...its log Once displayed Codes are erased but still available on the Analyzer s internal log see Internal Log on page 114 The alarm status of the other Analyzers can be observed by pressing the Alarm K...

Страница 110: ...110 of 220 Anatel A643a Alarms Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 111: ...is RS 232C interface communicates at 1200 baud 8 data bits 1 stop bit and no parity Three or five conductor cable is adequate for most serial interfaces AWG 24 is recommended depending on the particul...

Страница 112: ...er the electronic DIP switches are preset at the factory as follows Fig 8 1 External Printer Wiring TxD3 RxD3 SG PG Isolated DATA ACQUISITION PRINTER DIAGNOSTICS BIAS Non Isolated OUTPUTS INPUTS 4 20m...

Страница 113: ...NLINE LED illuminates to indicate an On entry the OFFLINE LED correspondingly indicates an Off entry Note Be sure to enter a setting for all eight switches because this setup mode cannot be cancelled...

Страница 114: ...inst data loss by chronologically recording any events An Audit Only selection in the Log Setup Menu records power cycles alarm codes and parameter changes The default setting of Data Audit also store...

Страница 115: ...wn Keys to specify the desired Log function 6 Press Eto perform the specified function Fig 8 2 Log Setup Print Log Generates a printout of all the data currently stored in the Analyzer s memory Print...

Страница 116: ...re indicating the year which starts the from date The year must be between 1990 and 2050 inclusive The year yy is interpreted as 20XX 2005 for instance if it is less than 90 otherwise it is treated as...

Страница 117: ...ation 1 With the desired Analyzer specified in any View press the Print Key to access its menu 2 Use the Up and Down Keys to select Sensor Print and then press Enter 3 Specify Printouts and press Ente...

Страница 118: ...ts is preceded by the following Analyzer specific header data 6 Press Esc repeatedly to exit this function and return to the normal display TOC Printout TOC Calibration on page 82 TOC Validation TOC V...

Страница 119: ...Anatel A643a Printer Output 119 of 220 RPS June 2007 Edition 12 Anatel Operator Manual Fig 8 9 Setup Printout Fig 8 10 Factory Printout...

Страница 120: ...120 of 220 Printer Output Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 121: ...current output may be converted to a voltage if desired by inserting a conversion resistor into the wiring scheme Software settings determine the analog output range in addition to its corresponding...

Страница 122: ...inals 6 Replace the metal strain relief plate 7 Replace the I O Connector Block on the bottom of the Analyzer taking care not to pinch any wires and secure it in place by tightening the screws 8 Recon...

Страница 123: ...onsists of 1 Specifying the analog output range 2 Defining the associated zero scale and full scale values that establish the resolution of that signal 3 Establishing the signal that is to be output i...

Страница 124: ...lay Print Sensor Name Diagnostics Fig 9 4 Sensor Setup Menu 1 SENSOR NAME X DAC Range Ext DAC Module DAC Modes Fig 9 5 Analog Setup DAC Range Sets the Analyzer s internal and external analog output ra...

Страница 125: ...Zero Scale and Full Scale TOC values To set the Analyzer s mA Range 1 With the DAC Range Menu displayed specify DAC mA Range and press Enter to display its parameters screen 2 Use the Up and Down Keys...

Страница 126: ...h the DAC Range Menu displayed use the Up and Down Keys to specify DAC Zero Scale 2 Press Enter to display its menu selections 3 Specify TOC DAC and press Enter to display its zeroscale parameter scre...

Страница 127: ...enu 10 Select DAC Full Scale and press Enter Note The Full Scale TOC value must be greater than the Zero Scale TOC value 11 Specify TOC DAC once again and then press E to display its full scale parame...

Страница 128: ...pecify the DAC Error Output 1 With the Analyzer s Analog Setup Menu displayed use the Up and Down Keys to specify DAC Modes 2 Select DAC Err Output and press Enter to display its parameter screen 3 Us...

Страница 129: ...rnal DAC Module includes enabling the Analyzer output defining its range as well as its zeroscale and full scale values and the signal that is to be output in the event of an alarm 9 3 1 Hardware Setu...

Страница 130: ...Access 643P Analyzer s integral printer is wired to its BIAS port An external 12 VDC supply must be provided for any DAC Modules used with these instruments 6 Replace the metal strain relief plate 7...

Страница 131: ...xternal DAC output consists of 1 1 Enabling the Analyzer s DAC output 2 Specifying the analog output range 3 Defining the associated zero scale and full scale values that establish the resolution of t...

Страница 132: ...tions 6 With the Analog Setup Menu displayed specify Ext DAC Module 7 Press Enter to view its parameter screen 8 Use the Up and Down Keys to toggle the software switch to Yes to enable this analog out...

Страница 133: ...ond to the Zero Scale and Full Scale Conductivity Resistivity or Temperature values depending on the output To set the Analyzer s DAC mA Range 1 With the Analog Setup Menu displayed select DAC Range t...

Страница 134: ...Display Units setting see Display Units on page 56 To set the output range 1 With the DAC Range Menu displayed use the Up and Down Keys to specify DAC Zero Scale 2 Press Enter to display its menu sel...

Страница 135: ...lect DAC Full Scale and press Enter Note The Full Scale Cond value must be greater than the Zero Scale Cond value 7 Specify Res Cond DAC and press Enter to display its full scale parameter screen 8 Us...

Страница 136: ...scaled temperature value for output To set the temperature output range 1 With the DAC Range Menu displayed use the Up and Down Keys to specify DAC Zero Scale 2 Press Enter to display its menu select...

Страница 137: ...Zero Scale Temp value 7 Specify Temp DAC and press Enter to display its fullscale parameter screen 8 Use the Up and Down Keys to scroll the setting until the desired value is displayed 9 Press Esc tw...

Страница 138: ...138 of 220 Analog Outputs Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 139: ...ded to act as or replace a PLC Digital input and output connections are made on the instrument s I O Connector Block as follows 1 Turn the Anatel A643a Analyzer OFF and disconnect the power cord from...

Страница 140: ...mon positive terminal They are driven by a 5 to 30 VDC external power source or the Analyzer s 12 VDC 0 5 Amp Bias and designed to operate from open collector open drain or relay outputs Each input dr...

Страница 141: ...xternal Digital Control 1 With the desired Analyzer selected in any View press the Manual Key to display its submenu Fig 10 1 Typical Digital Input Wiring TxD1 RxD1 RTS1 CTS1 SG PG TxD2 RxD2 SG PG TxD...

Страница 142: ...trol 7 Press Esc repeatedly to exit this function and and return to the normal display 10 3 Digital Outputs The digital outputs also transmit specific Anatel A643a information The first digital output...

Страница 143: ...le valve as open high state or closed low state Alternatively if temperature uncompensated conductivity alarm is enabled the output is based on the USP uncompensated conductivity alarm table see Uncom...

Страница 144: ...144 of 220 Digital Inputs Outputs Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 145: ...ess internal components Bias connections are made to the instrument s I O Connector Block as follows 1 Turn the Anatel A643a Analyzer OFF and disconnect the power cord from its source 2 Remove the I O...

Страница 146: ...ause erratic behavior loss of data instrument shutdown and or component damage Fig 11 1 Bias Connections Isolated DATA ACQUISITION PRINTER DIAGNOSTICS BIAS Non Isolated OUTPUTS INPUTS 4 20mA NET NET C...

Страница 147: ...200 baud 8 data bits 1 stop bit and no parity Three or five conductor cable is adequate for most serial interfaces AWG 24 is recommended depending on the connected device Note Always disconnect the in...

Страница 148: ...crews 8 Reconnect power and turn the Analyzer ON Note The I O Connector Block must be reinstalled correctly to conform to emissions specifications Fig 12 1 Serial Wiring TxD2 RxD2 SG PG TxD3 RxD3 SG P...

Страница 149: ...pair ASCII 13 10 0D 0A Hex Both commands and replies use a free field format so the number of delimiting spaces and length of each argument or data field may vary If a command is rejected due to inval...

Страница 150: ...arameter Set Commands Command Function Section HR t t i i Sample Time hh mm ss 5 5 1 1 Cycle Time hh mm ss 5 5 1 2 Absolute TOC Alarm Limit ppb 7 2 1 Reserved always 0 Reserved always 0 Analyzer Chann...

Страница 151: ...m value 9 2 2 4 TOC Mode Paper Saver Percentage Change 1 99 5 5 2 Purge Mode Paper Saver Percentage Change 1 99 5 6 1 Purge Mode Interval Between Printouts hh mm ss 5 6 1 Zero Scale TOC Range ppb 9 2...

Страница 152: ...ingle TOC 3 Digital TOC 4 Sample Manual 5 Manual Manual 6 Clean Mode 7 Purge Mode 8 Digital Purge 9 Temperature Test 10 Self Calibrate 11 Idle Mode 12 Failure Mode The state is 1 Idle 2 Sample 3 Oxidi...

Страница 153: ...libration and validation procedures performed on the instrument Table 12 5 Data History Command Command Function Comment PC Conductivity Calibration History Up to five calibrations are displayed PT TO...

Страница 154: ...154 of 220 Serial Communications Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 155: ...CAUTION Purge all water from the Analyzer when taking the instrument out of service Residual water can freeze inside the unit expand and damage the measurement cell Such damage is timeconsuming to re...

Страница 156: ...alyzer to operate in the Self Clean Mode for 3 to 4 hours longer if contamination is significant 6 Repeat step 1 through step 3 and select Auto TOC in the Modes Menu to terminate instrument self clean...

Страница 157: ...upstream isolation valve to stop water flow to the instrument CAUTION Unplug the Analyzer s power cord and exercise extreme CAUTION as there are HIGH VOLTAGES present inside the instrument s Power Sup...

Страница 158: ...sure accurate analyses The Anatel A643a logs UV lamp usage based on its total hours of operation Anatel recommends replacement of the UV lamp every six months to ensure uninterupted operation due to l...

Страница 159: ...ergh Drive Loveland Colorado 80538 U S A Attn UV Lamp Recycling Replace the UV Lamp when any of the following conditions occur If Code 42 UV Lamp appears in the Controller display after pressing Enter...

Страница 160: ...er alarm status screen and the associated LED for the analyzer will blink Red If a printer is connected to the analyzer Code 52 UV Failing will be printed following each TOC analysis and the following...

Страница 161: ...ilter assembly from the WATER IN port 4 The UV Lamp is located at the Water I O end of the A643a TOC Analyzer While holding the Water I O Cover remove it as outlined in Preparatory Maintenance Procedu...

Страница 162: ...abs of the UV Lamp Connector stem and with your thumb braced against the enclosure pull the plugs straight out of the receptacles Note If the instrument uses the prior UV Lamp Assembly design which in...

Страница 163: ...the UV Lamp so that its arrow aligns with the center of the upper bracket screw as shown 11 Holding the UV Lamp with the arrow aligned and tighten the Phillips head screws about 1 1 2 turns to secure...

Страница 164: ...tight 15 Align the cable pins and reconnect the Sample Valve Connector Also reconnect the Ground Wire 16 Tuck the wires and tubing inside the Analyzer enclosure and replace the Water I O Cover 17 Tigh...

Страница 165: ...to access its submenu 21 Specify Sensor Setup and press Enter 22 Specify Analysis Setup and press Enter 23 Specify More Setup and press Enter 24 Specify Cell Setup and press Enter 25 Specify Lamp Ins...

Страница 166: ...enclosure one positioned at each end of the instrument 3 Remove and rinse out the two air filters Allow them to dry completely before reinstalling them in the Analyzer 4 Replace the two Analyzer cover...

Страница 167: ...ce the instrument s lithium battery 1 Remove the Analyzer s Electronics Cover as outlined in Preparatory Maintenance Procedures on page 157 2 Remove the Power Supply Assembly from the enclosure being...

Страница 168: ...tie and remove the old battery Place the new battery in its holder making sure to observe polarity 8 Secure the battery in its holder with the new cable tie that is supplied with it 9 Firmly but gent...

Страница 169: ...eplace the Electronics Cover Make sure the DC cable is not pinched between the power supply and the circuit boards 13 Restore AC power to the Sensor The Controller initially will report Code 10 and Co...

Страница 170: ...lacement Strainer Element P N FG7017301 is available from Hach Ultra CAUTION Always disconnect the instrument from its power source before attempting to access internal components To replace the 15 Mi...

Страница 171: ...and collar are not found as described in step 4 then step 4 through step 7 have already been performed at Anatel In this case the Inlet Filter appears as shown Skip to step 8 5 Slide the nut on the o...

Страница 172: ...sion nut using the 9 16 wrench 12 Restore power and sample flow to the A643a TOC Analyzer and check for leaks Tighten fittings as necessary The inline Filter is now installed The 15 micron strainer el...

Страница 173: ...per into the inlet at the bottom of the Paper Holder until the auto loader catches it and feeds about 10 cm past the serrated Paper Cutter 5 Keep pressing the PAPER FEED switch until the paper feeds s...

Страница 174: ...174 of 220 Anatel A643a Maintenance Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 175: ...ns hardware and water chemistry Hardware alarms Codes 1 99 are indicative of either an electromechanical or analytical failure of the Analyzer These alarms could result from such conditions as an exha...

Страница 176: ...sts call the Anatel Service Department 11 Check Battery The lithium battery has expired Replace the battery and recalibrate the instrument 12 See Guide Possible hardware performance issue Call the Ana...

Страница 177: ...the Anatel Service Department 31 See Guide Possible hardware performance issue Call the Anatel Service Department 32 See Guide Possible hardware performance issue Call the Anatel Service Department 33...

Страница 178: ...are performance issue Call the Anatel Service Department 46 See Guide Possible hardware performance issue Call the Anatel Service Department 47 See Guide Possible hardware performance issue Call the A...

Страница 179: ...of certain ions This condition occurs primarily in water with less than 5 megohm cm resistivity If it persists the sample water is unsuitable for Anatel A643a analysis 37 38 Temperatures outside the...

Страница 180: ...turn authorization CAUTION Drain all water from the Analyzer when taking the instrument out of service see Draining the Instrument on page 181 Residual water will freeze inside the unit expand and dam...

Страница 181: ...oute To purge the Anatel A643a of entrained water 1 Press the ON OFF button to turn the Analyzer off 2 Close the user supplied upstream isolation valve to terminate the water supply to the Analyzer 3...

Страница 182: ...s electronic analysis and communications components to assure that they are functioning properly The results of these diagnostic tests are reported on the display as well as on an automatic printout...

Страница 183: ...d on the Controller s display and a printout is generated Contact Hach Ultra if the Anatel A643a fails any of these tests 3 Press Esc twice to return to the Electronics Menu to perform another circuit...

Страница 184: ...tic selection CAUTION Make sure that the sample vessel is securely installed before initiating the Valves Pump test 3 Press Enter to select the component s state For the Valves Pump test the states of...

Страница 185: ...ons The I O Menu offers two options Good Lamp Failing Lamp Bad Lamp 1X 16 Display Lamp ON 52 UV Failing 53 UV Lamp Bad C80 controller 1 Sensor Name Output Test Passed 1 Sensor Name Output Test Failed...

Страница 186: ...contacting Anatel for assistance 4 Press Esc repeatedly in order to return to previous display screens 14 4 3 1 DAC Output Test The analog signal that the Anatel A643a sends to an optional external D...

Страница 187: ...lections are within the minimum and maximum values over the specified range 4 20 or 0 20 in 1 mA increments 3 With the appropriate mA output showing on the Controller press Enter and the TOC temperatu...

Страница 188: ...188 of 220 Troubleshooting Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 189: ...test without attaching a sample vial to purge the unit of all liquid All analyzers returned for repair or replacement must be thoroughly cleaned with all process material removed Sludge contains bact...

Страница 190: ...190 of 220 Service Procedures Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 191: ...e subject to change without notice PERFORMANCE Note Repeatability of reading on an individual instrument Sample water temperature specification stated without external heat exhanger For sample water o...

Страница 192: ...2 over Full range Uncompensated Calibration Validation TOC Up to Four Point Calibration 0 ppb C blank 250 ppb C 500 ppb C 750 ppb C all sucrose One to Three Point Validation 250 ppb C 500 ppb C 750 pp...

Страница 193: ...mum Relative Humidity 100 RH non condensing Maximum Altitude 4 000 m 13 125 ft Size including sample vessel assembly 193 mm H x 489 mm W x 119 mm D 7 6 H x 19 25 W x 4 7 D Weight 6 58 kg 14 5 lb Analy...

Страница 194: ...d 12 VDC output 1 2 Amp max Digital I O Two opto isolated inputs Two opto isolated outputs Serial Interfaces RS485 opto isolated Network RS232 Data Acquisition RS232 Printer RS232 Diagnostics Fig B 2...

Страница 195: ...Power Consumption 2 Amps max 120 VAC 1 Amp max 230 VAC Fuse 3 Amp 250 VAC Fast Blow Power Cord 100 to 120 VAC Main 208 to 230 VAC Main Rating 125 VAC 10 Amp Foil Shield 100 Braid Shield 85 Connectors...

Страница 196: ...C to 40 C 32 F to 104 F Maximum Relative Humidity 90 RH Maximum Altitude 4 000 m 13 125 ft Power 9 VDC Power Pack 120 VAC 10 60 Hz standard 230 VAC 10 50 Hz optional Power Consumption 7 6 W max Case A...

Страница 197: ...ad battery is not field replaceable contact Anatel for replacement The battery can be recharged however by turning the printer OFF and the A 643a P ON for eight hours Fig B 4 Thermal Printer Print Met...

Страница 198: ...ion 12 Operator Manual Anatel To order these materials contact a local Hach Ultra representative or contact the factory at 800 866 7889 or 1 541 472 6500 Dimensions 160 mm W x 170 mm L x 66 5 mm D 6 3...

Страница 199: ...ition 12 Anatel Operator Manual Appendix C Certifications C 1 Overview This section contains the Declaration of Conformity certificate For more information contact a local Hach Ultra representative or...

Страница 200: ...ettive Las normas siguientes han sido utilizadas para verificar que el producto cumpla con las directivas Emissions EN 61000 3 2 00 Harmonic Current Emissions Limits EN 61000 3 3 95 Voltage Fluctuatio...

Страница 201: ...Anatel A643a Anatel A643a Menu Flowcharts 201 of 220 RPS June 2007 Edition 12 Anatel Operator Manual Appendix D Anatel A643a Menu Flowcharts...

Страница 202: ...202 of 220 Anatel A643a Menu Flowcharts Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 203: ...Anatel A643a Anatel A643a Menu Flowcharts 203 of 220 RPS June 2007 Edition 12 Anatel Operator Manual...

Страница 204: ...204 of 220 Anatel A643a Menu Flowcharts Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 205: ...accordance with all applicable local regulations The attached Material Safety Data Sheets MSDS are furnished to provide users with the chemical properties and precautionary procedures for the reagent...

Страница 206: ...206 of 220 Material Data Safety Sheets Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 207: ...Anatel A643a Material Data Safety Sheets 207 of 220 RPS June 2007 Edition 12 Anatel Operator Manual...

Страница 208: ...208 of 220 Material Data Safety Sheets Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 209: ...Anatel A643a Material Data Safety Sheets 209 of 220 RPS June 2007 Edition 12 Anatel Operator Manual...

Страница 210: ...210 of 220 Material Data Safety Sheets Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 211: ...hey almost always include hydrogen Oxidation The loss of electrons by a chemical species typically with oxygen Organic carbon for example oxidizes to carbon dioxide and water Parts per billion ppb A t...

Страница 212: ...212 of 220 Glossary Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel...

Страница 213: ...14 Controller Edit Mode 25 Fig 2 15 Change Character 26 Fig 2 16 Sensor Name Change 26 Fig 2 17 Controller Mounting Dimensions 27 Fig 2 18 Anatel A643a S Mounting Template 28 Fig 2 19 Anatel A643a P...

Страница 214: ...g Operator Password Screen 56 Fig 5 9 Display Units Menu 56 Fig 5 10 Display Units Menu 57 Fig 5 11 Display Units Screen 57 Fig 5 12 Uncompensated Conductivity Display 58 Fig 5 13 Purge Printout 59 Fi...

Страница 215: ...on Standard Criteria 83 Fig 6 3 Calibration Purge Mode 84 Fig 6 4 Calibration Mode 84 Fig 6 5 Remove Instrument Vessel 85 Fig 6 6 Calibration Data 85 Fig 6 7 TOC Calibration Results 86 Fig 6 8 Sample...

Страница 216: ...p Menu 104 Fig 7 12 C80 Alarm Beeper Screen 105 Fig 7 13 Reported Sensor Alarm 105 Table 7 1 Temperature based Conductivity Limits 106 Fig 7 14 Alarm Setup 107 Fig 7 15 Alarm Setup Menu 107 Fig 7 16 U...

Страница 217: ...o Scale Uncompensated Conductivity Display 135 Fig 9 28 Zero Scale TOC Data 135 Fig 9 29 Full Scale Uncompensated Conductivity Display 135 Fig 9 30 Full Scale TOC Data 136 Fig 9 31 DAC Zero Scale Menu...

Страница 218: ...A643a Air Filters 166 Fig 13 16 26 Pin Connectors 167 Fig 13 17 Lithium Battery 167 Fig 13 18 Replace Battery 168 Fig 13 19 Pin 1 169 Fig 13 20 Inline Filter Assembly 171 Fig 13 21 Collar Position 171...

Страница 219: ...Anatel A643a User Notes 219 of 220 RPS June 2007 Edition 12 Anatel Operator Manual User Notes...

Страница 220: ...220 of 220 User Notes Anatel A643a RPS June 2007 Edition 12 Operator Manual Anatel end of the book...

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