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Agilent Technologies 3200D, Руководство по эксплуатации

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86

3200D 

溶解氧测定仪用户手册

2

 
 

为了方便用户随时查看各个模块里面其它的参数值，仪器设置了一
个特别的查看功能。在测量状态下，按

“

模式

”

键，仪器即突出显

示测量窗口，如

图 

5

，重复按

“4/

”

或

“6/

”

键，可以查看其他测 

量参数，比如，当前测量参数为溶解氧参数，则重复按

“4/

”

或

“6/

”

键时，仪器会在溶解氧、饱和度、电极电流之间来回切换。

查看结束，如果用户在几秒钟里面没有继续按键，仪器会自动退出
查看状态。

连续测量模式 

这是最常使用的一种测量模式，开始测量后，仪

器始终连续测量、计算和显示测量结果，用户在测量期间可以查阅
测量参数、标定电极、贮存或打印测量结果等等，测量结束，用户
按

“

取消

”

键并

“

确认

”

后退出测量模式。

定时测量模式

 

定时测量模式是为了方便用户检测需要而设置

的，比如需要连续

30

分钟检测溶解氧浓度值，则用户可以选择这

种定时测量模式，开始测量后，仪器会自动测量、计算和显示测量
结果，到用户设定的时间间隔时，仪器自动贮存测量数据

(

如果

USB

接口连接有

PC

，仪器会自动打印出测量数据

)

，然后开始下

一次的测量。按

“

取消

”

键并

“

确认

”

后可以退出定时测量模式。

如果用户选择定时测量模式，需要再设置定时间隔，时间间隔

1~99

分钟，默认间隔为

10

分钟。

平衡测量模式 

用户首先应该设置好平衡条件 （详见

“

设置平衡

条件

”

），开始测量后，仪器自动测量、计算并显示测量结果，一

旦测量符合设定好的平衡条件，本次测量即结束。

在测量过程中，用户可以查阅测量参数、标定电极等。测量结束
后，用户可以贮存、打印测量结果；按

“

取消

”

键退出测量状态，

或者选择按

“

测量

”

键开始下一次测量。

图

5

Содержание 3200D

Страница 1: ...Agilent Technologies Agilent 3200D Dissolved Oxygen Meter Operating Guide...

Страница 2: ...d warranties of merchantability and fitness for a par ticular purpose Agilent shall not be liable for errors or for incidental or consequential damages in connec tion with the furnishing use or per fo...

Страница 3: ...adaptor 12 Installing the optional ground line 13 Installing Optional Software 14 2 Operation 15 Introduction 16 Where to find information 16 Term definitions 16 Proper use 17 Features 18 Specificati...

Страница 4: ...asure temperature 42 To view other parameters while measuring 42 Managing Data 44 To save data 44 To delete data 44 To output data 44 To view data 45 Turn off the 3200D Dissolved Oxygen Meter 50 Softw...

Страница 5: ...perating Guide 5 Check other possible causes 57 Meter Self Diagnostics and Messages 58 Severe errors 58 Error warning 59 Maintenance 61 Probe maintenance 61 Short term storage 61 Long term storage 61...

Страница 6: ...6 3200D Dissolved Oxygen Meter Operating Guide Contents...

Страница 7: ...ter Operating Guide 1 Installation Tools and Components for Installation 8 Installing the 3200D Dissolved Oxygen Meter 9 Installing Optional Software 14 The tools and accessories necessary for install...

Страница 8: ...Installation Tools and Components for Installation Agilent provides the tools needed for installation The following accessories are included in the shipping case Multifunction electrode holder G4389A...

Страница 9: ...s Installing the electrode holder 1 Place the electrode holder near the meter and move the arm into position Use the thumbscrews shown in Figure 1 to secure the arm in place 2 Clip the DO dissolved ox...

Страница 10: ...10 3200D Dissolved Oxygen Meter Operating Guide 1 Installation 3 Route the probe cable as shown Figure 2 Figure 2 Installed meter and probes Probes Meter Probe socket...

Страница 11: ...4 Locate the DO Temp probe socket on the back of the meter Plug the DO probe connector 5190 3997 into the DO Temp socket on the rear of the meter See Figure 3 Figure 3 The back view of the 3200D Disso...

Страница 12: ...back panel of the meter Insert the probe connector into the socket 2 Feed the probe cable through the hole of the multifunction electrode holder Installing the power adaptor The universal power adapt...

Страница 13: ...the power adapter to the power input on the meter A click will be heard when the plug is properly engaged Installing the optional ground line The meter ships with an optional ground line During use i...

Страница 14: ...nect the computer to the meter with a USB cable See the G4390A software documentation for more information If not using the G4390A software Agilent provides downloadable data printing software on the...

Страница 15: ...ent Control 23 Turn on the Meter 25 Setup 26 Prepare the DO Probe 37 Calibrate the DO Probe 39 Perform a Measurement 41 Managing Data 44 Turn off the 3200D Dissolved Oxygen Meter 50 Software Operation...

Страница 16: ...izable services as well as information related directly to your Agilent products and orders Log onto the portal at http www agilent com chem Term definitions Dissolved oxygen concentration The extent...

Страница 17: ...ot soak the DO probe in sodium sulfite solution If a probe is out of use for more than 6 hours rinse and store it in a protective container CAUTION Do not expose to corrosive gas Keep the sockets on t...

Страница 18: ...Zero Point and Full Scale A clear dot matrix LCD display Supports GLP standards Requires an operator number Records views and prints calibration data Stores 200 sets of measuring data Can view print a...

Страница 19: ...acy of electric unit DO concentration 0 10 mg L DO saturation 2 0 Temperature 0 1 C Normal working conditions Environmental temperature 0 40 C Relative humidity 85 Power supply Power adaptor 5185 8389...

Страница 20: ...a meter and a probe system The probe system is held in place by the electrode holder See Figure 6 Figure 7 and Figure 8 Figure 6 The meter electrode holder and probe Figure 7 The front view of the 32...

Страница 21: ...1 The Display The display shows the working condition and current setting of the 3200D Dissolved Oxygen Meter Figure 8 The back view of the Agilent 3200D Dissolved Oxygen Meter Figure 9 The initial st...

Страница 22: ...erating keys The keys are shown in Figure 10 and described in Table 1 on page 23 Most keys have two values a numeric entry and a function Which one applies depends on the display if it is waiting for...

Страница 23: ...election cursor upward when selecting Type the number 3 Store measurement data Type the number 4 Move the selection cursor left when selecting Type the number 5 Opens the Setup menu from the initial s...

Страница 24: ...Operating Guide 2 Operation Type the number 0 Begin measurement Type a decimal point Calibrate the DO probe Type a negative number Delete the data being viewed Meter power switch Table 1 Keypad functi...

Страница 25: ...on the display shows the Agilent name the meter model and other information 2 After the system self check the meter goes to the initial state shown in Figure 11 The left of the screen shows the curren...

Страница 26: ...reen appears See Figure 12 Measuring Mode Sets up current measuring mode Continuous Mode Timed Reading Mode Auto Lock Reading Mode and measuring parameter Set Condition Use this mode to set condition...

Страница 27: ...ys to highlight the desired parameter and press Setup to select it A check appears next to the selected parameter During measurement you can still view save and print the other parameter See To view o...

Страница 28: ...save or print results at any time during measurement To end a measurement run press Cancel followed by Enter Timed Reading The meter will automatically save measurement data periodically while measur...

Страница 29: ...ge 30 When the measurement begins the meter automatically measures calculates and displays the results Once the measurements meet the preset Auto Lock condition the measurement finishes and the screen...

Страница 30: ...screen locks displaying the final reading To set the conditions 1 From the initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow keys to navigate to S...

Страница 31: ...initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow keys to navigate to System Setup 3 Press Enter to select System Setup or press Cancel to exit T...

Страница 32: ...een 7 Once all of the system settings are made press Enter to save the new setup exit and return to the initial state Press Cancel to exit without saving changes Descriptions of the System Setup setti...

Страница 33: ...If Auto Delete is not enabled the meter does not save new data when its memory is full For example the meter permits up to 200 sets of data When you want to store the 201st set of data if Auto Delete...

Страница 34: ...screen appears on the display Use the arrow keys to choose either Chinese or English and press Enter To set the air pressure barometric pressure You do not usually need to set barometric pressure The...

Страница 35: ...er can power off automatically after a set time period To set the Auto Power Off time 1 From the initial state press Setup The setup screen appears See Figure 12 on page 26 2 Use the directional arrow...

Страница 36: ...e display Press Enter to restore parameters to their original settings Table 2 Default values for meter parameters Parameter Default value DO calibration data Zero Oxygen 0 nA Full Scale 1000 nA Calib...

Страница 37: ...atinum tip 7 Polarize the DO probe before use Connect the DO probe with a powered on 3200D DO meter Polarization takes 60 minutes The DO probe is always being polarized when connected with the meter s...

Страница 38: ...ng upon application conditions Refill the DO filling solution every 2 weeks to 2 months CAUTION There should not be any damage to the membrane Avoid touching the membrane to any solid or hard material...

Страница 39: ...lution or as described in the instruction manual for the DO probe 2 From the initial state or while measuring press Calibrate 3 Select Calib Zero Press Enter to select Zero Point Calibration as shown...

Страница 40: ...From the initial state or while measuring press Calibrate 6 Select Full Scale Press Enter to open Full Scale Calibration as shown in Figure 22 During calibration press Setup to set calibration paramet...

Страница 41: ...e Measuring Mode on page 26 4 Put the probe in the sample solution and press Measure to start taking a measurement according to the selected mode See Figure 23 The upper area of the screen shows the c...

Страница 42: ...according to the selected mode 5 After a measurement press Save to save data Press Output to print data Press Cancel to end measurement To measure temperature In any measuring state the meter directly...

Страница 43: ...Oxygen Meter Operating Guide 43 2 Press 4 or 6 to switch the view to the other parameter 3 If you do not press a key for a few seconds the meter will automatically exit from viewing mode and return to...

Страница 44: ...me stable In timed reading mode you can still save data manually but the meter automatically saves measuring data at a fixed periodic time interval See Measuring Mode on page 26 To delete data You can...

Страница 45: ...d data meets GLP standards The meter can store 200 sets of measurement data 1 In the initial state press View 2 Navigate to the type of data to view and press Enter See Figure 25 To View DO Data The m...

Страница 46: ...lay format depends on the viewing mode 2 The data displayed include save time and operator no Press the arrow keys to scroll through the saved data 3 Press Delete to delete data 4 To output stored dat...

Страница 47: ...10 06 20 OPERATOR NO 000 STORED NUM 002 NO 001 OPERATOR NO 000 STORED TIME 10 43 00 2010 06 20 PRESSURE 101 3kPa SALINITY 0 0g L ZERO 0nA FULL 1000nA CURRENT 0nA DO 0 00mg L SATURATION 0 0 TEMP 25 0c...

Страница 48: ...ss Enter The display is shown in Figure 28 The upper area displays last calibration data The bottom area displays current calibrated parameters 2 To print current data connect the meter with the PC Pr...

Страница 49: ...e 49 Figure 29 Output format MODEL 3200D DISSOLVED OXYGEN METER SOFTWARE VER 1 00 PRINT TIME 09 14 03 2010 06 20 OPERATOR NO 000 DO CALIB DATA CALIB TIME 08 12 00 2008 01 09 OPERATOR NO 000 PRESSURE 1...

Страница 50: ...line and salt solution The input terminal of the meter connector of the DO ATC probe must be kept clean and dry If the DO probe is used in a strongly humid place wipe the DO probe plug with clean gauz...

Страница 51: ...the software will recognize the meter model and type The software provides the functions corresponding to the meter type Refer to the software documentation for details To use the Data Printing softw...

Страница 52: ...52 3200D Dissolved Oxygen Meter Operating Guide 2 Operation...

Страница 53: ...Maintenance Troubleshooting the 3200D Dissolved Oxygen Meter 54 General Troubleshooting Procedure 56 Meter Self Diagnostics and Messages 58 Maintenance 61 Consumables and Ordering Information 62 This...

Страница 54: ...meet with the requirements 3 The power adaptor is damaged 4 The power socket has poor contact 5 The LCD is damaged After start up for a few minutes the user can hear a buzzing sound after pressing On...

Страница 55: ...king strong electromagnetic field an so forth 1 Replace the probe 2 Remove the electrical signal interference source Lift or move the beaker away from the source of interference Shield the meter and b...

Страница 56: ...ions For best results follow the troubleshooting order shown below Check the current response 1 Connect the meter to the ATC temperature diagnostic tool 5185 8390 shipped with the meter 2 Turn on the...

Страница 57: ...meter displays a temperature reading significantly different from 50 C there is a problem with the meter Contact Agilent service Check other possible causes If the meter is functioning properly that i...

Страница 58: ...er unable to finish necessary tasks In this case replacement or maintenance of the meter is required Minor errors which are prompts or warnings are caused by various reasons and can be corrected in se...

Страница 59: ...Error warning NOTE This table describes all error messages which may occur in use These error messages have different definition for different meters Table 4 Error warning codes Code Description Solu...

Страница 60: ...buffers 28 Temperature of pH buffer is out of range Cool or heat buffer 29 Calibrate the same buffer repeatedly Replace the buffer Due to incorrect operation 30 Number of pH buffers exceeds maximum R...

Страница 61: ...parts of the stem with distilled or deionized water and dry with a soft tissue Short term storage Between tests immerse the measuring tip in distilled water or calibration solution while the probe is...

Страница 62: ...n with stable and precise speed with a large adjustable range G4389A 3200EA Electrode Holder It is used to support several electrodes 5185 8389 AC Adaptor 100 240VAC 1A 50 60Hz G4388 27000 Stirring Ba...

Страница 63: ...Agilent Technologies Agilent 3200D...

Страница 64: ...3200D Agilent Technologies Inc 2012 Agilent Technologies Inc 5973 1779 2012 3 412 800 820 3278 Agilent Agilent Agilent...

Страница 65: ...3200D 65 3200D 67 68 3200D 69 69 70 71 71 72 73 3200D 75 76 76 Agilent 76 76 3200D 77 3200D 78 79 81 81 81 83 83 83 91 95 3200D 99 100...

Страница 66: ...66 3200D 101 101 101 101 101 3200D 103 104 105 105 105 105 106 106 107 109 110 111 111 111 3200D 113...

Страница 67: ...67 Agilent Technologies Agilent 3200D 1 3200D 68 3200D 69 72 73...

Страница 68: ...68 3200D 1 Agilent G4389A D6111 DO Probe 5190 3997 5185 8389...

Страница 69: ...1 3200D 69 3200D 3200D 1 2 3 4 5 6 7 8...

Страница 70: ...70 3200D 1 5190 3997...

Страница 71: ...1 3200D 71 100 240 VAC 1 A 50 60 Hz DC501...

Страница 72: ...72 3200D 1 G4390A USB...

Страница 73: ...1 3200D 73 3200D...

Страница 74: ...74 3200D 1...

Страница 75: ...75 Agilent Technologies Agilent 3200D 2 3200D 76 83 101 3200D...

Страница 76: ...76 3200D 2 Agilent 3200D 3200D 60 Agilent Agilent Web Agilent http www agilent com chem DO kPa g L...

Страница 77: ...2 3200D 77 5 3200D 3200D GLP GLP 200 USB PC PC bug...

Страница 78: ...78 3200D 2 3200D 3200D 0 00 45 00 mg L 0 0 300 0 5 0 110 0 C 0 01 mg L 0 1 0 1 C 0 10 mg L 2 0 0 1 C 0 40 C 85 5185 8389 100 240 VAC 1 A 9 VDC 1 A mm 190 190 105 kg 1 kg...

Страница 79: ...2 3200D 79 3 3200D 3200D...

Страница 80: ...80 3200D 2 3200D 1 2 3200D 1 2 3 USB 4...

Страница 81: ...2 3200D 81 3200D On Off 3200D 15 1 2 3 4 5 6 7 8 9 0 1 1 2 4 8 6 2 4 8 6 3 3 5 5 7 7...

Страница 82: ...82 3200D 2 9 9 0 0...

Страница 83: ...2 3200D 83 3200D 3200D 3200D 3200D 3200D 3200D 3200D On Off...

Страница 84: ...84 3200D 2 1 2 GLP 1 2...

Страница 85: ...2 3200D 85 3 4 3 4...

Страница 86: ...86 3200D 2 5 4 6 4 6 30 USB PC 1 99 10 5...

Страница 87: ...2 3200D 87 6 1 0 1 0 s 1 200 GLP 7 h 6...

Страница 88: ...88 3200D 2 000 200 7 200 201 201...

Страница 89: ...2 3200D 89 8 9 101 3kPa 8 9...

Страница 90: ...90 3200D 2 10 0 0g L 10 480min 0 nA 1000 nA 25 0 C 101 3 kPa 0 0 g L 10 min 000 1 0 10...

Страница 91: ...2 3200D 91 5 s 0 1 2 3 5190 0547 4 5 60 1 1 25 20 80 cm 2 2...

Страница 92: ...92 3200D 2 11 5 12 11 12...

Страница 93: ...2 3200D 93 13 14 13...

Страница 94: ...94 3200D 2 14...

Страница 95: ...2 3200D 95 200 200 USB PC PC...

Страница 96: ...96 3200D 2 3200D 15 GLP 200 16 10 USB PC MODEL 3200D DISSOLVED OXYGEN DETERMINATOR VER 1 00 PRINT TIME 09 03 28 15...

Страница 97: ...00 STORED NUM 003 NO 001 OPERATOR NO 000 STORED TIME 10 43 00 2010 06 20 PRESSURE 101 3kPa SALINITY 0 0g L ZERO OXYGEN 0nA FULL OXYGEN 1000nA CURRENT 0nA DO 0 00mg L SATURATION 0 0 TEMP 25 0c NO 002 O...

Страница 98: ...98 3200D 2 17 USB PC MODEL 3200D DISSOLVED OXYGEN DETERMINATOR VER 1 00 PRINT TIME 16 17...

Страница 99: ...00D 99 09 14 03 2010 06 20 OPERATOR NO 000 DO CALIB DATA CALIB TIME 08 12 00 2008 01 09 OPERATOR NO 000 PRESSURE 101 3kPa SALINITY 0 0g L ZERO OXYGEN 0nA FULL OXYGEN 1000nA TEMP 25 0c 3200D On Off 1 2...

Страница 100: ...100 3200D 2 5 6 7 60...

Страница 101: ...2 3200D 101 3200D 3200D G4390A PC DVD 1 On Off 2 USB PC 3 PC 1 On Off 2 PC 3 PC...

Страница 102: ...102 3200D 2...

Страница 103: ...103 Agilent Technologies Agilent 3200D 3 3200D 104 105 106...

Страница 104: ...104 3200D 3 1 1 2 3 4 5 1 2 3 4 5 2 1 2 1 2 3 1 2 1 2 4 1 2 1 2...

Страница 105: ...3 3200D 105 ATC 5185 8390 680 720nA 0 5nA 300 1000nA ATC 5185 8390 49 0 51 0...

Страница 106: ...106 3200D 3 18...

Страница 107: ...3 3200D 107 19...

Страница 108: ...01 3 02 4 03 5 6 7 20 1999 9 1999 9 mV 8 21 pH pX 3 000 21 000 pH 9 22 0 2000 mS cm 10 23 0 100 Mohm cm 11 24 6 0 120 0 C 12 25 0 4000 nA 13 26 pH 80 120 14 27 pH 15 28 pH 16 29 17 30 pH 5 18 31 pH 1...

Страница 109: ...109 Agilent Technologies Agilent 3200D 4 110 111...

Страница 110: ...110 3200D 4 1 2 3 4 5 6 60 1 1 25...

Страница 111: ...4 3200D 111...

Страница 112: ...112 3200D 4...

Страница 113: ...113 Agilent Technologies Agilent 3200D 5 3200D 3200D...

Страница 114: ...3200D 5 Agilent http www agilent com chem G4388A 3200SA G4389A 3200EA G4390A 5185 8389 100 240 VAC 1 A 50 60 Hz G4388 27000 5190 3997 D6111 3 0 20 mg L 0 45 C 5185 8390 ATC 5190 0547 3 30 mL 5190 054...

Страница 115: ......

Страница 116: ...Agilent Technologies Inc 2012 Printed in China 03 12 First edition March 2012 5973 1780 5973 1779 www agilent com Agilent Technologies...

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