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Spectris 04416001A Operator'S Manual Download Page 76

 

SERVO

PRO NANOCHROME Gas Analyser 

 

 

 

 

75 

04416001A / Revision 7  

  

 

3) Flow 
 

 

 

 

Figure 34 : Advanced configuration-Flow menu 

 

The 

Flow

 menu associates a flow with a regulator on an I/O Board and a plasma detector 

(see Figure 34).  

The menu shows the name given to each flow and its location on the appropriate I/O Board, 

and for a carrier regulator, its association with a plasma detector (used to generate alarms 

and errors). For sample regulators there is no association with a plasma detector.  

 

 

DO  NOT  CHANGE  THESE  SETTINGS:  they  are  factory 
configured. 

 
 

Summary of Contents for 04416001A

Page 1: ...Part Number 04416001A Revision 7 Language UK English SERVOPRO NanoChrome OPERATOR MANUAL...

Page 2: ...SERVOPRO NANOCHROME Gas Analyser 1 04416001A Revision 7...

Page 3: ...4 1 5 2 Auxiliary Oven Rear Connections 14 1 6 Standalone PC Rear Connections 15 2 SOFTWARE LICENSE 17 2 1 MICROSOFT SOFTWARE LICENSE TERM 17 3 SPECIFICATIONS 28 3 1 General 29 3 2 Gas 30 3 3 Oven 31...

Page 4: ...9 4 6 9 Export the Analyser Configuration 80 4 7 Analyser Calibration 81 4 7 1 Noise Threshold THRSH Calibration 81 4 7 2 Span Calibration 82 4 8 Calibration of the 4 20mA outputs 86 4 9 Remote 87 4 9...

Page 5: ...TART UP AND SHUTDOWN PROCEDURE 110 7 1 Equipment Tools 110 7 2 Installation requirements 110 7 3 Start up procedure 110 7 4 Shut down procedure 112 8 ROUTINE MAINTENANCE 113 9 STORAGE AND DISPOSAL 114...

Page 6: ...anual checks 48 Table 17 Diagnostic Analyse Chromatogram menu 51 Table 18 Trending menu summary of functions 54 Table 19 Oven set point 59 Table 20 Peak Configuration Columns 65 Table 21 Peak Data 65...

Page 7: ...Diagnostic menu 55 Figure 20 Configuration System menu 57 Figure 21 Configuration PID menu 61 Figure 22 Configuration Flow menu 62 Figure 23 Configuration Cycle menu 63 Figure 24 Cycle Peak Configurat...

Page 8: ...assis electrical connections 96 Figure 48 Master with 2 Secondary Chassis electrical connections 97 Figure 49 Stand alone PC with secondary electrical connections 98 Figure 50 Stand alone PC with two...

Page 9: ...SERVOPRO NanoChrome Important safety information is highlighted in this manual as WARNINGs and CAUTIONs which are used as follows WARNING Warnings highlight specific hazards which if not taken into a...

Page 10: ...rameters are controlled by the SERVOPRO NanoChrome analytical software package Each impurity peak is reported on screen with its process value The software offers advanced diagnostic tools and trendin...

Page 11: ...ectron or ion collision that is the kinetic energy of electrons or ions accelerated in an electric field in which the atoms or molecules of a gas are subjected to which cause the emission of light The...

Page 12: ...the I O board 1 3 6 I O board The I O board holds all the I O functions of the instrument shown in the table below Table 1 I O board All digital inputs and outputs analogue inputs and outputs are tran...

Page 13: ...cket 6 Gas trap outlet 7 Ethernet port 8 USB port 9 Analogue 4 20 mA outputs 10 Digital outputs 11 Digital input 12 Earth terminals for cable screens 13 Carrier gas inlet to detector 1 14 Carrier gas...

Page 14: ...e gas inlet 1 process 9 Sample gas inlet 2 span Note the RS 232 port is replaced with a RS 485 port on Secondary Chassis 1 on an analyser with multiple secondary chassis WARNING Any Connections on the...

Page 15: ...ed to the specific channel making the N2 determination and removes the small volume of interfering background gas which has co eluted with the N2 prior to the passing to the detector 1 5 2 Auxiliary O...

Page 16: ...ed with the standalone PC USB Ethernet must be fitted with ferrite beads W rth 74271131 or 74271221 depending on cable size which should be clamped around 2 turns of cable CAUTION To comply with the r...

Page 17: ...onal protective equipment WARNING Improper installation operation or service of this analyser may cause damage to the analyser and void the manufacturer s warranty WARNING All connections must be prop...

Page 18: ...n during activation and during your use of the software as per the privacy statement described in Section 3 If you do not accept and comply with these terms you may not use the software or its feature...

Page 19: ...use by one person at a time so long as you comply with all the terms of this agreement Updating or upgrading from non genuine software with software from Microsoft or authorized sources does not make...

Page 20: ...may only use such hardware or software if you have a license for each instance of the software you are using iii Device connections You may allow up to 20 other devices to access the software install...

Page 21: ...system Desktop functions as used in this agreement means a consumer or business task or process performed by a computer or computing device This includes word processing spreadsheets database schedul...

Page 22: ...software is counterfeit improperly licensed or includes unauthorized changes If activation fails the software will attempt to repair itself by replacing any tampered Microsoft software with genuine Mi...

Page 23: ...service representatives can t resolve it send a Notice of Dispute by U S Mail to the manufacturer or installer ATTN LEGAL DEPARTMENT If your dispute is with Microsoft mail it to Microsoft Corporation...

Page 24: ...00 USD The AAA rules will govern payment of filing fees and the AAA s and arbitrator s fees and expenses iii Disputes involving any amount If you start an arbitration we won t seek our AAA or arbitrat...

Page 25: ...ller This warranty is given in addition to other rights and remedies you may have under law including your rights and remedies in accordance with the statutory guarantees under the Australian Consumer...

Page 26: ...AVC and MPEG 4 visual standards and VC 1 video standards The software may include H 264 MPEG 4 AVC and or VC 1 decoding technology MPEG LA L L C requires thisnotice THIS PRODUCT IS LICENSED UNDER THE...

Page 27: ...ices including any linked terms You understand that by using the software and services you ratify this agreement and the linked terms There are also informational links in this agreement The links con...

Page 28: ...S AND DIRECT CONSEQUENTIAL SPECIAL INDIRECT OR INCIDENTAL DAMAGES UNDER ANY PART OF THIS AGREEMENT OR UNDER ANY THEORY THIS LIMITATION APPLIES TO I ANYTHING RELATED TO THIS AGREEMENT THE SOFTWARE INCL...

Page 29: ...be bonded to the case of the Master Secondary unit using braid less than 20 cm long WAR CAUTION To comply with the applicable requirements of EU EMC Directive The case of the Stand alone PC shall be...

Page 30: ...ents Voltage Frequency Power maximum Master chassis Secondary chassis Auxiliary oven Stand alone PC 100 to 120 Vac or 220 to 240 Vac1 2 50 to 60 Hz 400 VA 400 VA 100 VA 60 VA Fuse rating type Master S...

Page 31: ...argon with 1 ppb total impurity application dependent 553 7 kPa 80 1 psig 587 7 kPa 85 1 psig 90 cc min to 810 cc min3 Sample gas Type Pressure range Flow Hydrogen Oxygen Nitrogen Argon Helium 207 0 k...

Page 32: ...emperature range 5 C to 40 C Operating ambient humidity range 0 to 95 RH non condensing Maximum Operating altitude 2000 m max Ingress protection IP20 Table 5 Environmental limits 3 5 Digital Relay Out...

Page 33: ...ge 4 to 20 mA Less than 4 mA Over than 20 mA 24 mA maximum Cable requirements Type Size Multi strand twisted pair with overall screen 0 2 3 3 mm2 24 12 AWG Maximum length 30 m Table 7 4 20 mA outputs...

Page 34: ...ion of screening or similar protection Table 9 Ethernet cable 3 9 RS 232 Port Type Male 9 way D connector Cable requirements NULL modem Shielded cable Maximum length 10 m Table 10 RS 232 port 3 10RS 4...

Page 35: ...3 12Mains input cables Master Secondary Stand alone PC Type IEC 60320 1 C13 Cable requirements Screened Specified for 10 A 250 Vac Fit with a main plug that meets the requirement of the country where...

Page 36: ...ngth Figure 5 Edit Box control When an Edit Box control is available to accept an input a cursor appears To operate an Edit Box control from the keyboard Press LEFT or RIGHT to move the cursor Press H...

Page 37: ...r up one position Press DOWN to move the slider down one position Press HOME to move the slider to the top of the slide Press END to move the slider to the bottom of the slide To operate using the mou...

Page 38: ...eft clicking with the mouse to highlight the cell then enter the new value 4 1 6 Combo control The Combo Box control is used to choose a value between sets of predetermined values Figure 10 Combo Box...

Page 39: ...it checked enabled or unchecked disabled To operate using the mouse left click in the check box to make it checked enabled or unchecked disabled 4 1 8 Tab control The Tab control is used to switch bet...

Page 40: ...3 1 Real Time Chromatogram Menu The REAL TIME CHROMATOGRAM menu can initiate a cycle and visualise the resulting real time chromatogram The chromatogram presents all the peak data that can be configur...

Page 41: ...s detected and used for integration is presented in yellow below the raw signal coming from the detectors During the cycle the progress bar rises with time The bar starts at the left and ends at the r...

Page 42: ...ess the Historic Alarm menu This button will turn red when an alarm occurs turn yellow when the menu is opened and alarms are still active and turn green if the problem is resolved The Historic Alarm...

Page 43: ...ll saved data will be over written with the new data The oldest data will be over written first Note that a tick mark little vertical line is displayed on the real time chromatogram at every starting...

Page 44: ...t point greater than 10 cc min Low carrier flow When the carrier flow falls below 5 cc min for the plasma detector for 30 seconds a Plasma X on I O Board X shut down alarm will be initiated to protect...

Page 45: ...data with an electronic board inside the analyser 2 Peak value alarms Peak value alarms do not impact the system status alarm dry contact output Alarm 1 peak When the concentration of impurity is grea...

Page 46: ...s are reached Some system functions such as a real time chromatogram are disabled when alarms are active Rectify the problems before proceeding with your analysis When the problem is resolved the same...

Page 47: ...is divided in hardware component groups Acquisition boards read signals coming from detectors applying polarisation IO boards viewing oven temperatures changing plasma power Pressure regulators viewin...

Page 48: ...e of 4 levels Offset Displays the voltage applied at the input of the acquisition board to provide an offset to the signal Scale Factor Displays scale factor in use x1 x2 x5 or x10 applied to the gain...

Page 49: ...6Table 16 Table 16 Diagnostic menu lists parameters that can be manually changed to help diagnose a problem Parameter Meaning Active Detector Selects the detector seen by the system Only detectors for...

Page 50: ...he right starting and ending times for the peaks When the menu is first opened the software requests the name of a file that has been previously saved This can be a real time chromatogram or a trendin...

Page 51: ...ursor the data changes 1 Set times as start end F4 Use the Set times as start end F4 button to directly modify the peak data The times specified in the edit control for each position will be automatic...

Page 52: ...size Delete F7 Removes a trending from the memory Load F6 Opens and displays a trending file saved in memory Set times as start end F4 Changes the starting and the ending of the peak you select with t...

Page 53: ...n generator power and frequency These values must then be entered in the peak data table Before starting a trending ensure all parameters set in the CONFIGURATION SYSTEM menu such as sample flow carri...

Page 54: ...hat valve see Figure 18 If the box in the Follow column is unchecked the valve can be manually turned on and off using the combo box located in the State column The valve table showing the timings for...

Page 55: ...u valve state Push Button Hot key Functions Start Stop F2 Start and Stop a trending Generator Power F3 Set the generator power for the detector Re Zero F4 Executes a Zero Re Zero Det F5 Change the det...

Page 56: ...Figure 19 Diagnostic Advanced Diagnostic menu 1 4 20 mA Diagnostic This combo box is used to manually control the 4 20 mA analogue outputs First select the board to diagnose by using the combo box ju...

Page 57: ...his combo box is used to confirm the valves on the I O Boards are working properly First select the I O Board to diagnose by using the combo box just under the title Valves Diagnostic Use the combo bo...

Page 58: ...iguration System menu 1 Analog output Two modes are available The Hold mode maintains the 4 20 mA outputs even if a new cycle is started The Track mode ensures analogue outputs always track input gas...

Page 59: ...the analyser switches to the next higher range The next integration gives the proper result If the result of a peak is lower than 90 of the lower range currently set the analyser switches to this lowe...

Page 60: ...imum 300 Resolution 1 Regen temp 200 Table 19 Oven set point DO NOT CHANGE THESE SETTINGS they are factory configured 8 Remote Starting Enable When the box is checked a cycle can be started by the dig...

Page 61: ...nt configuration This button is used to print the system configuration For analysers with multiple configurations this function will only print the current system configuration 13 Change Password This...

Page 62: ...GURATION on the menu bar and then on PID to access the CONFIGURATION PID menu see Figure 21 This menu allows changes to the PID settings for flows and ovens Be sure to save the current settings before...

Page 63: ...then on Flow to access the CONFIGURATION FLOW menu see Figure 22 This menu contains the flow sensor table set up during the factory configuration The information on this table may be useful when serv...

Page 64: ...ystem information when a cycle Real time chromatogram is in progress 1 General Cycle Data and 4 20 mA Peak Association This menu is used to set the duration of the cycle length of one chromatogram and...

Page 65: ...he grid at the top of this menu shows general information see Table 20 Peak Configuration Columns Additional information about the peak currently highlighted in the grid is shown in the area below the...

Page 66: ...e maximum full scale of the analyser Range 1 Shows the factor selected to re scale Range 2 to the lower Range 1 Unit Unit of the peak PPM PPB or Sample loop Volume of sample introduced in ccs ml Table...

Page 67: ...this menu are described below for information only Figure 25 Peak Detection configuration menu DO NOT CHANGE THESE SETTINGS they are factory configured Integration algorithm The peak detection method...

Page 68: ...reducing the integration window as a function of height which in turn reduces the integrated baseline noise Figure 27 shows the principle used for the peak window reduction the three parameters that a...

Page 69: ...start reduction factor has been set to 15 and the max end reduction factor has been set to 30 then at the maximum the total window is reduced by 45 Yellow integrated peak If a peak is detected the fil...

Page 70: ...alve state Each row in the grid indicates a sequence for the selected valve see the example shown in Figure 29 The timings for valve ON open or OFF close are set during factory configuration Figure 28...

Page 71: ...le which is used to change a flow set point during a cycle A time of 7200 secs means that this point is not in use In the example shown in Figure 30 the set point is 30 cc min at the beginning of the...

Page 72: ...Date Time Click on Configuration on the menu bar and then on Date Time to access the CONFIGURATION DATE TIME menu see Figure 31 Use the combo box control to change the value of the date and the time C...

Page 73: ...HESE SETTINGS they are factory configured Access to the Advanced Configuration menu requires entry of a password The default password is the serial number of the analyser and can be changed in the CON...

Page 74: ...peration NOTE Turning off System Alarm can be dangerous For example when working with Hydrogen the analyser will stop advising of problems The menu allows the RS232 communication can be turned ON and...

Page 75: ...tector is associated to the plasma cell by selecting its location on an I O board and its number on this I O board The plasma detector association is used to process alarms such as Plasma Off Plasma O...

Page 76: ...I O Board and a plasma detector see Figure 34 The menu shows the name given to each flow and its location on the appropriate I O Board and for a carrier regulator its association with a plasma detecto...

Page 77: ...yser 76 04416001A Revision 7 4 Valve The Valve menu associates a valve number to a valve channel on an I O Board see Figure 35 DO NOT CHANGE THESE SETTINGS they are factory configured Figure 35 Advanc...

Page 78: ...er 77 04416001A Revision 7 5 Oven The Oven menu associates an oven with an I O Board and a channel on the I O board see Figure 36 DO NOT CHANGE THESE SETTINGS they are factory configured Figure 36 Adv...

Page 79: ...LARM menu Figure 37 This menu allows configuration of the alarms The status alarm relay can be closed or opened when a status alarm is activated by clicking on the relevant radio box button To set the...

Page 80: ...a printer copy the printer driver to a USB stick and insert into the USB port on the front of the analyser Click on the Add Printer button and enter the password either c a i or the serial number of t...

Page 81: ...access the CONFIGURATION SYSTEM menu Insert a USB stick in the USB port on the front of the analyser Click on the Export Configuration button to export the data to the USB stick A message will appear...

Page 82: ...nalysed The analyser must be properly started and purged before the execution of a calibration The calibration procedure consists of the Noise Threshold Calibration followed by the Span Calibration Fi...

Page 83: ...mpleted YES is displayed in the TRS done column of the grid 7 Disable the Noise Threshold Calibration with the Disable F2 button one button performs dual functions Enable or Disable depending on the a...

Page 84: ...n are set during factory configuration 6 Select OK and the pop up menu will disappear 7 For multiple peaks repeat the above steps for each peak name 8 For each peak to be calibrated left click on the...

Page 85: ...the active mode Figure 40 Calibration Span menu The value set in the Calib Gas Value column must be the impurity value of the calibration gas before the dilution The software automatically calculates...

Page 86: ...ea that covers the peak in counts digital converter units This area is used to generate the concentration displayed in the Result column Response factor this is the area counts divided by the value in...

Page 87: ...are normally on the first I O board for a multiple chassis analyser Step 2 Select the output to be calibrated Step 3 Connect an ammeter to the corresponding output on the rear panel of the analyser St...

Page 88: ...equired to use the Report Software Two types of IP address can be configured Static or DHCP A static address is an address that is manually set once and a DHCP address is an address that is automatica...

Page 89: ...oftware button is used to test the analyser detection of a USB key that can then be used to acquire data for the Report Software 4 9 2 Remote Control Click on Remote on the menu bar and then on Remote...

Page 90: ...n the menu bar to access the ABOUT MENU Figure 44 About menu This menu shows the software version of the user interface PC the firmware versions of the embedded electronic boards and information about...

Page 91: ...s When the stored data reaches 99 capacity the new data will over write the files starting with the oldest To transfer the data insert a USB key into the port at the front of the analyser and press th...

Page 92: ...analyser is powered off If you close the analyser without using Quit there is the risk that data will be corrupted After the Quit button has been pressed wait for the black screen and then turn the po...

Page 93: ...ediately contact Servomex or local Servomex agent 4 If the analyser is not going to be used immediately o Place the analyser and any other equipment supplied back in its protective packing o Store the...

Page 94: ...upported both by the front and the back 6 1 1 Electrical safety WARNING Ensure that the electrical installation of the analyser conforms to all applicable local and national electrical safety requirem...

Page 95: ...ctrical supply cables must be rated of temperature of 70 C or higher Route cables that you connect to the analyser so that they do not present a trip hazard When carrying out insulation testing discon...

Page 96: ...er source must use properly rated cables see section 3 12 If an auxiliary oven is supplied connect the cable coming out of the auxiliary oven to the chassis connector named Auxiliary Oven see section...

Page 97: ...RO NanoChrome that is supplied with a master chassis and two secondary chassis The RS 485 port of the Master Chassis connects to the first RS 485 port of Secondary Chassis 1 The second RS 485 port of...

Page 98: ...RO NANOCHROME Gas Analyser 97 04416001A Revision 7 Figure 48 Figure 48 Master with 2 Secondary Chassis electrical connections WARNING The units shall only be connected using the cables supplied by Ser...

Page 99: ...always be connected to the same protective earth as the secondary chassis of the system If an auxiliary oven is supplied connect the cable coming out of the auxiliary oven to the connector named Auxil...

Page 100: ...PC with two secondary chassis The stand alone PC RS 232 port To Analyser connects to the RS 232 port on the Secondary Chassis 1 The RS 485 port on Secondary Chassis 1 connects to the RS 485 port on S...

Page 101: ...VOPRO NANOCHROME Gas Analyser 100 04416001A Revision 7 Figure 50 Stand alone PC with two Secondarys electrical connections WARNING The units shall only be connected using the cables supplied by Servom...

Page 102: ...tal input connection WARNING The digital input terminals are separated from the analyser mains circuits by reinforced insulation The terminals must only be connected to circuits that are themselves se...

Page 103: ...2 3 4 20 mA outputs The schematic of the 4 20 mA output circuit is shown in Figure 53 Use a shielded twisted cable to connect between the analyser and the monitoring system with a load resistor connec...

Page 104: ...7 4 20 mA 7 7 7 F7 8 4 20 mA 8 8 8 F8 9 HR HR HR F9 Table 24 4 20 mA connections and associated fuses WARNING The analogue output terminals are separated from the analyser mains circuits by reinforce...

Page 105: ...tional RS 232 port The computer is connected to the analyser by the mean of a DB 9 RS 232C Null modem cable The computer must have appropriate software to read the data transmitted by the analyser See...

Page 106: ...ampling system includes any pressure regulator valve line fitting filter purifier etc which is in contact with the sample or carrier gas to be introduced into the analyser Even small leaks can introdu...

Page 107: ...as purifier to generate the carrier gas 1 Gas Purifier The SERVOPRO PureGas purifier is available with either compression or VCR fittings and for use with 110V or 220VAC power supplies The model numbe...

Page 108: ...The carrier gas is normally He which will be taken to Carrier Inlet 1 For multiple chassis configurations the carrier gas should be split to feed each chassis Carrier Inlet 2 Carrier Inlet 2 will be...

Page 109: ...ses carrier gas to dilute a calibration gas to a fixed ratio nominally a factor of 20 to generate a suitable span gas concentration That means a suitable span gas concentration of 5ppm will be diluted...

Page 110: ...o 6 for all chassis CAUTION A SERVOPRO NanoChrome may consist of multiple chassis Each chassis has its own internal dilution system which will require verification of the dilution ratios for each rele...

Page 111: ...aps are removed Do not pressurise detector vent s The carrier gas must be connected to the analyser before power is applied 1 Verify main voltage rating 2 Connect carrier gas purifier and follow insta...

Page 112: ...em To purge the internal dilution system go into Calibration Calibration menu and click the button Click for Span This activates the internal dilution system Leave the analyser in that state for 5 min...

Page 113: ...for 12 injections Verify that the last 4 results are within repeatability specification Compare with results from the analyser Test Results Sheet TRS 21 Inject the process gas continuously and monitor...

Page 114: ...e same value as for the previous calibration procedure This will ensure the same sample volume is injected The default value is 50 cc min per channel 4 Clean the cabinet fan filter periodically This w...

Page 115: ...ciated equipment in a clean dry area Do not subject it to excessively hot cold or humid conditions 9 2 Disposal Dispose of the analyser and any associated equipment safely and in accordance with the l...

Page 116: ...e Directive by the application of EN 61010 1 and rated for Over Voltage Category II Pollution Degree 2 The analyser complies with the Class B digital apparatus requirements of ICES 001 of Canada throu...

Page 117: ...cter No Character ASCII Code No hex Meaning 1 3Eh 2 B 42h command ID 3 1 31h 1 success 4 1 or 0 31h or 30h Analyser ready 1 ready 0 not ready still running 5 1 or 0 31h or 30h Run Modus 1 measurement...

Page 118: ...n 0 and 9 20h or 30h to 39h 81 Space or any Character between 0 and 9 20h or 30h to 39h 82 Space or any Character between 0 and 9 20h or 30h to 39h 83 Space or any Character between 0 and 9 20h or 30h...

Page 119: ...an 30h or 31h 5 3Ch 5 Peak 2 0 or 1 30h or 31h 6 Peak 3 0 or 1 30h or 31h 7 Peak 4 0 or 1 30h or 31h 8 Peak 5 0 or 1 30h or 31h 9 Peak 6 0 or 1 30h or 31h 10 Peak 7 0 or 1 30h or 31h 11 Peak 8 0 or 1...

Page 120: ...nstable baseline 1 2 3 4 5 21 24 3 No peak 6 7 8 9 19 22 23 24 26 4 Saturated detector signal 1 2 3 4 19 21 24 5 Negative peaks 1 2 3 4 24 6 NMHC baseline drift 10 7 Poor repeatability on span calibra...

Page 121: ...ide integration window 15 14 Span bottle almost empty 10 content 16 15 Unstable ambient conditions pressure temperature 17 16 Span gas mixture 18 17 Wrong span gas background mixture 19 19 Damaged det...

Page 122: ...is stable 15 Verify that carrier gas set points are as per analyser TRS Verify that carrier gas flow is stable Verify that oven temperature are as analyser TRS and stable Revalidate PIDs and re save...

Page 123: ...amination such as particulates or moisture 27 Connect a flow meter to the carrier vent Reduce carrier supply pressure to have a vent flow close to the one specified in the analyser TRS 28 Verify dilut...

Page 124: ...implement the WEEE Directive For additional information and advice on the disposal of the analyser in accordance with the requirements of the WEEE Directive contact Servomex at info servomex com or yo...

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