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SI Analytics TITRONIC 300 Operating Manual Download Page 34

 

  

84 

 

4.5.4

 

Sample identification 

In the manual titration it is possible to input a sample identification. The possible input includes manual, automatic 
or no sample identification at all. 
 

Fig. 62 

 

For the manual sample  ID, a prompt for the sample  ID  will always be displayed at the start of the method  (Cp. 
also ch

apter 3.6, Main menu). For an ‘automatic’ sample ID there will be selected a master ID (in the current case 

this is water, cp. Fig. 68), which will then automatically be numbered starting on 01. 
 

Fig. 63 

 

After a new power-up, numbering will resume with 01. 
 

4.5.5

 

Documentation 

Fig. 64 

 

Two different format settings are available for documentation on a printer or USB memory stick: short and GLP: 
 

Summary of Contents for TITRONIC 300

Page 1: ......

Page 2: ...6 Instructions importantes Le manuel d utilisation fait partie de l appareil Prière de lire et d observer attentivement le mode d emploi avant la première mise en marche de l appareil et de le conserver Pour des raisons de sécurité l appareil ne pourra être utilisé que pour les usages décrits dans ce présent mode d emploi Nous vous prions de respecter également les modes d emploi pour les appareil...

Page 3: ...ng with the Piston burette TITRONIC 300 66 3 1 Front Keyboard 66 3 2 Display 66 3 3 Manual controller 67 3 4 External PC Keyboard Optional 67 3 5 Menu Structure 68 3 6 Main Menu 70 3 6 1 Manual Titration 70 3 6 2 Dosage 72 4 Method Parameters 75 4 1 Method editing and new method 75 4 2 Default Methods 76 4 3 Copy Methods 76 4 4 Delete Methods 77 4 5 Change Method Parameters 77 4 5 1 Method type 77...

Page 4: ...ment Non compliance may result in injury or material will be destroyed Status at time of printing Advanced technology and the high quality of our products are guaranteed by a continuous development This may result in differences between this operating manual and your product A potentially more recent version of this manual is available on our internet website at www si analytics com The German ver...

Page 5: ...spensions containing high solids percentages may clog or even damage the dosing system General provisions The safety guidelines that are applicable to the handling of chemicals have to be observed under all circumstances This applies in particular to inflammable and or etching liquids Guarantee We provide guarantee for the device described for two years from the date of purchase This guarantee cov...

Page 6: ...upply power supply 100 240 V 50 60 Hz power input 30 VA Input 12 Volt DC 500 mA Use the Power supply TZ 1853 Type No FW 7362M 12 only RS 232 C Interface RS 232 C interface separated Daisy Chain function available Data bits adjustable 7 or 8 Bit default 8 Bit Stop bit adjustable 1 or 2 Bit default 1 Bit Start bit static 1 Bit Parity adjustable even odd none Baud rate adjustable 1200 2400 4800 9600 ...

Page 7: ...idity 80 for temperatures up to 31 C linear decrease down to 50 relative humidity at a temperature of 40 C Dosing units Cylinder Piston burette TITRONIC 300 20 ml DURAN borosilicate glass 3 3 cylinder Piston burette TITRONIC 300 50 ml DURAN borosilicate glass 3 3 cylinder UV protection cover made out of TROGAAMID blue transparent Valve volume neutral cone valve made from fluorocarbon polymers PTFE...

Page 8: ...ed into the casing If the Piston Burette TITRONIC 300 has been altered technologically or if unauthorized personnel tried or succeeded to open the instrument as attempt to repair it In case that the user operates such a device all thereof resulting risks are on the user The Piston Burette TITRONIC 300 must not be stored or operated in humid rooms For reasons of safety the Piston Burette TITRONIC 3...

Page 9: ...e of the power supply TZ 1853 has to be plugged in to the 12 V socket in see Fig 3 back panel chapter 2 3 on the back panel of the Piston Burette Then plug the power supply into the plug socket Fig 1a Place the power supply easily accessable in order to be able to remove the Piston Burette anytime easily from the power circuit The stirrer connects to the right side at the bottom and is locked in p...

Page 10: ...face mini USB for connection to a PC 5 Connection of the external power supply TZ 1853 6 On Off switch 2 3 3 Connecting a printer Printers with a USB interface are to be connected to one of the two USB A interfaces These printers have to feature HP PCL emulation 3 3 enhanced 5 5e no GUI and GDI printers 2 3 4 Connecting a USB device manual controller keyboard memory device hub The following USB de...

Page 11: ...ll appear once the boot sequence is completed Fig 4 Using MODE followed by System settings you navigate to the system settings The very first menu is to be used for setting the language of the country Fig 5 The first menu is the language settings Fig 6 Use OK to call the menu Select the national language using the arrow keys confirm it with ENTER OK ...

Page 12: ...62 Fig 7 The selected language will appear immediately Pressing the ESC key twice will return the user to the main menu ...

Page 13: ...ing tube and suction hose 4 TZ 1748 stand rod 5 Z 305 titration clamp 6 TZ 3620 dosing hose with dosing tip and holding bracket bracket TZ 3875 7 TZ 3803 1 litre reagent bottle brown 8 TZ 3656 titration tip unit blue 9 TZ 3801 valve cover lid and TZ 3000 3 2 way valve 10 TZ 3130 20 ml dosing unit or TZ 3160 50 ml dosing unit 11 TZ 3283 connection hose 12 TZ 3281 suction hose 1 2 3 4 5 6 7 8 9 10 1...

Page 14: ...adequately sized waste bin has to be placed below the titration tip On the main menu fig 9 Fig 9 Press MODE key and select Rinsing Fig 10 Confirm the selection by pressing OK At this point you can select the number of rinsing cycles Fig 11 Initial filling requires a minimum of two rinsing cycles You can stop the rinsing operation Fig 12 and 13 at any time by pressing STOP and then resume rinsing w...

Page 15: ...ig 12 Fig 13 Fig 14 Fig 15 The rinsing program Fig 12 15 can be canceled at all time with STOP and the continued with START When the rinsing is finished you can get back to the start menu by pushing 2 x ESC ...

Page 16: ...T Changing the current method new method copy and delete method standard methods ESC ESC will take you back to the previous menu level START STOP Start and Stop of a current method FILL Filling the burette Arrow key up Choosing of a menu or changing a number Arrow key down Choosing of a menu or changing a number Arrow key right Changing position of the cursor Enter 3 2 Display The display consists...

Page 17: ...andard methods F4 FILL Fill the interchangeable unit F5 Display and modification of the balance data F6 MODE Selection of method rinsing system settings balance data F7 SYS System settings language selection time date F8 CAL No function on the TITRONIC 300 F9 Change of sign F10 DOS Call dosing menu Num Scroll and Lock Lock Without function Prt Sc and Sys Rq Without function ESC Selection of the me...

Page 18: ... used Fig 19 Fig 19 Pressing START will result in the immediate execution of the method shown EDIT F3 will take you to the method parameters Fig 20 Fig 20 At this point you can modify the current method create a new method call and memorise standard methods copy or delete an existing method print a method titration methods only Use the und keys to select the submenus confirm your selection with OK...

Page 19: ...selection with OK ENTER Once the selection made you will return to the main menu with the newly selected method If no method is selected ESC will also take you back to the main menu To navigate directly to the system settings Fig 22 and Fig 23 you can use the SYS F7 key you can also navigate there through the method selection menu Fig 22 Fig 23 ...

Page 20: ...tion is always performed using the manual controller Manual titration is impossible without the manual controller Fig 25 Using START pressing the Black key on the manual controller will start the manual titration method Depending on the settings of the method the system will prompt you for the sample description Fig 26 and the sample weight Fig 27 You can use an external PC keyboard optional to en...

Page 21: ...input of the sample description and or the sample weight sample volume the following display will appear Fig 29 You can control the metering rate with the black key of the mouse A single depression of the key will cause a step up to the first level Depending on the size of the dosing unit this corresponds to 0 0025 ml 20 ml or 0 00625 ml 50 ml Displayed are 0 003 or 0 006 ml from a single step If ...

Page 22: ...the STOP F2 key or approx for 1 sec the grey key of the mouse The titration result will be calculated and displayed and optionally printed on the connected printer or USB stick in PDF format Fig 31 ESC will take you back to the start menu way to start the next titration immediately Filling of the interchangeable unit occurs automatically 3 6 2 Dosage To start a dosage method please use the START F...

Page 23: ...ill not occur automatically unless the maximum cylinder volume has been reached or the automatic filling option always was activated The unit can be filled at any time using FILL A dosing operation can also be performed without any dosing method with the DOS F10 key of the external keyboard Fig 35 This is the point to input the volume which will be dosed following the confirmation with OK ENTER ...

Page 24: ...erformed using OK or ENTER Filling of the unit following dosage will not occur automatically here unless the maximum cylinder volume has been reached The unit can be filled at any time using FILL ESC will take you back to the main menu ...

Page 25: ...t for the input of a method name Fig 38 This prompt will not appear in the case of the modification of an already created method Fig 38 The method name can contain up to 21 characters Special characters are also possible If no keyboard is connected the method name being displayed has to be adopted in the present case Method 01 Numbering of methods will occur automatically Press OK ENTER to confirm...

Page 26: ...sequently you will be taken to the Change method parameters item Please continue at this point with Chapter 4 5 4 3 Copy Methods Methods can be copied or stored with a new name If you select this function the current method will be copied and you can include a new name Fig 41 Fig 41 A new name with the suffix 1 will be assigned automatically so as to avoid the existence of 2 methods having the sam...

Page 27: ...The input or modification of the method name was already described in Chapters 4 1 and 4 3 Fig 43 4 5 1 Method type On the Method type you can select whether you wish to perform a manual titration or a dosage or whether you wish to prepare a solution Fig 44 Fig 44 The selection of the Method type will have an influence of the further parameterisation of the method For instance if you select the do...

Page 28: ...ion On the Formula Selection submenu you can select the appropriate calculation formula Fig 47 The following calculation formulae are available for manual titration Titration formula Additional information ml Used to calculate the consumption in ml ml B T M F1 W F2 Formula for calculating the concentration of a sample taking into account a blank value in terms of ml B ml T M F1 W F2 Formula for ca...

Page 29: ...eviations used ml Titration solution consumption in ml B Blank value in ml in most cases determined by titration T Titer of the titration solution e g 0 09986 M Mol Mol or equivalent weight of the sample e g NaCl 58 44 F1 Factor 1 Conversion factor F2 Factor 2 Conversion factor W Weight sample weight in grams or sample volume in ml After selecting a formula please confirm your selection with OK EN...

Page 30: ...eight is automatically transferred by a connected balance Fixed sample weight A fixed sample weight is input in g This weight will then automatically be used for each start of the method without any sample weight being enquired by a prompt Manual sample volume The sample volume in ml is prompted at the start of the method and manually input Fixed sample volume A fixed sample volume is input in ml ...

Page 31: ... 5 Global Memories If a titration result should be used again later e g the factor or titer of a solution or a blank value it can be saved automatically The creation of a global memory is possible when using an external keyboard only The creation of a global memory can be managed with the system settings or by typing Shift F5 on the external keyboard This leads to the Global memory Fig 54 A global...

Page 32: ...ther be accepted or substituted by a designation of a blank value or a titer Fig 57 This value can be used with the formula Fig 58 The blank value being titrated previously is always taken into account automatically Fig 59 ...

Page 33: ...sing speed ml min 20 ml 40 50 ml 100 The filling speed can be set in terms of seconds from 20 to 999 The standard setting of this value is 30 seconds For diluted aqueous solutions the filling speed can be six to 20 seconds For non aqueous solutions the filling speed should be set to the 30 seconds In the case of highly viscous solutions such as concentrated sulphuric acid the filling speed should ...

Page 34: ...ID will always be displayed at the start of the method Cp also chapter 3 6 Main menu For an automatic sample ID there will be selected a master ID in the current case this is water cp Fig 68 which will then automatically be numbered starting on 01 Fig 63 After a new power up numbering will resume with 01 4 5 5 Documentation Fig 64 Two different format settings are available for documentation on a ...

Page 35: ...d name date time sample description sample weight sample volume results and calculation formula N A Same as Short documentation plus method contents Dosing Only method printout Method name date time dosing parameters N A N A The documentation can also be stored in PDF and CSV files on a connected USB stick ...

Page 36: ... Fig 67 Setting the national language was already described in Chapter 2 5 5 1 Reagents Dosing Unit In this menu you can set the size of the dosing unit 20 or 50 ml perform an exchange of the dosing unit and enter reagents data being stored during manual titration in the GLP documentation Fig 68 5 1 1 Dosing unit exchange Confirm with OK ENTER the size of the dosing unit ...

Page 37: ... dosing unit starts without any warning Therefor please place the titration tip in a reagents bottle or beaker The piston is moving up to 85 Fig 70 Then the system prompts to unlock the dosing unit Fig 70 Then please unlock the dosing unit as shown in fig 71 Fig 71 ...

Page 38: ...ttach the new one just like it was before The two struts of UV protection must comply with the mark on the housing Fig 73 Fig 73 Accept by pushing OK ENTER In case you changed the size of the dosing unit you can choose which size you attached Fig 74 If you want to change the reagents data you can reset all reagent data ...

Page 39: ...be chosen Unit size 20 or 50 ml adjustable Reagent name default blank Concentration default 1 000000 Concentration determined on default actual date To be used until default actual date Opened Produced on default actual date Test according to ISO 8655 default actual date Charge description default blank Last modification default actual date ...

Page 40: ...2 5 5 3 RS232 Settings The RS232 settings item can be used to determine the device address of the TITRONIC 300 and set the parameters of the two RS232 interfaces separately Fig 78 The device address can be set from 0 15 Address 1 is the default setting Fig 79 ...

Page 41: ... is preset to 4800 It may be set to 1200 19200 Fig 81 The parity setting can be selected amongst No Even and Odd No is the standard setting Fig 82 You may select between 7 and 8 data bits 8 bits is the standard setting Fig 83 ...

Page 42: ...tte please use the USB socket When printing please check whether the correct printer is connected It is not possible to print HP printer layouts on a Seiko thermal printer or vice versa The printer settings should always be checked and adjusted after changing the printer Fig 85 Only one printer at a time can be connected because automatic printer recognition is not supported HP PCL is the default ...

Page 43: ...fer to chap 5 9 The RESET has to be confirmed separately once again Fig 87 5 7 Device Information Device Information contains information about the current software version the serial number of the device printer driver and update version device address set number of measurements Starts of a method a number of strokes filling cycles Fig 88 Please hold this device information ready for service purp...

Page 44: ...ries can be stored and restored on a connected USB memory It is also possible to transfer the settings from one titrator to another one The backup will be started with Settings backup Abb 90 Back settings is displayed during the backup in blue Abb 91 After a Reset or a maintenance case it is possible to restore the backup with Restores settings ...

Page 45: ...rt werden die Einstellungen übertragen bzw wieder hergestellt Abb 92 Abb 93 5 10 Software Update Fig 94 An update of the device software requires a USB stick containing a new version For this operation the two files that are needed have to be located in the root directory of the USB stick ...

Page 46: ...e function The valid software updates will be shown on the display In the present case this is Version 14_29 from week 29 year 2014 Fig 95 After starting the update using OK ENTER next thing to appear is the following graphic Fig 96 which will change after a few seconds to the following display Fig 97 ...

Page 47: ...re completely and proceed to a new start Please note During the update the device must not be switched off Important In the course of an update the methods will not be deleted You can continue to use them If no valid update file is stored on the USB stick the following message will appear Fig 99 ...

Page 48: ...nces The balance is to send the balance data via RS 232 C only by means of a print command The balance is to send the balance data only after the display standstill The balance should never be set to automatic sending and or send continuously Handshake on the balance must be set to off or even Software Handshake or Pause No special characters such as S or St are allowed to be used as prefix in the...

Page 49: ... a change a star will appear opposite the weighed in quantity Fig 101 Weights may be deleted or added individually It is also possible to delete all weights at one stroke Fig 102 If no balance data is available the No balance data found message will appear Fig 103 ...

Page 50: ... connect the TITRONIC 300 via a mini USB to a USB interface of a PC To accomplish this connection a driver has to be installed on the PC Then the USB B interface takes over the function of the RS232 1 interface Please contact SI Analytics for acquiring the software The address always consists of two characters e g address 1 of the two ASCII characters 0 and 1 The addresses can be set from 00 to 15...

Page 51: ...ume in ml aa0 200 aaDA dose volume without filling with adding the volume aaY aaDB dose volume without filling reset of the volume aaY aaDO dose volume with filling without adding the volume aaY aaGDM dosing speed in ml min aaY aaGF filling time in seconds min is 20 default 30 aaY aaES ESC function one step backwards aaY aaEX EXIT function back to main menu aaY aaGDM dosing speed in ml min 0 01 10...

Page 52: ...eaking this may result in damage to the piston burette If the liquid is left within the system you will also have to reckon with corrosion and an alteration of the solutions used over time which includes e g crystallisation Considering that as of the state of the art there are no plastic hoses available for the use in titration equipment which would be perfectly free of diffusion phenomena particu...

Page 53: ... cylinder and in the titration hose where they can be detected easily If bubbles become visible please re tighten all connections finger tight and then repeat dosing If air bubbles still remain within the system 6 please check the valve and replace the hose connections The air bubbles may also occur at the interface between the sealing lip of the piston and the cylinder If a reduction of the filli...

Page 54: ...80 Formulae for manual titration 78 Front Keyboard 66 interchangeable units 103 Interrupted use 102 Main Menu 70 Maintenance 102 manual controller 67 manual controller TZ 3880 60 Manual Titration 70 max dosing titration volume 83 method name 75 method parameters 75 new method 75 printer 60 Reagents Dosing Unit 86 RESET 93 RS232 Settings 90 safety information 58 Sample identification 84 Sample weig...

Page 55: ......

Page 56: ...igences spécifiées pour le produit sont respectées Certificado del fabricante Certificamos que el aparato arriba mencionado ha sido controlado de acuerdo con la norma DIN EN ISO 9001 sección 8 2 4 Seguimiento y medición del producto y que cumple con los requisitos de calidad fijados para el mismo Hersteller Manufacturer Xylem Analytics Germany GmbH Dr Karl Slevogt Str 1 82362 Weilheim Germany SI A...

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