Reactor-Ready - Lab Reactor
8. Set-Up & Operation
8.1 Optimising the thermal performance of Reactor-Ready
The thermal performance, whether heating or cooling, will be affected by:-
a. Ambient temperature and atmospheric conditions
b. Liquid load to be heated/cooled
c. Heating and cooling power of the thermoregulator
d. Nature of the thermofluid
Please take care to consider and optimise these parameters if you wish to maximise the
performance of your Reactor-Ready system.
8.2 Operating temperature range
Reactor-Ready can be used from -60°C to 190°C (thermofluid temperature) without damage
to the unit. The working reaction temperature range will vary depending on thermoregulator,
vessel size, contents volume etc as stated above.
8.3 Setting up Reactor-Ready
8.3.1
Identify a level and clear space within your fumehood to site your Reactor-Ready
assembly. Moving the assembly after set-up is not recommended so take care to plan your
services and connections carefully.
8.3.2
You will require two power outlets for an overhead stirrer and thermoregulator, cooling
water supply for the reflux condenser, inert gas and vacuum supply for operating under an
inert atmosphere.
8.3.3
Make sure there is room for connections to your thermoregulator and that all thermofluid
hoses can be positioned and supported safely. Position the Base on a flat surface within your
fumehood such that the 5 feet are squarely positioned. Check that all feet are contacting the
fumehood surface and that the Reactor-Ready unit is level. Adjustments can be made to
individual feet by screwing in or out to achieve this. Locate the Drip Tray in the base.
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Warning - Risk of burns from hot or cold parts -
The Reactor-
Ready unit will remain hot or cold for some considerable time after the heat-
ing/cooling source has been switched off. A temperature probe or temperature
sensitive label can be used to indicate when components are too hot or cold
to touch. Always wear suitable protective equipment such as gloves, face pro-
tection, aprons etc.
!
Warning -
Reactor-Ready should only be operated by trained and compe-
tent personnel. As with all chemistries, a full risk assessment should be per-
formed prior to starting, and care should be taken to monitor your reactions at
all stages. During operation Reactor-Ready should not be left unattended
unless in a supervised area.
!
Warning -
Always refer to the manufacturers specifications for your ther-
mofluid before using it with Reactor-Ready to be sure of any limitations or
safety restrictions.
!
Warning -
Always read the overhead stirrer instructions before operating
the system.
!
Warning -
Always refer to the manufacturers operating instructions for your
thermoregulator before using it with Reactor-Ready to be sure of any limita-
tions or safety restrictions.
!
8.3.1
8.3.3
