Pike 10Spec Installation And User Manual Download Page 6

 

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Installation 

The 10Spec accessory has been aligned and tested in the PIKE Technologies facility on the make of your 
FTIR spectrometer to ensure that it performs to specifications. However, some variation in optical 
alignment can occur from spectrometer to spectrometer. To allow for this difference, there are 
alignment screws located within the 10Spec assembly for fine-tuning once the accessory is installed in 
the spectrometer.  

 

Accessory Installation 

1.   Set your FTIR spectrometer to collect data at 4 cm

-1

 spectral resolution (including the FTIR J-stop). 

 
2.  The 10Spec accessory fits into the sample compartment of the FTIR spectrometer. Your 10Spec is 

provided with the appropriate sample compartment baseplate for the model FTIR instrument you 
specified.  Before inserting the accessory in the sample compartment, ensure that your 
spectrometer is aligned. If the instrument is not aligned, maximize the interferogram signal (the IR 
energy throughput) of your FTIR spectrometer. This should be performed by following the 
manufacturer’s instructions. 

 
3.   Fasten the accessory directly into the FTIR sample compartment or onto the FTIR sample 

compartment baseplate. In order to locate the accessory in the correct position, simply place the 
entire accessory into the FTIR sample compartment with the 10Spec label facing the front and line 
up the baseplate provided with the holes/pins in your model FTIR spectrometer. 

 
4.   Tighten the mounting screws to firmly position the accessory baseplate onto the FTIR sample 

compartment baseplate. 

 

Accessory Alignment 

The 10Spec accessory may not require any alignment when installed - see page 5 for minimum energy 
throughput values. However, should you choose to fine-tune the accessory, follow these steps: 
 
1.

 

Place the 10Spec into the sample compartment. Using the large mask (2 inch), place the gold mirror 
over the mask opening (sample position). 

  
2.

 

Remove the front panel of the 10Spec by removing thumb screws. 

 
3.

 

Display the live interferogram of the FTIR spectrometer and adjust the output (detector) side tilt 
mirror. The location of this mirror is shown in Figure 2 (page 4). Turn the individual screws clockwise 

Summary of Contents for 10Spec

Page 1: ...Installation and User Guide 10SpecTM 10 Degree Specular Reflectance Accessory...

Page 2: ...s This document contains confidential or proprietary information of PIKE Technologies Inc Neither this document nor the information herein is to be reproduced distributed used or disclosed either in w...

Page 3: ...y 2 Packing List 2 Installation 3 Accessory Installation 3 Accessory Alignment 3 Performance Verification 5 Using Your 10Spec Accessory 5 Reflectance Spectra and Applications 6 Free Standing Films 6 E...

Page 4: ...the sample is approximately 12 mm The accessory may be used to measure the reflectivity of glass per ASTM Standard E1585 93 and other specular reflectance experiments The 10Spec is well suited for sp...

Page 5: ...accessory we have included a packing list Please inspect the package carefully Packing List 10Spec Manual 10Spec Accessory Sample Masks 3 8 5 8 2 PN 350 010000 PN 010 10XX PN 010 3010 Quantity 1 Quan...

Page 6: ...ur FTIR spectrometer This should be performed by following the manufacturer s instructions 3 Fasten the accessory directly into the FTIR sample compartment or onto the FTIR sample compartment baseplat...

Page 7: ...tput mirror is accessed from the back of the accessory 7 Repeat the entire procedure two to three times to fine tune the accessory This is an initial alignment procedure which optimizes the 10Spec to...

Page 8: ...of the accessory should be at least 15 at 1000 cm 1 If your accessory does not meet this minimum value contact PIKE Technologies Please have ready the serial number of your accessory found on rear of...

Page 9: ...od of the fringes will give the thickness of the film as long as the refractive index is known For an angle of incidence and a refractive index n the equation governing this measurement is where m is...

Page 10: ...s the sample is smooth flat and non scattering Effect of Dispersion The spectra of many samples are distorted by anomalous dispersion in the sample The reflectivity of a sample is dependent upon the r...

Page 11: ...rsion Kramers Kronig Transform In order to produce a spectrum that is corrected for this anomalous dispersion a correction known as a Kramers Kronig transformation may be performed on the spectrum Thi...

Page 12: ...the infrared with the minimum spectral interferences the mirrors used in this device are uncoated bare aluminum on a glass substrate Since the coatings are soft care must be taken to avoid damage Nor...

Page 13: ...6125 Cottonwood Drive Madison WI 53719 5120 608 274 2721 TEL 608 274 0103 FAX info piketech com www piketech com...

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