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Troubleshooting
276
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Check that the injector is not clogged. You will need to remove the Quick-
Change Torch Module and disassemble the torch as described in
on page 173. Remove the spray chamber and either
remove the torch and then the injector or remove the injector leaving the torch
in place.
Performance Problems
Checking the Sample Introduction System
Many performance problems (such as poor precision or loss of signal) can be traced
to the setup and condition of the sample introduction system.
The following list describes general checks for the sample introduction system,
which should be done on a regular basis. Typical symptoms of problems are listed to
help you determine whether maintenance is required.
If you have already done performance checks, refer to the Syngistix Software Guide
on the Syngistix Document Pack CD for details
.
The sodium bullet test is also a good way of visually checking the sample flow in the
plasma and, therefore, indicates problems in sample introduction. This test is
described earlier in this chapter.
Pump and Pump Tubing
Is the tubing overstretched, or does it have flat spots, leaks, or discoloration?
Install new tubing, stretching it gently beforehand. If using organics, special tubing
should be used. See the list of replacement parts at the end of
Is the flow of liquid irregular?
Refer to the adjustment procedure in
Do the pump rollers bind or not roll easily? Are there grooves in the pump rollers?
On the PerkinElmer pump, the pump head may be removed for cleaning. The pump
head may also be replaced. See
Summary of Contents for AVIO 200
Page 1: ...AVIO 200 SPECTROMETER Hardware Guide ICP OPTICAL EMISSION ...
Page 2: ......
Page 3: ...AvioTM 200 Spectrometer Customer Hardware and Service Guide ...
Page 12: ...Contents 10 ...
Page 30: ...28 ...
Page 31: ...Safety Practices 1 ...
Page 32: ...30 Safety Practices ...
Page 56: ...54 Safety Practices ...
Page 57: ...Preparing Your Laboratory 2 ...
Page 58: ...Preparing Your Laboratory 56 ...
Page 70: ...Preparing Your Laboratory 68 ...
Page 71: ...System Description 3 ...
Page 72: ......
Page 97: ...Installation 4 ...
Page 98: ......
Page 119: ...Installation 117 Figure 4 8 Replacing the torch 1 3 4 6 8 2 9 10 5 7 ...
Page 121: ...Installation 119 1 2 7 9 8 10 3 4 5 6 ...
Page 164: ...Installation 162 ...
Page 165: ...Maintenance 5 ...
Page 166: ......
Page 184: ...Maintenance 182 1 2 7 9 8 10 3 4 5 6 ...
Page 188: ...Maintenance 186 Figure 5 8 Replacing the Torch 1 3 4 6 8 2 9 10 5 7 ...
Page 272: ...Maintenance 270 ...
Page 273: ...Troubleshooting 6 ...
Page 274: ......
Page 293: ...Troubleshooting 291 Figure 6 1 Normal Plasma Conditions at 0 torch position ...
Page 294: ...Troubleshooting 292 Figure 6 2 Normal Plasma at 3mm position ...
Page 297: ...Troubleshooting 295 Figure 6 5 Injector too far forward ...
Page 298: ...Troubleshooting 296 Figure 6 6 No Aux Gas Torch may be glowing ...
Page 299: ...Troubleshooting 297 Figure 6 7 Air Leak or Spray Chamber Temperature too high ...
Page 300: ...Troubleshooting 298 Figure 6 8 Thin Plasma due to leak in Plasma Gas Line ...
Page 308: ......