parr 4520 Operating Instructions Manual Download Page 5

 

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4520 Bench Top Reactors

Parr Instrument Company 

 

 

Intended Usage

 

This system has been designed for use as 

a high pressure reactor system.  It has been 
designed, built, and tested to strict physical 
and electrical standards.  However, it is the 
user's responsibility to install and operate it in 
conformance with local pressure and electrical 
codes.  If this equipment is used in a manner 
beyond its intended usage, the protection 
provided by the equipment may be impaired. 

 

 

 

User’s Responsibility 

All Parr reactors and pressure vessels are 

designed and manufactured with great care to 
assure safe operation when used within their 
prescribed temperature and pressure limits.  
But . . . the basic responsibility for safety when 
using this equipment rests entirely with the 
user; who must: 

1.  Select a reactor or pressure vessel 

that 

has the capability, pressure rating, 
corrosion resistance, and design features 
that are suitable for its intended use.  Parr 
engineers will be glad to discuss available 
equipment and material options with 
prospective users, but the final 
responsibility for selecting a reactor or 
pressure vessel that will perform to the 
user's satisfaction in any particular reaction 
or test must rest with the user - not with 
Parr. 

In exercising the responsibility for the 

selection of pressure equipment, the 
prospective user is often faced with the 
choice between over-or under-designed 
equipment.  The hazards introduced by 
under-designed pressure vessels are 
readily apparent, but the penalties that 
must be paid for over-designed apparatus 
are often overlooked.  Recognizing these 
criteria, Parr reactors and pressure vessels 
are offered in several different styles, each 
designed for convenient use in daily 
operation within certain temperature and 
pressure limits, using gaskets, closures, 
and other elements carefully selected for 
safe operation within the limits specified for 
that design.  But in order to preserve the 
validity of these designs, all temperature

 

and pressure limits must be observed, and 
no attempt should be made to increase 
these limits by making alterations or by 
substituting components which are not 
recommended by Parr Instrument 
Company. 

2.  Install and operate

 the equipment within 

a suitable barricade, if required, with 
appropriate safety accessories and in full 
compliance with local safety codes and 
rules. 

All standard Parr pressure vessels are 

provided with either a suitable relief device 
or a means to attach one (typically in the 
form of a plugged opening).  When a 
pressure vessel is delivered without a 
pressure venting device, it is the 
customer’s responsibility to provide 
pressure relief in order to protect the 
operator and the equipment from 
destructive high pressures.  If you need 
more information or need help in selecting 
a proper relief device, please contact Parr 
Instrument Company. 

3.  Establish training procedures

 to ensure 

that any person handling the equipment 
knows how to use it properly. 

4. 

 

Maintain the equipment

 in good 

condition and establish procedures for 
periodic testing to be sure the vessel 
remains structurally sound. 

 

 

 

Unpack Carefully 

Unpack the equipment carefully and check 

all the parts against the packing list.  If 
shipping damage is discovered, report it 
immediately to the delivering carriers.  The 
vessel, motor, heater, and temperature 
controller may be packed separately for 
convenience in shipping, but these parts are 
easily reassembled.  Examine the 
components closely for any loose parts or 
shipping damage and be sure to check all 
layers of packing materials thoroughly so as 
not to overlook any parts which might 
otherwise be discarded. 

 

Summary of Contents for 4520

Page 1: ...383M 4520 BenchTop Reactors Operating Instruction Manual...

Page 2: ...14 Releasing Pressure 14 To Open the Vessel at Completion of a Test 15 Initial Operating Test 15 Variable Speed Electric Motor 15 Accessories 16 Internal Cooling Coils 16 Liners 16 Spare Parts Kit 16...

Page 3: ...e type and rating of fuse 4 Disconnect from the power supply before maintenance or servicing To avoid personal injury 1 Do not use in the presence of flammable or combustible materials fire or explosi...

Page 4: ...tude Limit 2 000 meters Storage 25 C and 65 C 10 to 85 relative humidity Provisions for Lifting and Carrying The Series 4520 Bench Top Reactors and their components are very heavy Before moving ensure...

Page 5: ...n daily operation within certain temperature and pressure limits using gaskets closures and other elements carefully selected for safe operation within the limits specified for that design But in orde...

Page 6: ...rmined by the physical characteristics of the vessel material and will be prescribed on an individual basis The maximum working pressure and temperature for any vessel is governed by the design of the...

Page 7: ...ector is to be used only with Parr Instrument Company motor assemblies supplied with the appropriate motor power cord 2 For Fixed Head Reactors Bolt the stand to the bench table or floor using the hol...

Page 8: ...the power cord into an appropriate outlet Power for these reactors should be drawn from a grounded outlet capable of carrying up to the full current rating of the reactor 11 If an electric stirrer mot...

Page 9: ...nstructions based upon the fixed head or movable vessel options There are differences in the design of the stand components which adapt the vessels to the support system Flat PTFE Gasket or Self Seali...

Page 10: ...alve is easily identified when the vessel is open by noting that it is connected to a dip tube which extends to a point near the bottom of the cylinder This is an angle pattern valve with an attached...

Page 11: ...alve Gas Release Valve Pressure Gage Plug extra port Gas Release Valve Stirrer Shaft Assembly Adjustable Impeller Thermocouple Gas Inlet Valve Coupling for Gas Hose Connection Adapter Bushings Thermow...

Page 12: ...shed in a variety of ranges to met individual needs Typically the gage and the rupture disc are furnished as matched ranges For applications where a gage is selected with a range under 1000 psi a reli...

Page 13: ...a firm but hard pull to each bolt Allow the vessel to stand for about five minutes after the initial tightening procedure to allow for the flow of the PTFE gasket under load then retighten the bolts S...

Page 14: ...w for expansion as a result of the heating process As a general rule the liquid charge should not exceed two thirds of the capacity of the cylinder Too much liquid in the vessel can lead to the develo...

Page 15: ...should be taken when lifting the head from the cylinder so damage will not occur to the internal fittings Initial Operating Test Read all operating instructions carefully so as to be well acquainted...

Page 16: ...acement coil with the internal fittings before tightening the nuts Once the nuts are tightened it may be necessary to manually squeeze or slightly adjust the serpentine loops of the coil to position i...

Page 17: ...d adjust the oiler to feed one drop per minute into the air stream For long continuous runs at high speeds the oiling rate should be increased to three drops per minute If the motor becomes sluggish f...

Page 18: ...contain switches and other elements that are not explosion proof The minimal spark hazard associated with these units can be resolved by installing the controller in a remote location outside of the h...

Page 19: ...kept of deflections at specific test pressures so that any increase in deflection becomes a warning that the metal has lost strength Any cylinder that fails to return to its original dimensions after...

Page 20: ...se compression ring be sure that it is in place on the head before attaching any head fittings The compression ring cannot be installed after fittings have been screwed into the head 8 Clean all threa...

Page 21: ...from alternate materials use the codes shown below as a suffix to the standard part number CM Alloy 400 CC Alloy 20Cb3 CT Alloy 600 CAD Titanium G2 CG Alloy B 2 CAA Titanium G4 CXA Zirconium G702 CH...

Page 22: ...rmocouple 1000 mL A472E6 Thermocouple 2000 mL A888HC2 Safety Rupture Disc assembly without disc see 231M A2685HC Cooling Sleeve assembly LD A740HC Cooling Sleeve assembly HD A1120HC6 Magnetic Drive as...

Page 23: ...23 4520 Bench Top Reactors Parr Instrument Company Removable Head Style Parts Lists Front View Removable Head Flat Gasket...

Page 24: ...24 4520 Bench Top Reactors Parr Instrument Company Removable Head Flat Gasket...

Page 25: ...25 4520 Bench Top Reactors Parr Instrument Company Fixed Head Style Parts Lists Front View Fixed Head Flat Gasket Light Duty Footless Mag Drive...

Page 26: ...26 4520 Bench Top Reactors Parr Instrument Company Back View Fixed Head Flat Gasket...

Page 27: ...27 4520 Bench Top Reactors Parr Instrument Company Fixed Head Flat Gasket...

Page 28: ...ng Internal 2 HD 732HC Snap Ring External 1 HD 2429HC Bushing PTFE HD UPPER DRIVE SHAFTS A2562HC Upper Drive Shaft A1120HC LD A2562HC2 Upper Drive Shaft A2140HC LD A2564HC Upper Drive Shaft A1120HC6 h...

Page 29: ...29 4520 Bench Top Reactors Parr Instrument Company Overarm Assembly...

Page 30: ...op and bottom on the head Change to appropriate material suffix for special alloy vessels for internal connection 2998HC10 Cooling Coil Serpentine 1L 2998HC20 Cooling Coil Serpentine 2L A92HWAD Male C...

Page 31: ...ter Assembly 1000W 230V 1L A2256HC12EB Heater Assembly 1000W 115V 1L w thermowell Part No Description A2256HC12EE Heater Assembly 1000W 230V 1L w thermowell A2256HC20EB Heater Assembly 1500W 115V 2L A...

Page 32: ...Revision 02 08 13...

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