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1108 Oxygen Combustion Vessel

P a r r   I n s t r u m e n t   C o m p a n y

12

Maintenance and Safety Instructions

Bomb Maintenance

Under normal usage Parr oxygen combustion ves-
sels will give long service if handled with reason-
able care. However, the user must remember that 
these bombs are continually subjected to high 
temperatures and pressures which apply heavy 
stresses to the sealing mechanism. The mechanical 
condition of the bomb must therefore be watched 
carefully and any parts that show signs of weakness 
or deterioration should be replaced before they fail. 
Otherwise, a serious accident may occur.
 

Do not fire the bomb 

if gas bubbles are observed 

anywhere indicating a possible gas leak. Disas-
semble the parts and install new seals immediately. 
The bomb head parts which require closest attention 
and most frequent replacement are: the 230A O-ring 
head gasket, all the 238A sealing rings, the 415A 
O-ring and the 20VB PCTFE valve seat in the needle 
valve.

When replacing the 230A head gasket, stretch the 
new O-ring and let it snap into place to be sure that 
it moves freely in its groove and is not twisted.

The 20VB valve seat in the needle valve deteriorates 
with use, not only in the needle area but on the un-
derside of the seat as well. Leakage and a possible 
serious burn-out can result from a worn or damaged 
seat if it is not replaced promptly. As a basic rule, 
the 20VB valve seat and the two 238A O-rings on 
the valve needle should be replaced after every 500 
firings or every six months, whichever occurs first. 
If the bomb is used for samples containing chlorine, 
these parts should be replaced after every 250 fir-
ings.

To replace the valve seat, unscrew the 397A com-
pression nut; remove the valve stem and the old 
seat, and disassemble all of the parts. Drop a new 
20VB valve seat into the body and push it down 
into place. Slide a 7VBCM Monel washer, two 238A 
O-rings and the 378A packing cup onto the A420A 
valve needle assembly with the needle pointed up-
ward; then adjust the parts on the needle so that the 

tip of the needle is flush with-or slightly recessed 
into-the bottom of the packing cup. Insert this as-
sembly into the 396A outlet valve body and press it 
firmly against the valve seat by tightening the 397A 
compression nut to 100 inch-pounds of torque.

A Parr 475A Service Clamp offers a convenient 
means for clamping the bomb head firmly in a vise 
without damaging the head when replacing any of 
the bomb head parts.

Keep the 397A compression nut on the valve needle 
tightened firmly at all times. Frequent tightening 
is important. This nut, if slightly loose, may allow a 
leak to develop during the rapid pressure rise upon 
ignition. This type of leak may not be detectable be-
fore firing; but if it develops, the hot gases can ignite 
the 20VB valve seat and burn through the head.
Do not use extreme force when closing the needle 
valve. A moderate but firm turn on the valve knob 
should be sufficient to stop all gas flow. Excessive 
needle pressure will deform and possibly close the 
gas passage. If this happens, unscrew the valve 
body and replace the 20VB valve seat. Accumulated 
salt deposits may also clog the gas passage, mak-
ing it difficult to release pressure at the end of a run. 
To avoid this, clean the passage through the valve 
needle and deflector nut with a small drill.

The 238A sealing ring in the insulated electrode 
should be replaced with the same frequency as the 
20VB valve seat. Also, keep the 411A terminal nut 
tight at all times. As the 238A sealing ring ages and 
hardens it becomes a partial electrical conductor, 
permitting misfires and producing unwanted heat-
ing effects. Periodic replacement will eliminate this 
potential problem.

The threads on the screw cap should be checked 
routinely for any burns or other deformity. After 
long use, the threads on the screw cap may become 
worn to the point where they will no longer provide 
a safe closure for the bomb, and the screw cap will 
have to be replaced. The following procedure can be 
used to check the extent to which the threads have 
become worn:

Summary of Contents for 1108

Page 1: ...205M 1108 Oxygen Combustion Vessel Operating Instruction Manual...

Page 2: ...very Procedure 7 Samples and Sample Holders Particle Size and Moisture Content 8 Combustion Aids 8 Sample Pellets 8 Combustion Capsules 8 Foodstuffs and Cellulosic Materials 9 Coarse Samples 9 Corrosi...

Page 3: ...nstructions carefully in order to obtain a complete understanding of the capabilities and limitations of an 1108 Oxygen Combustion Vessel and to be well aware of the pre cautions to be observed in its...

Page 4: ...ications Parr offers the 1108CL Oxygen Combustion Vessel described below It should be noted that all instructions for the 1108 apply equally to the 1108CL as well A Chlorine Resistant Bomb The 1108CL...

Page 5: ...flame emerging from it will not impinge directly on the tip of the straight electrode Liquids in the Bomb Most combustion procedures call for a small amount of liquid to be placed in the bottom of the...

Page 6: ...ng Filling the Bomb The instructions below de scribe a manual system us ing the 1825 Oxygen Filling Connection furnished with other Parr apparatus Oxygen for the bomb can be drawn from a standard comm...

Page 7: ...stand Do not twist the head during removal Pull it straight out to avoid sticking Examine the interior of the bomb for soot or other evidence of incomplete combustion If such is found the test will h...

Page 8: ...st be added in a pellet form 2 gm pellets Never combust benzoic acid in powder form Sample Pellets One of the most useful techniques for handling powdered samples is to compress the material into a ta...

Page 9: ...h sulfur samples or with samples contain ing over 20 mg of chlorine may corrode the metal surfaces and produce a dull film on the inner walls of the bomb Materials containing appreciable amounts of ca...

Page 10: ...ent collapse of the disc when pres sure is applied Fill the bomb with oxygen to the usual charging pressure but add oxygen slowly so that the tape will not collapse into the cup Fire the bomb and comp...

Page 11: ...r condition sometimes causes spalling and the ejection of unburned fragments 5 The use of an ignition current too low to ignite the charge or too high causing the fuse to break before combustion is un...

Page 12: ...A valve needle assembly with the needle pointed up ward then adjust the parts on the needle so that the tip of the needle is flush with or slightly recessed into the bottom of the packing cup Insert t...

Page 13: ...the resistance of the metal to further attack can be improved by restoring the surface to its original highly polished condition Bombs needing repolishing or other repair work can be returned to the...

Page 14: ...Maintenance Checklist Refer to page 12 13 16 17 of the 1108 Operating Instruction Manual for assembly instructions and parts diagram 500Test Maintenance Replace the following Date Date Date Date 410A...

Page 15: ...Notes w w w p a r r i n s t c o m 15...

Page 16: ...Spacer 13 SC1932SC10 Socket Head Set Screw 14 278A3 Adapter Bushing 15 404A2 Deflector Nut 16 406A Lock Nut 17 5A10 Loop Electrode with Sleeve 18 4A10 Straight Electrode with Sleeve 19 401A Sleeve Ins...

Page 17: ...i n s t c o m 17 Parts for the 1108 Oxygen Combustion Vessel 1 3 10 30 28 9 19 A A A A 2 4 5 6 8 7 11 9 29 7 7 27 26 25 24 23 13 12 15 20 21 22 18 15 14 16 17 PROPRIETARY NEITHER THE DRAW NOR INFORMA...

Page 18: ...tion A1673E2 Kit Electric Parts for 2901EB EE 1203EEE Cord 10A 220V Cont Europe Plug 1202EEE Cord 13A 220V BS Plug 2000E Transformer 120 240 VAC 24V XB0010 1 8ID ShrinkTubing Black 34E2 Cord w 115VAC...

Page 19: ...e seat PCTFE 21VBBB Lantern ring brass 53A Oxygen gage 3 1 2 0 60 atm 112VB4AK Valve needle 124VB Union nipple brass CGA540 A140VB Toggle relief valve A150VB Valve knob 188A2 Filling connection body b...

Page 20: ...Revision 08 26 13...

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