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USER MANUAL

Manual Version:

1.0.C

Product Code:

T2006A

Product Version:

1.0

Software Version:

1.0

POTENTIOSTAT

Summary of Contents for T2006A

Page 1: ...USERMANUAL Manual Version 1 0 C Product Code T2006A Product Version 1 0 Software Version 1 0 POTENTIOSTAT ...

Page 2: ...Servicing 9 4 Requirements 9 5 Unpacking 10 5 1PackingList 10 5 2DamageInspection 10 6 Specifications 10 7 SystemComponents 11 8 Installation 12 9 Operation 13 9 1TakingaMeasurement 13 9 2SoftwareSettingsandControls 14 9 3TestCellChip 19 9 4PerformingCyclicVoltammetryofFerrocene 20 9 5Maintenance 23 10 Troubleshooting 24 11 Relatedproducts 25 11 1RelatedConsumables 25 11 2RelatedEquipment 25 ...

Page 3: ...ingimportant informationaboutmaterialsincluding Reductionandoxidationpotentials Reversibilityofareaction Electrontransferkinetics Energylevelsofsemiconductingpolymers ThePotentiostatiscapableofoutputtingpotentialsup10V andmeasuringcurrentsaslowas10nA allowingforawiderangeofmaterialcharacterisation Theeasy to usePCsoftwareincludedwiththesystem allowsanyonetoperformthemeasurement ...

Page 4: ...ssila com declarethattheDoCisissuedunderoursoleresponsibility andbelongstothefollowingproduct Product Potentiostat T2006A1 Serialnumber T2006A1 xxxx Objectofdeclaration Potentiostat T2006A1 Theobjectofdeclarationdescribedaboveisinconformity withtherelevantUnionharmonisationlegislation EMCDirective2014 30 EU RoHSDirective2011 65 EU Signed Name DrJamesKingsley Place Sheffield Date 01 10 2019 ...

Page 5: ...τότηταςΕΕ Κατασκευαστής OssilaLtd SolproBusinessPark WindsorStreet S47WD ΗνωμένοΒασίλειο ΔηλώνουμευπεύθυναόnοαναφερόμενοςεξοπλισμόςσυμμορφώνεταιμετησχεnκήνομοθεσίαεναρμόνισηςτηςΕΕπουυπάρχει σnςπροηγούμενεςσελίδεςτουπαρόντοςεγγράφου Español DeclaracióndeconformidadUE Fabricante OssilaLtd SolproBusinessPark WindsorStreet S47WD ReinoUnido Declaramosbajonuestraúnicaresponsabilidadqueelsiguienteproduct...

Page 6: ...dsorStreet S47WD ReinoUnido Declarasobsuaexclusivaresponsabilidadequeoequipamentoindicadoestáemconformidadecomalegislaçãodeharmonização relevantedaUEmencionadana s página s anterior es destedocumento Română DeclaraţiedeconformitateUE Producător OssilaLtd SolproBusinessPark WindsorStreet S47WD RegatulUnit DeclarăpeproprierăspunderecăechipamentulprezentatesteînconformitatecuprevederilelegislaţieiUEd...

Page 7: ...uppliedwitha24V 2ADCpoweradapterwithapowercordforthecountryofpurchase in accordancewithEuropeanCommissionregulationsandBritishStandards Useofanyotherelectricalpower cables adaptors ortransformersisnotrecommended 3 3HazardIcons Thefollowingsymbolscanbefoundatpointsthroughoutthemanual Noteandreadeachwarningbefore attemptinganyassociatedoperationsassociatedwithit Table3 1 Hazardwarninglabelsusedinthi...

Page 8: ...heunittoOssilaLtd Thewarrantywillbeinvalidatedif ModificationorservicehasbeencarriedoutbyanyoneotherthananOssilaengineer Theunithasbeensubjectedtochemicaldamagethroughimproperuse Theunithasbeenoperatedoutsidetheusageparametersstatedintheuserdocumentation associatedwiththeunit Theunithasbeenrenderedinoperablethroughaccident misuse contamination improper maintenance modification orotherexternalcause...

Page 9: ...onentsforevidenceofshippingdamage Ifdamagehasoccurred pleasecontactOssila directlyforfurtheraction Theshippingpackagingwillcomewithashockindicatortoshowiftherehasbeen anymishandlingofthepackageduringtransportation ThePotentiostatspecificationsareshowninTable6 1below 6 Specifications Table6 1 Potentiostatspecifications Potentialrange 7 5V Potentialcompliance 10V Appliedpotentialresolution 333μV App...

Page 10: ...tiostatcomprisesfouritems theOssilaPotentiostat bananacables poweradaptor and OssilaCyclicVoltammetrysoftware 7 SystemComponents Figure7 1 OssilaPotentiostat Figure7 2 Cellconnectioncable Figure7 3 The24VDCpoweradapter ...

Page 11: ...e SMU Driver folderandruneither Windows 32 bitSMUDriver for32 bitoperatingsystemsor Windows64 bitSMUDriver for64 bit operatingsystems II Note onWindows10thedriverswillinstallautomaticallywhentheunitisconnected III Ifthedriversfailtoinstall pleaserefertotheSMUUSBDriverInstallationGuidefoundonthe USBmemorystick 3 Connectthe24V 2ADCpoweradaptortothepowersocketontherearoftheunit 4 Connecttheunittoyour...

Page 12: ...dclipconnectstotheworkingelectrode II Theblackclipconnectstothecounterelectrode III Theblueclipconnectstothereferenceelectrode 4 StarttheOssilaCyclicVoltammetrysoftware ThewindowshowninFigure9 2willopen 5 Entertheappropriatesettingsforyourexperimentintothesoftware explainedinmoredetailin Section9 2 6 Clickthe Measure button I Thesystemwillsweepthepotentialbetweentheworkingelectrodeandreferenceelec...

Page 13: ...ls 9 2 1MeasurementSettings Figure9 2 OssilaCyclicVoltammetrysoftware Figure9 3 Measurementsettings I ConnectedSystems SelecttheCOMportoftheconnectedunityouintendtouse I Thisboxwillbepopulatedautomaticallywiththeaddressesofanyunitsconnectedtothe computerwhenthesoftwarestarts II Torescanforconnectedunits incasetheconnectionischanged clicktherefreshiconnextto thedrop downbox ...

Page 14: ...IV PotentialVertex1 V Thefirstpotentialinvoltsatwhichthescanchangesdirection V PotentialVertex2 V Thesecondpotentialinvoltsatwhichthescanchangesdirection VI ScanRate mV s Therateatwhichthepotentialwillbechangedduringthescan measuredinmillivoltspersecond VII Cycles Thenumberoftimesthescanwillberepeated I SaveSettings Savesthecurrentsettingsasaprofilethatcanbeloadedquicklyforuseatanothertime Whencli...

Page 15: ...ttothe drop downbox Figure9 5 Controlstostartandstopthemeasurement Figure9 6 Readoutofthepotentialandcurrentatthemousecursorlocation I Measure Clickingthisbuttonwillstartthemeasurementusingthechosensettings Thisbuttoncannotbeclickedifthesoftwarehasnotdetectedaunit II Abort Stopsameasurementthatiscurrentlyinprogress I PotentialandCurrentReadout Whilstthemousecursorisoverthegraph thepotentialandcurr...

Page 16: ...clicking the A buttoninthebottom leftofthegraph asshowninFigure9 7 III SelectingandRemovingCurves Whentherearemultiplecurvesonthegraph oneofthemisconsideredtheactivecurve Thiscurvewillbe displayedinblue whilsttheothercurveswillbegrey Bydefault thelastcurvetobemeasuredistheactive curve Youcanchangewhichcurveistheactivecurvebyclickingonanycurveusingtheleftmousebutton Toremoveanindividualcurvefromthe...

Page 17: ...Directory and SampleName fieldsmustbefilledinbeforethe measurementcanstart thesearedetailedbelow II SaveDirectory Setsthelocationinwhichtosavetheresults Thiscanbeseteitherby I Manuallytypingthedirectoryintothefield II Copyingandpastingitfromyourfileexplorer III Clickingthefoldericoninthefield whichwillopenadialogboxtoallowtheselectionofafolder tosaveto III SampleName Setsthenameofthecomma separate...

Page 18: ...dingonthedirectionofthepotentialscan 9 3TestCellChip Figure9 10 OssilaTestCellChip Figure9 11 SettingsformeasuringtheTestCellChip 9 3 1TakingaMeasurement 1 PluginandturnonthePotentiostat 2 UsethecellconnectioncabletoconnectthePotentiostattothesamecolourconnectorsonthe TestCellChip I RedconnectortoWE1 2 3 or4 II BlackconnectortoCE III BlueconnectortoRE 3 StarttheOssilaCyclicVoltammetrysoftware Thew...

Page 19: ...licvoltammetry I BeforeStarting WerecommendswitchingonthePotentiostat30minutespriortouse Thisallowsittowarmupandreacha stabletemperature ensuringastablemeasurement Furthermore ensurethatallapparatus solventsandelectrolytesaredry Thisisbecausethepresence ofwateranditsredoxby productsmayreducethesolventpotentialwindoworreactwiththesolventor analyte II CleanandDrytheElectrochemicalCellandElectrodes T...

Page 20: ...utylammoniumhexafluorophosphate 387 4g mol necessarytomakeup20mlof0 1Msolution Addacetonitrileuptomarkofthevolumetricflaskand stiruntiltheelectrolytehasdissolved Securetheelectrochemicalcellwithaclamptoensureitisstablebeforeaddingthe20mlofelectrolyte solution Oncedissolved addapproximately10mgofFctothesolutionandstirtodissolveit IV SetuptheElectrodes Placethecapontheelectrochemicalcell theninsertt...

Page 21: ...9 13 sweepingthevoltagefrom 0 4Vto0 6Vandbackto 0 4V Setthe StartPotential and PotentialVertex2 fieldsto 0 4Vandthe PotentialVertex1 fieldto0 6V Thescanrateandnumberofcyclesneedtobeset Thescanratewillaffectthemagnitudeofthecurrent peaksinthescan withfasterscanratesresultingingreatermeasuredcurrents Inthismeasurementwe willuseascanrateof100mV s sosetthe ScanRate fieldto100mV s Thenumberofcyclesisho...

Page 22: ...ameasurementisabortedpartway through youmayneedtocleantheworkingelectrodetoremoveanymaterialwhichhasbuilt upthere Figure9 15 Atypicalvoltammogramforferrocene Thecellandelectrodesshouldalwaysbethoroughlyrinsedimmediatelyaftereachexperimentwiththe solventthatwasusedinyourelectrolyte Alwayssetthecelltodry preferablyinanoven beforeyouprepare yourelectrolyte Thishelpsreducecontaminationofyoursolution 9...

Page 23: ...alledon thecomputer b Thesoftwarehasnotinstalledproperly a InstallthesoftwareonacomputerwithWindows Vistaornewer b Tryreinstallingthesoftware Cannotconnectto thesystemviaUSB a TheUSBcablemaynotbe connectedproperly b TheUSBcablemaynotbeconnected toaworkingUSBport c TheUSBdriversmaynotbeinstalledor maynothaveinstalledproperly d TheUSBcableisdefective a EnsuretheUSBcableisfirmlypluggedin atbothends b...

Page 24: ...ic devices no programming knowledge necessary Source voltage measure current get data Simplify and accelerate your data collection Accurate pre calibrated and tested micropipettes available in a range of volumes Clear and amber screw top vials suitable for storage of solvents solutions and samples An easy to use tool for the rapid measurement of sheet resistance resistivity and conductivity of mat...

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