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41

40

7. Probe Care and Maintenance

pH electrode care

Since your pH electrode is susceptible to dirt and contamination, clean it every one
to three months depending on the extent and condition of use. For specialty elec-
trode care, consult the instruction manual included with your electrode.

pH electrode storage

For best results, always keep the pH bulb wet. Use the protective electrode storage
bottle or rubber cap filled with electrode storage solution to store your electrode (see
page 46 for ordering information). Also, you can store in a pH 4 buffer with 1/100
part of saturated KCl. Other pH buffers are OK for storage, but NEVER use distilled
water for storage.

After measuring

1. 

Rinse the pH electrode and reference junction in de-ionized water.

2. 

Store the electrode as recommended above in “pH electrode storage,” or as 
recommended by the manufacturer.

3. 

Prior to next use, rinse the liquid junction with de-ionized water and tap dry—
never wipe electrode.

If this does not restore electrode to normal response, see

“Reactivating the pH electrode” section below.

pH electrode cleaning

Salt deposits:

dissolve the deposits by immersing the electrode in tap water for ten

to fifteen minutes. Ten thoroughly rinse with distilled water.

Oil/grease film:

wash electrode pH bulb gently in some detergent and water. Rinse

electrode tip with distilled water or use a general purpose electrode cleaner (see
page 40 for ordering information).

Clogged reference junction:

heat a diluted KCl solution to 60 to 80°C. Place the

sensing part of the electrode into the heated solution for about 10 minutes. Allow the
electrode to cool in some unheated KCl solution.

Protein deposits:

prepare a 1% pepsin solution in 0.1 M of HCl. Set the electrode in

the solution for five to ten minutes. Rinse the electrode with distilled water.

Reactivating the pH electrode

If stored and cleaned properly, your pH electrode should be ready for immediate
use. However, a dehydrated bulb may cause sluggish response. To rehydrate the
bulb, immerse the electrode in a pH 4 buffer solution for 10 to 30 minutes. If this
fails, the electrode requires activation. Never touch or rub glass bulb. Contact
builds up an electrostatic charge.

CONTINUED ON NEXT PAGE

7.1

Notes

To clear all pH data, see page 31.

See page 51 for a table of factory default settings.

P9.0: Resetting to factory default settings (conductivity/TDS)

This program lets you reset all conductivity parameters to factory default settings.
This clears all calibration data any other conductivity setup functions you might
have changed. The following settings will remain as you have set them:

• temperature unit of measure (°C or °F)
• The temperature offset calibration value
• All pH calibration data and parameters

MEAS

SETUP

mS

µ

S

ppt

ppm

A

MEAS

SETUP

MEAS

SETUP

mS

µ

S

mS

µ

S

ppt

ppm

ppt

ppm

B

6.10

From measurement mode

1. 

Press the Mode key 

to select 

conductivity measurement mode.

2. 

Press Setup key 

to enter Set Up mode.

3.

Press the 

and 

keys

to scroll through

subgroups until you view parameter
“P5.0” in the lower display. 

See figure

4. 

Press the ENTER key

.

See figure

5. 

Press the 

and 

keys

to toggle

between NO and YES.
• NO retains current settings
• YES resets to factory default settings

6.

Press the ENTER key

to confirm 

selection and to return to measurement
mode.

A

B

Summary of Contents for 35631-00

Page 1: ...me period please return freight prepaid and correction will be made without charge OAKTON alone will determine if the product problem is due to deviations or customer misuse Out of warranty products w...

Page 2: ...ady indicator auto endpoint function 28 P3 2 Selecting number of pH calibration points 29 P3 3 Selecting C or F 30 6 5 Program 4 0 Resetting to factory default settings pH 31 6 6 Program 5 0 Viewing p...

Page 3: ...splay also shows error messages keypad functions and program functions mS ATC READY MEAS CAL HOLD ERR F SETUP ON OFF C S K pH mV pH ppt ppm 2 1 Primary display Secondary display 3 2 21 20 14 17 16 15...

Page 4: ...ions In advanced set up mode Press CAL MEAS to return to main menu from sub menus Press CAL MEAS again to return to measurement mode from main menu ENTER Press to confirm values in Calibration mode an...

Page 5: ...To connect the pH electrode 1 Slide the BNC connector of the probe over the BNC connector socket on the meter Make sure the slots of the connector are in line with the posts of the socket Rotate and...

Page 6: ...eplaced on a point by point basis in pH and on a range by range basis in conductivity or TDS For example pH if you previously calibrated your meter at pH 4 01 7 00 and 10 01 and you recalibrate at pH...

Page 7: ...each of the ranges you are measuring All new calibration data will over ride existing stored calibration data for each measuring range you calibrate If you are measuring in ranges near to or greater t...

Page 8: ...and 1 If necessary press the MODE key to select TDS mode See figure 2 Rinse the probe with de ionized water or a rinse solution then rinse with a small amount of calibration standard 3 Dip the probe i...

Page 9: ...nal reading To exit this program without confirming the temperature calibration value DO NOT press ENTER in step 7 Press CAL MEAS instead 5 Measurement To take readings 1 Rinse the pH electrode with d...

Page 10: ...y to toggle between conductivity and pH readings Taking Conductivity or TDS Measurements ATC READY MEAS C S A A 5 2 B B Immerse probe beyond upper steel band Notes You can use the conductivity TDS man...

Page 11: ...h time you turn the meter off 5 4 From measurement mode 1 Press the Mode key to select conductivity measurement mode 2 Press Setup key to enter Set Up mode 3 Press the and keys to scroll through subgr...

Page 12: ...E C CAL F F The meter will now compensate readings for the manually set temperature Notes To exit this program without confirming the manual temperature compensation value DO NOT press ENTER in step...

Page 13: ...onductivity TDS calibration data R2 R2 0 0 199 9 S 10 0 99 9 ppm P5 3 View conductivity TDS calibration data R3 R3 0 1999 S 100 999 ppm P5 4 View conductivity TDS calibration data R4 R4 0 00 19 99 mS...

Page 14: ...electrode parameters for diagnostic purposes It lets you view P2 1 Electrode offset P2 2 Electrode slope SETUP pH A A SETUP mV pH B B 6 3 SETUP pH C C From measurement mode 1 Press the Mode key to se...

Page 15: ...See figure 5 Press the and keys to select the configuration you require OFF switches the READY indicator off ON switches the READY indicator on ON and HOLD together switches the auto endpoint feature...

Page 16: ...the ENTER key See figure 5 Press the and keys to toggle between NO and YES NO retains current settings YES resets to factory default settings 6 Press the ENTER key to confirm selection and to return...

Page 17: ...to your calibration 6 7 mS SETUP S ppt ppm A A SETUP K B B From measurement mode 1 Press the Mode key to select conductivity or TDS measurement mode 2 Press the Set up key to enter Set Up mode See fig...

Page 18: ...eter 7 1 See figure 5 Press the and keys to select the configuration you require ON switches the READY indicator on OFF switches the READY indicator off ON and HOLD together switches the auto endpoint...

Page 19: ...solution See Appendix 2 on page 49 for information on how to calculate the TDS factor 7 Press the and keys to select your calculated TDS conversion factor 8 Press the ENTER key to confirm selection a...

Page 20: ...e temperature coefficient is the amount of change in conductivity per degree of temperature it is expressed in percent per C or F Entering the exact temperature coefficient of your solution lets you a...

Page 21: ...ode into the heated solution for about 10 minutes Allow the electrode to cool in some unheated KCl solution Protein deposits prepare a 1 pepsin solution in 0 1 M of HCl Set the electrode in the soluti...

Page 22: ...nstead of performing this reactivation procedure 1 Dip or stir the pH electrode in alcohol for 5 minutes 2 Leave the electrode in tap water for 15 minutes 3 Dip and stir the electrode in concentrate a...

Page 23: ...al LCD Operating temperature 0 to 50 C 32 to 122 F Power four 1 5 V AAA batteries included Battery life 200 hours continuous use Probe connectors pH mV BNC connector Conductivity TDS Temperature notch...

Page 24: ...00654 00 pH 4 01 calibration buffer 1 pint WD 00654 04 pH 7 01 calibration buffer 1 pint WD 00654 08 pH 10 01 calibration buffer 1 pint WD 00654 12 pH 12 45 calibration buffer 1 pint Model No Solution...

Page 25: ...in the above formula The result should be the TDS value 12 Appendix 1 Conductivity to TDS Conversion Factors 1 Factor the conductivity to ppm TDS conversion factor Multiply conductivity by this factor...

Page 26: ...the meter readings 15 Appendix 4 Meter factory default settings Resetting the meter to factory default settings clears all calibration data and most other setup functions you might have changed The fo...

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