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MIC SAS II 5800 Operator Manual in PDF format

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NOTE

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— Cautions contain information to help prevent actions that may damage the

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Original Instructions (English)
Part Number 580-42800-01 (Rev - ) Released June 2019
Copyright 2019
Micromeritics Instrument Corporation
4356 Communications Drive
Norcross, GA / USA / 30093-2901

iv

MIC SAS II 5800 Operator Manual

580-42800-01 (Rev - ) — June 2019

Summary of Contents for MIC SAS II 5800

Page 1: ...OPERATOR MANUAL 580 42800 01 June 2019 Rev MIC SAS II 5800 SUB SIEVE AUTOSIZER...

Page 2: ...s Instrument Corporation Copyright The software described in this manual is furnished under a license agreement and may be used or copied only in accordance with the terms of the agreement ___________...

Page 3: ...ations of this warranty will be limited under the following conditions 1 Certain products sold by MICROMERITICS are the products of reputable manufacturers sold under their respective brand names or t...

Page 4: ...a wide range of industrial sectors PID Eng Tech Madrid Spain complements Micromeritics renowned offering for catalyst characterization with technology for the measurement and optimization of catalytic...

Page 5: ...770 662 3696 www Micromeritics com Instrument Service or Repair Phone 1 770 662 3666 International contact your local distributor or call 1 770 662 3666 Service Helpdesk Micromeritics com Micromeriti...

Page 6: ...elp prevent actions that may damage the analyzer or components WARNING Warnings contain information to help prevent actions that may cause personal injury EU DECLARATION OF CONFORMITY To view the full...

Page 7: ...C SAS II 5800 1 6 2 MIC SAS Menu Selection 2 1 Load a Sample 2 3 Remove the Brass Sample Plug 2 4 3 Records Menu Selection 3 1 Reports 3 5 Calibration Report 3 5 Fisher Number Map Report 3 6 Log Repor...

Page 8: ...11 7 Troubleshooting and Maintenance 7 1 Gas Connections 7 3 Guidelines for Connecting Gases 7 3 Replace a Gas Cylinder 7 4 Connect a Regulator and a Gas Line to a Gas Cylinder 7 6 Power Instrument On...

Page 9: ...essure is maintained throughout the analysis by controlling the flow rate with a mass flow controller MFC After passing through the sample the gas passes through a flow restrictor to maintain some bac...

Page 10: ...ston Seals the top of the sample tube Safety shield Covers the exposed moving parts of the piston and anvil Touchscreen Touchscreen to run analyses and review edit records USB port The USB ports on th...

Page 11: ...ernal power supply Shelf for external power supply For external power supply storage USB ports 2 The USB ports on the front and back of the instrument can be used interchangeably however to prevent wi...

Page 12: ...particles may become airborne or skin contact may occur with the sample POWER SUPPLY Use of a power cord or power supply not provided with the instrument could cause personal injury or damage to the...

Page 13: ...on the instrument See Maintenance Menu Selection on page 6 1 Help Use to display instrument help Click the Online Help button scan the QR code or go to the specified web page Menu Selections INSTRUMEN...

Page 14: ...2 0 9 Compression accuracy 0 05 mm Environment temperature 15 to 35 C operating 0 to 50 C non operating Repeatability 3 Precision 3 Power 30 W Power supply External power supply 100 240 VAC 10 Power...

Page 15: ...onitor analyses The MIC SAS II performs two types of analyses l Organic mainly pharmaceuticals l Inorganic mainly for heavy metal powders such as tungsten When START is tapped the button changes to CA...

Page 16: ...ame text box Name of the analysis batch Cancel button Cancels the analysis and disengages the piston Collate results check box Produces a table in the Summary report All analyses with the same batch n...

Page 17: ...sample tube on top of the paper filter and press down until the sample tube is firmly seated around the brass plug 5 Insert the sample into the sample tube and weigh the sample tube assembly with the...

Page 18: ...tion tool into one sample brass plug and screw the extraction tool into the brass plug 3 Remove the brass plug from the bottom of sample tube 4 Pour out the sample or if necessary push the sample out...

Page 19: ...e bottom of the window l Fisher Number Map Report on page 3 6 l Calibration Report on page 3 5 l Log Report on page 3 8 Field or Button Description Batch Name Name of the analysis batch Control icons...

Page 20: ...lected record s as a ZIP file file format is MICSAS YYYY MM DD zip where YYYY MM DD is the download date to a USB device If using a remote browser a directory selector is opened for exporting the sele...

Page 21: ...sults check box Produces a table in the Summary report All analyses with the same batch name and the Collate option enabled appear in the Summary report Mass text box The sample mass Material text box...

Page 22: ...3 Records Menu Selection VIEW A RECORD Tap a blue link on the Records list to view a record 3 4 MIC SAS II 5800 Operator Manual 580 42800 01 Rev June 2019...

Page 23: ...dow and tap Calibration Report The Calibration Report lists l Temperature offset l Pin slope l Pin offset l Pdiff slope l Motor current percent l Disengage position l Engage position The date and time...

Page 24: ...f the Records window and tap Fisher Number Map A Fisher number map is a polynomial that relates SAS particle size to Fisher number for a particular material The Fisher particle size shown in reports i...

Page 25: ...lds have errors Selecting a row or focusing the Fisher number field highlights the corresponding point in the graph Changing the selections or the Fisher number for a selected point updates the coeffi...

Page 26: ...ation Home end entry shows the new home position l Analysis started with mass not within 5 of density l Pause resume and cancel l Shield placement and removal during analysis l Emergency stop and rese...

Page 27: ...ecords menu select one or more records then tap the Report icon 2 Select either Size Control Chart or Surface Area Control Chart Size Control Chart Control Charts MIC SAS II 5800 Operator Manual 580 4...

Page 28: ...3 Records Menu Selection Surface Area Control Chart 3 10 MIC SAS II 5800 Operator Manual 580 42800 01 Rev June 2019...

Page 29: ...ds menu item l Select one or more records to print l Click the printer icon A single import will be generated for all selected records Click the printer icon at the top of the page to send the report...

Page 30: ......

Page 31: ...Columns are sortable by tapping the column header l Tapping a link in a table row displays the SOP Tap a blue link in the SOP list to view or edit SOP details Tap the plus icon on the toolbar to creat...

Page 32: ...excluding the volume of pores and cavities Analysis Type button The type of analysis l Organics mainly pharmaceuticals l Inorganics mainly for heavy metal powders such as tungsten Batch name text box...

Page 33: ...ity button Organics Select the initial porosity for the analysis Last Modified The date and time the record was last modified Mass text box The sample mass Material text box Type of sample material us...

Page 34: ...olbar Deletes the selected SOPs from the list Tap the box to the left of the record to select it then tap the Delete icon to delete the selected SOPs Tap to create a new SOP SOP continued 4 4 MIC SAS...

Page 35: ...the direction of a Micromeritics Service Representative Component Description Anvil Anvil with O ring inside sample tube A brass plug with filter paper is placed between the sample material and the a...

Page 36: ...r Off On screen message that displays when power to the stepper motor has been powered off Shield Off On screen message that displays when the safety shield is not in place All buttons are disabled un...

Page 37: ...position is where there is no gap between the plugs RETURN THE PISTON TO THE HOME POSITION 1 Tap Instrument on the menu 2 Tap Home The piston lowers to the home position Home Position MIC SAS II 5800...

Page 38: ......

Page 39: ...the instrument Field or Button Description Advanced button Administrator level configuration options enabled only when the instrument is in the Idle state Maintenance 6 Maintenance Menu Selection MIC...

Page 40: ...lear the log file and remove tem porary and cached files from the disk l Upload logo button Tap to select a logo to display on reports See Upload Logo on page 6 11 l Allow calibration check box Enable...

Page 41: ...Name text box The name of the instrument ie lab number etc NTP button Enable to use Network Time Protocol for setting the instrument s clock The instrument must be attached to a network with NTP serv...

Page 42: ...reports To upload a logo tap Advanced on the Maintenance window Software version Version of the installed software application Surface area unit button Select whether surface areas are expressed as c...

Page 43: ...k Interface Cards NICs only change the settings of the NIC that is connected to the instrument Refer to the computer s operating system manual or the internet for instructions on how to change the net...

Page 44: ...ched to the instrument When configuration is complete use the Jobs tab to view queued print jobs 1 Tap the Maintenance tab 2 Tap Printers at the bottom of the window 3 On the Administration tab select...

Page 45: ...nter If the printer will be shared with other devices select the Share This Printer option Tap Continue when done 5 Select the printer model from the Model drop down list then tap Add Printer Printer...

Page 46: ...p Set Default Options 7 Tap the Printers tab The installed printer displays 8 Tap the Administration drop down list and tap Set as default printer 9 To specify additional printer options tap the Admin...

Page 47: ...10 Tap MIC SAS to return to the application Printer Installation MIC SAS II 5800 Operator Manual 580 42800 01 Rev June 2019 6 9...

Page 48: ...ument OFF attach or remove the keyboard then power the back ON See Power Instrument On and Off on page 7 8 Alternatively use the following instructions Attach a keyboard and refresh the browser 1 With...

Page 49: ...nt Ensure the file name is either MICSAS PNG or MICSAS BMP No other file names or file extensions are sup ported 2 Tap the Maintenance menu then tap Advanced 3 Tap Upload Logo 4 On the Confirm Action...

Page 50: ...2 Click Upload Logo and access the logo file Ensure the file extension is either PNG or BMP No other file extensions are supported 3 Select the file in the list then click Upload 4 On the Confirm Act...

Page 51: ...d the correct mass and density have been entered Cause The top brass sample plug and filter paper are not in place Action Install top brass sample plug and filter paper Cause Sample has escaped the tu...

Page 52: ...ded Action Go to the Instrument view and tap the stop icon white square in a blue rectangle If the piston is still unresponsive cycle power on the instrument Cause The emergency stop button was presse...

Page 53: ...ternally with a polymer l Long gas lines such as those used with gas cylinders placed in remote areas must be evacuated for an extended period of time to remove ambient gases When possible avoid placi...

Page 54: ...type 3 Open the gas regulator shut off valve by turning the knob counter clockwise Gas will be ven ted from the regulator 4 Turn the regulator control knob clockwise to open and vent any remaining gas...

Page 55: ...124 kPag AutoPore 50 60psig 345 404 kPag Gemini 15 18 psig 103 124 kPag MIC SAS II 15 20 psig 103 138 kPag TriStar 15 18 psig 103 124 kPag Regulator Pressure Settings Exceeding the maximum recommende...

Page 56: ...se 4 Attach the gas regulator to the connector on the gas cylinder Hand tighten the nut then use an appropriate wrench to tighten an additional 3 4 turn 5 Check for leaks at the high pressure side of...

Page 57: ...Purge the air from the gas line a Open the regulator shutoff valve b Open the gas cylinder shutoff valve and flow gas for 10 to 30 seconds c Close the gas cylinder shutoff valve and allow regulator p...

Page 58: ...nd will need to be reset See Home Position on page 5 3 Power ON the equipment in the following order 1 Plug in the instrument There is no ON OFF power switch 2 Allow the instrument to run for approxim...

Page 59: ...nt The following steps do not change any calibrations Pressing other buttons on the left side of the display may change calibrations 4 Install an empty sample tube 5 Enter a flow rate of 10 sccm and t...

Page 60: ......

Page 61: ...Internet connection is required for online help If internet connection is not available on the instrument go to http bit ly 2PCKB7B on a device with internet access or scan the QR code 8 Help MIC SAS...

Page 62: ......

Page 63: ...Records 3 1 SOP 4 1 menu selections 1 5 MIC SAS II about 1 1 MIC SAS menu selection 2 1 P power analyzer on and off 7 8 print records 3 11 INDEX A about the MIC SAS II 1 1 about this manual iv B brow...

Page 64: ...s 1 6 remote computer configuration 6 5 reports calibration 3 5 control chart 3 5 3 9 Fisher number map 3 6 log 3 8 S safety precautions 1 4 sample load 2 3 remove brass sample plug 2 4 SOP menu selec...

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