Metrohm 830 Page 24 Instructions For Use Manual Download | Manualshive

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2 Installation

2.4.8 Triathlon

Autosampler

Example

Automatic analysis of anions or cations on a modular system with elec-

tronic suppression using the Triathlon Autosampler.

Instruments

•

2.830.0020 830 IC Interface

•

2.819.0110 819 IC Detector

•

2.820.0210 820 IC Separation Center 820 with 1 injector and

column

heater

•

2.818.0110 818 IC Pump

•

2.135.0100 Triathlon

Autosampler

Interconnection

819

820

818

830

PC

6.2134.100

6.2134.130

6.2115.070

6.2134.090

6.2125.090

Triathlon

6.2134.000

6.2134.040

Fig. 11:

Connection of 819, 820, 818 and Triathlon

830 IC Interface / 8.830.1003 Instructions for Use

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Summary of Contents for 830

Page 1: ...830 IC Interface Instuctions for Use 8 830 1003 CH 9101 Herisau Switzerland E Mail info metrohm com Internet www metrohm com ...

Page 2: ......

Page 3: ...CH 9101 Herisau Switzerland E Mail info metrohm com Internet www metrohm com 830 IC Interface 5 830 0020 Program Instructions for Use 8 830 1003 07 2003 pkl ...

Page 4: ...dition 2003 These instructions are protected by copyright All rights reserved Although all the information given in these instructions has been checked with great care errors cannot be entirely excluded Should you notice any mistakes please inform the author at the address given above ...

Page 5: ...2 4 1 General information 10 2 4 2 819 IC Detector 820 IC Separation Center 818 IC Pump 12 2 4 3 833 IC Liquid Handling Pump Unit 13 2 4 4 833 IC Liquid Handling Suppressor Unit 14 2 4 5 833 IC Liquid Handling Sample Prep Unit 15 2 4 6 833 IC Liquid Handling Dialysis Unit 16 2 4 7 833 IC Liquid Handling Ultra Filtration Unit 17 2 4 8 Triathlon Autosampler 18 2 4 9 766 IC Sample Processor 19 2 4 10...

Page 6: ...g 7 Connection of 2 819 820 2 818 and 833 Suppressor Unit MIC 3 14 Fig 8 Connection of 833 Sample Prep Unit to MIC 6 for Neutralization 15 Fig 9 Connection of 819 820 818 833 Suppressor Unit and 833 Dialysis Unit 16 Fig 10 Connection of 819 820 818 833 Suppressor Unit and 833 Ultra Filtration Unit 17 Fig 11 Connection of 819 820 818 and Triathlon 18 Fig 12 Connection of 819 820 818 and 766 19 Fig ...

Page 7: ...s an overview of all the Metrohm instruments which can be connected to the 830 IC Interface and are described in these Instruc tions for Use It is also possible to connect Bischoff instruments please refer to the IC Net on line program help as well as the relevant Bischoff instruction manuals 830 IC Interface 819 IC Detector 820 IC Separation Center 818 IC Pump 833 IC Liquid Handling Unit 812 IC V...

Page 8: ...ntrols of the 830 IC Interface The numbering applies through out the instructions for use i e bold numbers in the text e g 5 refer to the parts and controls illustrated here 1 Fig 2 Front of 830 IC Interface 1 Mains pilot lamp Lights up when instrument is switched on 830 IC Interface 8 830 1003 Instructions for Use 2 ...

Page 9: ... connection see section 2 2 6 PC connection RS232 interface System 1 7 Analog signal connection 8 Remote input output lines connec tion RUN 9 Remote input output lines connec tion COM 10 RS232 interfaces System 2 11 Analog signal connection 12 Remote input output lines connec tion RUN 13 Remote input output lines connec tion COM 14 RS232 interfaces 830 IC Interface 8 830 1003 Instructions for Use ...

Page 10: ...startup procedure operation and technical specifications of this instrument The Instruc tions for Use are organized as follows Section 1 Introduction General description of instrument parts and con trols and safety notes Section 2 Installation Mains connection connection to PC connection of external instruments Section 3 Operation Operation via IC Net Section 4 Appendix Technical data standard equ...

Page 11: ...ing This symbol indicates a possible risk of death or injury to the user and possible damage to the instrument or its components by electricity Danger Warning This symbol indicates a possible risk of death or injury to the user and possible damage to the instrument or its components Attention This symbol indicates important information that you should read before continuing Information This symbol...

Page 12: ...stru ment must not be opened nor must parts be removed from it other wise there is a danger of coming into contact with components which are live Hence always disconnect the instrument from all voltage sources before you open it and ensure that the mains cable is disconnected from mains connection 5 Protection against static charges Electronic components are sensitive to static charging and can be...

Page 13: ...rived without damage compare with delivery note and list of accessories in section 4 2 In the case of transport damage see instructions in section 4 5 1 Warranty 2 1 3 Location Position the instrument in the laboratory at a location convenient for op eration free from vibrations and protected against a corrosive atmos phere and contamination by chemicals 2 1 4 Arrangement of the instruments The mo...

Page 14: ... Germany 6 2133 070 with plug NEMA 5 15 USA which are three cored and fitted with a plug with an earthing pin If a dif ferent plug has to be fitted the yellow green lead IEC standard must be connected to the earthing socket 2 protection class 1 Any break in the earthing inside or outside the instrument can make it a hazard Plug the mains cable into mains connection plug 5 at the 830 IC Inter face ...

Page 15: ...e is available on the PC then the 6 2125 110 Adapter cable or a commercially available adapter must be used 830 6 2134 100 Fig 4 Connection of 830 IC Interface to PC 2 3 2 Software installation The PC program IC Net 2 3 is required for the operation of the 830 IC Interface this is contained on the 6 6034 033 CD included in the acces sories This program runs under Windows 2000 and Windows XP oper a...

Page 16: ...rnal instruments using the mains switch 2 Connect instruments Connect the instruments to the 830 IC Interface according to the connection diagrams shown in sections 2 4 2 to 2 4 15 by using the cables named in the diagrams Other instrument combinations can be set up by using these examples as a guide 3 Switch on all instruments Switch on 830 IC Interface and all external instruments using the main...

Page 17: ...6 IC Sample Processor RS232 settings handshake SWchar RS232 settings RS control on Triathlon Autosampler This instrument is already pre configured no additional set tings must be made 812 IC Valve Unit This instrument is already pre configured no additional set tings must be made 816 IC Eluent Selector Switch on external control via RS232 interface using the EXT switch 828 IC Dual Suppresso Switch...

Page 18: ...ts corresponds to the Modular IC System 1 MIC 1 Advanced 2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center with 1 injector and column heater 2 818 0110 818 IC Pump 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2134 090 6 2125 090 6 2134 040 Interconncection Fig 5 Connection of 819 820 and 818 MIC 1 830 IC Interface 8 830 1003 Instructions for Use 12...

Page 19: ...C 2 Advanced 2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0230 820 IC Separation Center with 1 injector suppressor module and column heater 2 818 0110 818 IC Pump 2 833 0010 833 IC Liquid Handling Pump Unit 833 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2134 090 6 2125 090 6 2128 180 6 2134 040 Interconnection Fig 6 Connection of 820 819 818 and 833 Pump Unit MIC 2 830 I...

Page 20: ...tor für System 2 anions 2 820 0220 820 IC Separation Center with 2 injectors and column heater 2 818 0110 818 IC Pump for System 1 cations 2 818 0110 818 IC Pumpe for System 2 anions 2 833 0020 833 IC Liquid Handling Suppressor Unit for System 2 anions Interconnection 819 2 819 1 820 818 1 830 PC 6 2134 100 6 2115 070 6 2134 090 6 2125 090 6 2143 200 833 818 2 6 2125 090 6 2115 070 6 2134 090 6 21...

Page 21: ...0220 820 IC Separation Center with 2 injectors and column heater 2 818 0110 818 IC Pump 2 833 0010 833 IC Liquid Handling Pump Unit 2 833 0020 833 IC Liquid Handling Suppressor Unit 2 833 0030 833 IC Liquid Handling Sample Prep Unit Interconnection 830 833 Suppressor 833 Sample Prep 833 Pump 820 818 819 PC 6 2134 100 6 2134 090 6 2134 090 6 2134 130 6 2143 210 6 2115 070 6 2125 120 6 2125 090 6 21...

Page 22: ... IC Separation Center 820 with 2 injectors and column heater 2 818 0110 818 IC Pump 2 833 0020 833 IC Liquid Handling Suppressor Unit 2 833 0040 833 IC Liquid Handling Dialysis Unit Interconnection 833 Dialysis 833 Suppressor 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2134 090 6 2125 090 6 2143 220 6 2134 040 Fig 9 Connection of 819 820 818 833 Suppressor Unit and 833 Dialysis Unit 830 ...

Page 23: ...etector 2 820 0210 820 IC Separation Center 820 with 1 injector and column heater 2 818 0110 818 IC Pump 2 833 0020 833 IC Liquid Handling Suppressor Unit 2 833 0050 833 IC Liquid Handling Ultra Filtration Unit Interconnection 833 Ultra Filtration 833 Suppressor 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2134 090 6 2125 090 6 2143 220 6 2134 040 Fig 10 Connection of 819 820 818 833 Supp...

Page 24: ... 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center 820 with 1 injector and column heater 2 818 0110 818 IC Pump 2 135 0100 Triathlon Autosampler Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2134 090 6 2125 090 Triathlon 6 2134 000 6 2134 040 Fig 11 Connection of 819 820 818 and Triathlon 830 IC Interface 8 830 1003 Instructions for Use 18 ...

Page 25: ...nts 2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center 820 with 1 injector and column heater 2 818 0110 818 IC Pump 2 766 0010 766 IC Sample Processor Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2125 090 6 2141 110 766 6 2134 080 6 2134 090 6 2134 040 Fig 12 Connection of 819 820 818 and 766 830 IC Interface 8 830 1003 Instructions ...

Page 26: ...nstruments 2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center with 1 injector and column heater 2 818 0110 818 IC Pump 2 791 0020 791 IC VA Detector Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2125 090 6 2134 090 6 2128 130 791 6 2134 040 Fig 13 Connection of 819 820 818 and 791 830 IC Interface 8 830 1003 Instructions for Use 20 ...

Page 27: ...2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center with 1 injector and column heater 2 818 0110 818 IC Pump 2 761 0020 761 Compact IC with suppressor module Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2125 090 6 2134 090 761 6 2134 100 6 2134 040 Fig 14 Connection of 819 820 818 and 761 830 IC Interface 8 830 1003 Instructions for U...

Page 28: ...ced enhanced by the 830 IC Interface 2 830 0020 830 IC Interface 2 817 0010 817 Bioscan 2 812 0010 812 IC Valve Unit 812 with 1 valve 2 818 0110 818 IC Pump Interconnection 818 830 PC 6 2134 100 6 2134 090 812 817 6 2128 100 1 2 3 4 5 6 7 8 9 Ground Fill Inject AUX 1 AUX 2 1 2 Adapter 6 2125 150 Fig 15 Connection of 817 812 and 818 MIC 8 830 IC Interface 8 830 1003 Instructions for Use 22 ...

Page 29: ... Interface 2 819 0110 819 IC Detector 2 820 0230 820 IC Separation Center with 1 injector suppressor module and column heater 2 818 0110 818 IC Pump 2 816 0010 816 IC Eluent Selector Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2125 090 6 2134 090 816 6 2134 080 6 2134 040 Fig 16 Connection to 819 820 818 and 816 830 IC Interface 8 830 1003 Instructions for Use 23 ...

Page 30: ...anced 2 830 0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0210 820 IC Separation Center with 1 injector suppressor module and column heater 2 818 0110 818 IC Pump 2 devices 2 828 0010 828 IC Dual Suppressor 820 818 819 6 2134 090 6 2134 130 6 2125 090 6 2115 070 830 6 2134 100 818 6 2134 080 828 6 2128 180 PC 6 2134 040 Interconnection Fig 17 Connection to 819 820 2x818 and 828 MIC 10 830...

Page 31: ...0020 830 IC Interface 2 819 0110 819 IC Detector 2 820 0230 820 IC Separation Center with 1 injector and suppressor module and column heater 2 818 0010 818 IC Pump 2 837 0030 837 IC Combi Degasser Interconnection 819 820 818 830 PC 6 2134 100 6 2134 130 6 2115 070 6 2125 090 6 2134 090 837 6 2128 180 6 2134 040 Fig 18 Connection to 819 820 818 and 837 830 IC Interface 8 830 1003 Instructions for U...

Page 32: ...0 IC Interface is switched on and off using mains switch 3 on the rear of the instrument see Fig 3 After the instrument has been switched on a self test is running The mains pilot lamp 1 flashes twice slowly and remains on to show that the instrument is ready for use if an error ocurrs the mains pilot lamp 1 starts flashing fast If the mains pilot lamp is flashing fast after the instrument is swit...

Page 33: ... Links Init The Init tab of the 830 IC Interface window contains data acquisition pa rameters for the 830 IC Interface Label Optional label to name the interface with maximum 8 characters ROM version Instrument program version number Measuring per second Number of data points measured per s Entry range 10 20 30 50 60 points s Range Range for AD converter Example converts 2500 mV to 224 bits Entry ...

Page 34: ...ted Protocol be tween 830 IC Interface and PC select this option if there is a problem with the RS communication using the Protected Protocol Baud Rate Display of the baud rate of the device Parity Display of the parity check Handshake Display of the software handshake mode FIFO size Display of the intermediate memory in byte The values are displayed correctly only if the 830 IC Interface is con n...

Page 35: ...COM If this entry is clicked with the right mouse but ton the following menu appears Put on desktop Possibility for setting RS232 interface parame ters details see on line help Change Possibility for changing the RS232 interface The following window is opened where the COM port can be changed by clicking on the desired entry 830 IC Interface 8 830 1003 Instructions for Use 29 ...

Page 36: ...sists of the tabs Program and Events setup Time program On the Program tab of the 830 System window a user defined time program for the event output lines of the 830 IC Interface can be en tered This program is started automatically as defined in the Start mode window either at the moment the determination is started Start with de termination or at the moment the sample is injected Start with inje...

Page 37: ...not started Add Add new program instruction Delete Delete selected program instruction Verify Test the time program error messages are dis played if program is wrong List of program instructions The following program instructions can be added to the time program on the Program subpage Instruc tion Entry Meaning Events 0 1 p Set event output lines 1 7 to the desired values For entry of the first va...

Page 38: ...ting the event output lines 1 7 Selection 0 line off inactive open 1 line on active 0 V p pulse pulse length 150 ms leave line in current status For entry of the first value enter 1 0 p or For entry of the other values move the cursor in front of the value to be changed and enter 1 0 p or Add Add new remote command Delete Delete selected remote command Activate Activate the defined remote commands...

Page 39: ...nes of system 1 or system 2 of the 830 IC Interface These startup values are sent each time the system is connected or a determination is started Each event output line can be set to the following values 0 Line off inactive open 1 Line on active 0 V For technical data to the event output lines see section 4 1 830 IC Interface 8 830 1003 Instructions for Use 33 ...

Page 40: ...TH to be replaced by Metrohm Service only using the same type Additional electronic overload protection PC interface RS232 Connector Dsub connector 9 pin male 1 5 9 6 Baud rate 1 200 115 200 Data bits 8 Stop bits 1 Handshake Xon Xoff none Parity none even odd FIFO 0 16 Bytes Pin assignment Pin 1 4 6 internally connected Pin 2 RxD Received Data Pin 3 TxD Transmitted Data Pin 5 GND Signal Ground Pin...

Page 41: ...n 5 GND Signal Ground for Dev 1 4 Pin 7 TxD Transmitted Data for Dev 5 8 Pin 8 RxD Received Data for Dev 5 8 Pin 9 GND Signal Ground for Dev 5 8 Remote interface Events Output lines 7 potential free relay contacts per system for controlling external instruments RUN COM Maximum contact load 30 V 1 A DC Input lines 1 digital input per system for external method start 5V 470k 47k Ext Start RUN COM Ma...

Page 42: ...2 Analog 1 Pin 3 Analog 1 Pin 6 Analog 2 Pin 7 Analog 2 Safety specifications Construction testing according to EN IEC 61010 1 UL 3101 1 protection class 1 degree of protection IP40 Safety directions The Instructions for Use include information and warnings which must be heeded by the user to assure safe operation of the instrument Electromagnetic compatibility EMC Emitted interference Standards m...

Page 43: ...y Storage transport 20 70 C Housing Material of cover Polyurethane rigid foam PUR with fire protection for fire class UL94VO CFC free Material of base Steel enameled Dimensions Width 260 mm Height 130 mm Depth 340 mm Weight with accessories 4 8 kg 830 IC Interface 8 830 1003 Instructions for Use 37 ...

Page 44: ...ble 830 IC Interface PC 1 6 6034 033 Software CD IC Net 2 3 1 6 2122 0X0 Mains cable according to customer s specification Cable socket Cable plug Type IEC 320 C 13 Type SEV 12 CH 6 2122 020 Type IEC 320 C 13 Type CEE 7 VII D 6 2122 040 Type CEE 22 V Type NEMA 5 15 USA 6 2122 070 1 8 830 1003 Instructions for Use english for 830 IC Interface 1 8 110 8283 Instructions for Use IC Net english for PC ...

Page 45: ...t channel 1 2 or 3 4 6 2128 180 Remote connection cable Connection cable 830 IC Interface 833 6 2134 000 RS232 connection cable Connection cable 830 IC Interface Triathlon Autosampler 6 2134 080 RS232 connection cable Connection cable 830 IC Interface 1 external device 818 819 766 etc 6 2141 110 Connection cable Connection cable 830 IC Interface 819 IC Detector 766 788 IC Sample Processor accessor...

Page 46: ...idating your 830 IC Interface It can also provide you with validation documentation which will help you to carry out your installation qualifi cation IQ and operational qualification OQ Further information about QA GLP and validation can also be found in the brochure Quality management with Metrohm which is also ob tainable from your local Metrohm agency Checking the electronic and mechanical asse...

Page 47: ...r has no rights or claims ex cept those mentioned above If damage of the packaging is evident on receipt of a consignment or if the goods show signs of transport damage after unpacking the carrier must be informed immediately and a written damage report demanded lack of an official damage report releases Metrohm from any liability to pay compensation If any instruments and parts have to be returne...

Page 48: ... IEC 61000 4 8 EN IEC 61000 4 11 EN IEC 61000 4 14 NAMUR Safety specifications EN IEC 61010 1 UL 3101 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Body CB IEC The instrument meets the requirements of the CE mark as contained in the EU directives 89 336 EEC and 73 23 EEC and fulfils the following specifications EN 61326 Electric...

Page 49: ...f instrument develop ment Software development Software development occurs in terms of the software life cycle Tests are performed to detect programming errors and to assess the program s functional ity in a laboratory environment Components All components used in the Metrohm instruments have to satisfy the quality standards that are defined and imple mented for our products Suppliers of component...

Page 50: ... 8213 39 818 IC Pump Compliance White Paper IC Cap 1 0 8 110 8303 38 Connection to 830 12 IC Net 2 3 8 110 8193 38 IC Cap 1 0 8 110 8309 38 Settings 10 IC Net 2 3 8 110 8193 38 Connection possibilities 1 819 IC Detector Instrument Connections Connection to 830 12 Description 1 Figure 3 Settings 10 Switch on off 26 Technical Data 34 ff 820 IC Separation Center to external instruments 10 Introductio...

Page 51: ...on card 8 110 8207 39 Remote connection 12 Figure 3 13 Figure 3 8 Figure 3 Technical Data 35 9 Figure 3 Remote connection 12 Technical Data 35 Remote connection 13 Technical Data 35 Remote connection 9 Technical Data 35 Remote input lines 35 Remote output lines 30 35 RESET 31 ROM version 27 RS settings 28 RS232 interface 10 Figure 3 Technical Data 35 RS232 interface 14 Figure 3 Technical Data 35 R...

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