Lauda Puridest PD 2 D Operating Instructions Manual Download Page 7

09/2020

Puridest Bi Distillation Apparatus

7 / 32

1

Using of the Bi Distillation Apparatus

Intended Use

1.1

In LAUDA Puridest Bi Distillation Apparatus models PD 2 D, PD 4 D and PD 8 D, electric heating elements serve to boil
water in the mono stage boiler (left-hand side) and evaporate it. The steam is led to the steel condenser of the mono stage
where it condenses on a water-cooled cooling coil. The produced distillate drips into the boiler of the bi stage (right-hand
side), or can be withdrawn through a stop cock made of borosilicate glass. The electric heating elements in the bi stage
bring the water in the right-hand side alembic to the boil. The steam is led into the condenser of the second distillation
stage and condenses as bi distillate on a water-cooled cooling coil. The condenser of the bi stage, including the splash
protection and cooling coil as well as the complete bi distillate outlet with dust cover are made of Duran® / borosilicate
glass 3.3.
The filling level of both boilers is monitored by two float switches, the heating elements of both stages are additionally
controlled by thermostatic low water cut-offs. After switching the Double Distiller on, it is automatically operated.
Depending on the model, the Double Distiller produces approx. 2 litres (PD 2 D), 4 litres (PD 4 D) or 8 litres (PD 8 D)
bi distillate per hour.
Mono- and Bi-distillate is withdrawn through the two glass fittings at the front of the unit. Attention, the distilled water
leaves the Distillation Apparatus with more than 90 °C! Danger of scaldings! Depending on the tap water quality, the
produced mono distillate has a conductivity of approx. 2.2  µS/cm at 25°C. The  produced  bi  distillate  is dependent  on
the quality of the evaporated mono distillate and has a conductivity of approx. 1.6 µS/cm at 25°C. To feed the Distillation
Apparatus, preferably use tap water of drinking quality. Please also observe the information in chapters 17.2 to 17.4 of
these instructions on the possible use of filters and cartridges to pretreat the tap water .

 The Bi Distillation Apparatus must be operated within the user's field of vision.

The information contained in these operating instructions must by all means be read and observed. Only
then a perfect operation of the Bi Distillation Apparatus can be guaranteed. The units may only be installed
and operated by persons who have made themselves familiar with these operating instructions.

Caution:
The accessible inner parts of the housing that can be reached after removing the outer white cover get
strongly heated up during operation. These parts may only be touched after they have cooled down, or
when wearing suitable safety gloves.

Improper Use

1.2

LAUDA Puridest Bi Distillation Apparatus, operated in a laboratory, are no Medical Devices. They fall neither under na-
tional nor international Medical Device Directives and have to be used and applied accordingly. The Distillation Apparatus
must not be used in potentially explosive surroundings. The Distillation Apparatus must neither be set up nor operated in
laboratory areas with aggressive or corrosive ambient conditions.

Summary of Contents for Puridest PD 2 D

Page 1: ...Operating Instructions Puridest Bi Distillation Apparatus PD 2 D PD 4 D PD 8 D...

Page 2: ...2 32 Puridest Bi Distillation Apparatus 09 2020...

Page 3: ...in switch II Pilot lamp Operation Mono stage III Pilot lamp Low water Mono stage IV Pilot lamp Clean V Pilot lamp Operation Bi stage VI Pilot lamp Low water Bi stage Before installation please check w...

Page 4: ...4 32 Puridest Bi Distillation Apparatus 09 2020...

Page 5: ...water supply 10 7 3 Cooling water outlet 11 7 4 Drain Bi stage boiler 11 7 5 Drain Mono stage boiler 11 7 6 8 Initiation 11 9 Functional Description 12 Distillation Apparatus for double distillation 1...

Page 6: ...the mains supply examples 22 14 1 14 1 1 PD 2 D for 230 V 22 14 1 2 PD 4 D and PD 8 D for 220 V 3 at Mains supply 230 V 3 PE 50 60 Hz 23 14 1 3 PD 4 D and PD 8 D for 220 V 3 at Mains supply 230 V 3 PE...

Page 7: ...led water leaves the Distillation Apparatus with more than 90 C Danger of scaldings Depending on the tap water quality the produced mono distillate has a conductivity of approx 2 2 S cm at 25 C The pr...

Page 8: ...Distillation Apparatus PD 2 D net weight 20 4 kg PD 4 D net weight 27 5 kg and PD 8 D net weight 43 0 kg must be lifted carried and transported to the location by at least two persons The Distillation...

Page 9: ...d back onto the unit and secure with the two screws and four quick release catches Then install the glass fittings Screw together the glass valve with the mono distillate outlet left hand front of the...

Page 10: ...n accessory Only fitted if a separate water supply was ordered The water inlet for the separate water supply feeds pretreated water to the boiler of the Distillation Appa ratus through a solenoid valv...

Page 11: ...ing or maintenance can be connected Caution The water leaves the boiler of the Distillation Apparatus with temperatures of up to 100 C Danger of scaldings Water connections pos and are parts of an acc...

Page 12: ...valve for withdrawal of mono distillate is closed the mono distilled water is led into the boiler of the bi stage Once the heating elements in the bi stage are below water level the heating elements...

Page 13: ...tage boiler and rinse the boiler with clear water several times Commercial descaling agents suitable for use with stainless steel can also be used according to the manufacturer s in structions e g rea...

Page 14: ...f the water in the boiler caused by the distillation process in the mono stage boiler foam will form during evaporation of water Once the foam gets in contact with the electrode in the mono stage boil...

Page 15: ...ee of charge and will have it materially recycled Before the unit is returned a legally binding declaration must be provided from the sender confirm ing that the unit is free from harmful and or hazar...

Page 16: ...C 15 K Electromechanical temperature limiter with capillary tube sensor Switch off temperature 135 C 15 K Water pressure min max 3 bar 7 bar 43 5 psi 101 5 psi 3 bar 7 bar 43 5 psi 101 5 psi Electrica...

Page 17: ...ctromechanical temperature limiter with capillary tube sensor Switch off temperature 135 C 15 K Water pressure min max 3 bar 7 bar 43 5 psi 101 5 psi Electrical connection Mains supply On site fuse 22...

Page 18: ...amp Clean LED 6 V DC H2 Pilot lamp Low Water mono stage LED 230 V AC H3 Pilot lamp Operation mono stage LED 230 V AC H4 Pilot lamp Low Water bi stage LED 230 V AC H5 Pilot lamp Operation bi stage LED...

Page 19: ...09 2020 Puridest Bi Distillation Apparatus 19 32 PD 4 D version 220 V 3 13 2 PD 4 D version 400 V 3 13 3...

Page 20: ...20 32 Puridest Bi Distillation Apparatus 09 2020 PD 8 D version 220 V 3 13 4 PD 8 D version 400 V 3 13 5...

Page 21: ...PD 4 D PD 8 D Mains supply 220 V 3 N PE 50 60 Hz Model PD 4 D PD 8 D Mains supply 400 V 3 N PE 50 60 Hz ge gr yellow green PE Protective earth PE Protective earth PE Protective earth bl blue N N sw b...

Page 22: ...on site B2 CEE plug not assembled according to IEC standard 60309 2 F1 Mains fuse on site by customers F2 Mains fuse on site by customers F3 Mains fuse on site by customers S1 Main switch on site by c...

Page 23: ...plate PD 4 D and PD 8 D Mains connection through on site switch S4 all pole separa tion from the mains possible 14 1 3 PD 4 D and PD 8 D for 220 V 3 at Mains supply 230 V 3 PE 50 60 Hz see nameplate P...

Page 24: ...plate PD 4 D and PD 8 D Mains connection through on site switch S4 all pole sepa ration from the mains possible 14 1 5 PD 4 D and PD 8 D for 400 V 3 at Mains supply 400 V 3 N PE 50 60Hz see nameplate...

Page 25: ...09 2020 Puridest Bi Distillation Apparatus 25 32 15 List of spare parts When ordering spare parts please always state type and serial number of the unit in question...

Page 26: ...15101 Hose connector 0015115 Hose connector 10 A000115 Hose tap 11 A000084 Heating element Mono stage 2 0k W PD 2 D 1 pce PD 4 D 2 pcs and PD 8 D 3 pcs 12 0014516 Lock for housing 13 0012308 Connectio...

Page 27: ...Apparatus without illustration Separate Water Supply with solenoid valve Only factory installation into models PD 2 D to PD 8 D is possible When the storage tank is full the solenoid valve switches o...

Page 28: ...filter and fillings mounted completely Part No A000136 Part No A000135 Hose Set consisting of hoses for water inlet and outlet length 1 5 m including hose clips Hose Set Hose Set for seperate water s...

Page 29: ...09 2020 Puridest Bi Distillation Apparatus 29 32...

Page 30: ...30 32 Puridest Bi Distillation Apparatus 09 2020...

Page 31: ...09 2020 Puridest Bi Distillation Apparatus 31 32...

Page 32: ...LAUDA GFL Gesellschaft f r Labortechnik mbH Schulze Delitzsch Stra e 4 5 30938 Burgwedel Deutschland Tel 49 0 5139 9958 0 Fax 49 0 5139 9958 21 E Mail info lauda gfl de Internet www GFL de...

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