Knick Protos 3400 User Manual Download Page 132

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132

ORP Calbration/Adjustment

The potential of a redox electrode is calibrated using a redox (ORP) buffer solu-

tion. In the course of that, the difference between the measured potential and

the potential of the calibration solution is determined. This potential difference

is printed on the calibration solution bottle and is defined as the voltage across

the redox electrode and a reference electrode.

Examples:

220 mV

Pt against Ag/AgCl, KCl 3 mol/l

427 mV

Pt against SHE

During measurement this difference is added to the measured potential.

ORP

= mV

meas +

∆

ORP

= displayed oxidation-reduction potential (measured ORP)

meas

= direct electrode potential (ORP input, see Sensor monitor)

∆mV

= delta value, determined during calibration

ORP related to the standard hydrogen electrode (SHE)

The oxidation-reduction potential can also be calibrated automatically with

respect to the standard hydrogen electrode (SHE). To do so, you must first

select the reference electrode used (see Parameter setting).

The temperature behavior of the reference electrode is automatically taken into

account.

You can choose from the following types of reference electrodes:

Ag/AgCl, KCl 1 mol/l

(silver/silver chloride)

Ag/AgCl, KCl 3 mol/l

(silver/silver chloride)

Hg, Tl/TlCl, KCl 3.3 mol/l

(Thalamid)

Hg/Hg

, K

saturated

(mercury sulfate)

Calibration / Adjustment

ORP calbration/adjustment

ORP calibration

Summary of Contents for Protos 3400

Page 1: ...ing Aktuelle Produktinformation www knick de Analysenmesssystem Protos 3400 X Betriebsanleitung Messmodul Protos CONDI 3400 X 051 zur Leitfähigkeitsmessung mit induktiven Sensoren Deutsch The Art of Measuring Aktuelle Produktinformation www knick de Analysenmesssystem Protos 3400 X Betriebsanleitung Messmodul Protos CONDI 3400 X 051 zur Leitfähigkeitsmessung mit induktiven Sensoren Deutsch User Ma...

Page 2: ...ice Return of products under warranty Please contact our Service Team before returning a defective device Ship the cleaned device to the address you have been given If the device has been in contact with process fluids it must be decontaminated disinfected before shipment In that case please attach a corresponding certificate for the health and safety of our service personnel Disposal Please obser...

Page 3: ...le 14 Short Description Menu Structure 15 Short Description BASE Module 17 Overview of the System Components 18 PHU 3400 X 110 Module 20 Terminal Plate PHU 3400 X 110 Module 21 Inserting the Module 22 Wiring Example VP and SixPlug 23 Connecting the Probe Controller 25 Menu Selection 26 Menu Structure 26 Passcode Entry 27 Changing a passcode 27 Configuring the Measurement Display 28 Start Up 30 Par...

Page 4: ...ogbook Factory Setting 53 Configuring a Current Output 54 Current Outputs Characteristics 55 Output Filter 57 NAMUR Signals Current Outputs 58 NAMUR Signals Relay Contacts 59 Relay Contacts Protective Wiring 60 Relay Contacts Usage 61 Relay Contacts Sensoface Messages 62 Rinse Contact 63 Limit Value Hysteresis Contact Type 64 Icons in the Measurement Display 64 OK1 OK2 Inputs Specify Level 65 Sele...

Page 5: ...r Setting Installation 81 Selecting the Measurement Procedure 82 External Control via DCS 82 Control via Process Control Cystem DCS 83 Control Programs and Meas Procedures 84 Sensor Detection 85 Probe 85 Configuring Media Monitoring 86 Media Adapter 87 Additional Media 2 87 Start Up 87 System Forecast Ceramat SensoGate 88 Reference Probe Travel Profiles 89 Creation of a Probe Travel Profile and Pr...

Page 6: ...ernal Control via DCS 109 Control via Process Control System DCS 110 Control Programs and Meas Procedures 111 Sensor Detection 112 Probe 112 Media Adapter 113 Additional Media 2 113 Start Up 113 Calibration Adjustment 114 Calibration Methods 116 One Point Calibration 116 Two Point Calibration 116 Three Point Calibration 116 Sensor Replacement First Calibration 116 Temperature Compensation 117 Auto...

Page 7: ...nance via Protos 3400 X 137 Diagnostics Functions 141 Point of Meas Description 141 Logbook 141 Device Description 142 Diagnostics of PHU 3400 X 110 143 Module Diagnostics 143 Sensor Monitor 143 Calibration Timer 144 Tolerance Adjustment 144 Cal Record 145 Sensor Network Diagram 145 Statistics 145 Diagnostics of Unical 9000 X 146 Unical Status 146 Unical Network Diagram 146 Diagnostics of Uniclean...

Page 8: ...t 178 Buffer Table DIN 19267 179 Buffer Table NIST Standard DIN 19266 2000 01 180 Buffer Table Techn Buffers to NIST 181 Buffer Table Hamilton 182 Buffer Table Kraft 183 Buffer Table Hamilton A 184 Buffer Table Hamilton B 185 Buffer Table HACH 186 Buffer Table Ciba 187 Buffer Table Reagecon 188 SW 3400 002 Specifiable Buffer Sets 189 Overview of Parameter Setting 190 Index 196 Menu Selection 210 Q...

Page 9: ... Passcodes This prevents unauthorized modification of device settings or manipulation of the measurement results Appropriate use of these passcodes makes them suitable as electronic signature Audit Trail Log Every change of device settings can be automatically recorded and docu mented in the Audit Trail Log on the SmartMedia card The recording can be encrypted Conformity with FDA 21 CFR Part 11 Th...

Page 10: ...rdous location observe the specifica tions of the EC Type Examination Certificate and if applicable of the Control Drawing download www knick de Before commissioning you must prove that the device may be connected with other equipment such as a supply unit including cables and wires In hazardous locations the device shall only be cleaned with a damp cloth to prevent electrostatic charging Devices ...

Page 11: ...erent modules FRONT BASE slots 1 3 using the arrow keys Device description Return 22 7 C 7 00 pH Operating panel Protos Module FRONT 3400 011 Hardware 1 1 Software A 2 Serial number 08150815 BASE Module FRONT Query actual device module software When the analyzer is in measuring mode Press menu key open Diagnostics menu Device description Options Device description Return 22 7 C 7 00 pH Input for p...

Page 12: ...12 ...

Page 13: ...tional functions options Additional functions must be ordered separately They are supplied with a device specific TAN for function release 3 module slots for free combination of measuring and communication modules Measuring modules pH ORP Temp O2 Temp Noncontacting conductivity Temp Contacting conductivity Temp Memosens sensors Additional functions Activation via device specific TAN SmartMedia car...

Page 14: ... properly seated and clean Green LED Voltage supply okay 5 self sealing cable glands M20 x 1 5 for entry of voltage supply and signal lines 2 softkeys with context sensitive functions User interface with plaintext menus as recom mended by NAMUR Menu texts can be switched to German English French Italian Swedish Portuguese or Spanish Intuitively acquirable menu logic based on Windows standards Cont...

Page 15: ...ASE Module 1 Module 2 Module 3 SYSTEM FRONT BASE Module 1 Module 2 Module 3 Message list Point of meas description Logbook Device description FRONT BASE Module 1 Module 2 Module 3 4 5 6 Legend 1 Pressing the menu key accesses menu selection 2 Pressing the meas key returns to measurement 3 Menu groups are selected using the arrow keys 4 Press enter to confirm enter passcode 5 Further menu items are...

Page 16: ...cords Exchange of parameter sets 5 parameter sets can be stored on the SmartMedia card 2 of them can be loaded simultaneously to the analyzer and be switched by remote control Parameter sets can be transmitted from one analyzer to the other Function expansions are possible with additional software modules which are released using transaction numbers TAN Software updates The circumferential sealing...

Page 17: ...otice concerning SmartMedia Card The SmartMedia card may be inserted or replaced with the power supply switched on Before a memory card is removed it must be closed in the main tenance menu When closing the device make sure that the sealing is properly seated and clean Module equipment Module identification Plug Play Up to 3 modules can be combined as desired Several input and communication module...

Page 18: ...s The system is operated from the Protos 3400 X Four operating modes are provided calibration parameter setting maintenance diagnostics The PHU 3400 X 110 module consists of 2 functional groups PHU 3400 X 110 measuring circuit Unical 9000 X Uniclean 900 X probe control pH 25 6 C 09 03 07 Protos 3400 X e g Unical 9000 X Service switch Max 10 m Max 10 m To probe pH temp max 20 m Power supply Compres...

Page 19: ... OK 2 Contacts K1 K2 K3 Alarm K4 I 2 mA I 1 VariPower 0 4 20 mA pH Temp Module slot Module slot mA 0 4 20 mA Unical 9000 X or Uniclean 900 X Probe RTD Unical pH ORP MΩ kΩ Interface PHU 3400 X 110 module Temp Protos 3400 X basic unit The PHU 3400 X 110 module is located in one of the 3 module slots available PHU 3400 X 110 controller module for retractable fittings and Unical 9000 X Uniclean 900 X ...

Page 20: ...with Protos 3400 X or as download at www knick de Measuring Circuit and Probe Control Function Blocks Probe Controller The PHU 3400 X 110 module allows connection of the Unical 9000 X probe controller for fully automated pH measurement cleaning and calibration or the Uniclean 900 X probe controller for fully automated pH measurement Measuring Circuit Even without the Unical 9000 X Uniclean 900 X t...

Page 21: ...te PHU 3400 X 110 Module Attaching the Terminal Plates The terminal plates of the lower modules can be sticked to the inner side of the door This facilitates maintenance and service Terminal Plate PHU 3400 110 Module ...

Page 22: ...ble To avoid interferences the cable shielding must be completely covered by the ESD shielding cap Close ESD shielding cap covering terminals 2 and 8 Connect RS 485 interface to probe controller terminals 16 19 Close device tighten screws at the front Switch on power supply Set parameters Make sure that the cable glands are tightly closed to protect against humidity The terminals 2 and 8 are cover...

Page 23: ...23 Wiring Example 1 Wiring Example VP and SixPlug Multisense electrode pH ORP temp with solution ground SG Core Shield Green White Blue PHU 3400 110 GN YE UNICAL 9000 X Green Yellow Brown White ...

Page 24: ...24 Wiring Example 2 Wiring Example VP and SixPlug Electrode pH temp without solution ground SG Jumper Green White PHU 3400 110 Core Shield GN YE UNICAL 9000 X Green Yellow Brown White ...

Page 25: ...A RS 485 B GND Power Green Yellow Brown White Connecting the Probe Controller Probe Controller for Fully Automated Measurement Cleaning and Calibration Unical 9000 X Uniclean 900 X Controller The Unical 9000 X Uniclean 900 X probe controllers come with installation manuals free download at www knick de 16 17 18 19 ...

Page 26: ...mode Measuring Menu Structure Calibration Maintenance Parameter setting Diagnostics Menu groups Select using arrow keys 1 2 3 1147 2958 1246 Operator level 1989 Administrator level Passcode as delivered Selection of further menu items 8 06 pH 25 1 C 1 Pressing menu accesses menu selection 2 Pressing meas returns to measurement 3 Arrow keys for selecting a menu group 4 enter key for confirming a se...

Page 27: ...nge a passcode Open the menu selection menu Select parameter setting Administrator level enter passcode Select System control Passcode entry Passcode Entry Menu Display System control Passcode entry Passcode entry Administrator OK 25 6 C 7 00 pH Passcode entry Administrator 25 6 C 7 00 pH cal Calibration On Off maint Maintenance On Off Change passcode opl Operator level 1147 On Off Close cal Calib...

Page 28: ... the modules can be displayed The table on the next page describes how to configure the measurement display Secondary displays Additional values also date and time can be displayed depending on the modules installed Measurement display Typical measurement display Softkeys In measuring mode the softkeys allow selection of values for the secondary displays or control of functions user defined 1 pH 2...

Page 29: ...surement press meas Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Parameter setting Administrator System control Return 25 6 C Module BASE 3400 021 7 00 pH Module PH 3400 035 Module FRONT 3400 011 Administrator Languages Return 25 6 C Measurement recorder 7 00 pH English Measurement display Module FRONT 3400 011 65 C 7 00 pH 1 primary value 1st primary value Viewing angle 2 prim...

Page 30: ...iclean 900 X Ceramat WA 150 X or other retractable fittings Warning Before working on the retractable fitting it must be moved into SERVICE position Be sure to read and observe the user manual of the retractable fitting Caution Be sure to execute the following steps in the specified order 1 Insert the PHU 3400 X 110 module see Page 22 2 Connect sensor cable and probe controller see Pages 23 25 3 C...

Page 31: ...ock symbol The functions are released or blocked using the softkey Operator level Access to all functions which have been released at the Administrator level Blocked functions are displayed in gray and cannot be edited Fig Viewing level Display of all settings No editing possible Menu selection Return to meas 25 6 C 11 03 pH Select enter Lingua Parameter setting Return 25 6 C 11 03 pH Viewing leve...

Page 32: ...ftkey function changes to Release Open parameter setting Select Operator level passcode 1246 Select Module PHU for example Now the locked function is displayed in gray and marked with the lock icon Module PHU 3400 110 Administrator 25 0 C Return Sensor data Cal preset values 11 03 pH ORP rH value Delta function TC process medium Input filter Block Parameter setting Administrator 25 0 C Return Modu...

Page 33: ...as 25 0 C Select enter Lingua 11 03 pH Parameter setting Administrator 25 0 C Return Module PHU 3400 110 Module FRONT 3400 011 Module BASE 3400 021 11 03 pH System control Module PH 3400 035 Module PHU 3400 110 Administrator 25 0 C Return TC process medium Sensor data Cal preset values 11 03 pH ORP rH value Delta function Input filter Block During parameter setting the analyzer is in HOLD mode Cur...

Page 34: ...th Individual selected Off failure maintenance request Auto Individual Off failure maintenance request Calcheck checks the difference between calibration buffers and measured values Auto Individual Off failure maintenance request Parameter Default Selection Range Notes Off On suppression of fast transients at the input Input filter Pulse suppression Off Sensor data Sensor type Temperature detectio...

Page 35: ...s cannot be edited Sensoface provides information on the sensor condition evaluating the sensor data Great deviations are signaled Sensocheck can be switched off The following parameters are monitored Slope zero reference impedance for ISFET sensors glass impedance pH electrodes response time CalCheck The tolerance limits are displayed in gray Limit violations can be signaled by a message either f...

Page 36: ...function and confirm with enter Menu selection Return to meas Select enter Lingua 7 00 pH 25 6 C 25 6 C Return 7 00 pH Parameter setting Administrator System control Module FRONT 3400 011 Module BASE 3400 021 Module PHU 3400 110 25 6 C Abort 7 00 pH Sensocheck Ref el Administrator Nominal Min Max Message 005 0 kOhm 003 1 kOhm 100 0 kOhm Maint request Off Failure pH pH 24 3 C Sensocheck Automatic m...

Page 37: ...arameters in a graphic diagram Sensor network diagram Return 24 1 C 7 00 pH 2 Zero point 1 Slope 4 Glass impedance 3 Ref impedance 5 Response time 7 Calcheck 6 Cal timer Info Parameter Slope Zero Reference impedance Glass impedance Response time Fine Standard Coarse Calibration timer Calcheck Sensoface Criteria Standard 59 2 7 00 Rcal Rcal Critical range 53 3 or 61 6 00 or 8 00 0 6 Rcal or 100 kΩ ...

Page 38: ...ic buffer Knick 2 00 4 01 7 00 9 21 Merck Riedel 2 00 4 00 7 00 9 00 12 00 DIN 19267 1 09 4 65 6 79 9 23 12 75 NIST standard 4 006 6 865 9 180 NIST technical 1 68 4 00 7 00 10 01 12 46 Hamilton 2 00 4 01 7 00 10 01 12 00 Kraft 2 00 4 00 7 00 9 00 11 00 Hamilton A 2 00 4 01 7 00 9 00 11 00 Hamilton B 2 00 4 01 6 00 9 00 11 00 Hach 4 01 7 00 10 00 Ciba 2 06 4 00 7 00 10 00 Reagecon 2 00 4 00 7 00 9 ...

Page 39: ...justment Yes No First Calibration Yes Erase tolerance band New entry Zero Slope T band check No Yes Zero Tolerance Yes Slope Tolerance Yes Calibration Old tolerance band Adjustment New tolerance band Manual check No No No Start tolerance band End of tolerance band ...

Page 40: ...r 006 Current characteristic 005 Cal tolerance band Inactive Inactive Inactive Active Inactive Menu selection Open parameter setting From the measuring mode Press menu key to select menu Select parameter setting using arrow keys confirm with enter Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Parameter setting Administrator System control Return 25 6 C Module BASE 3400 021 Modul...

Page 41: ...on when the electrode is exposed to high stress temperature extreme pH values Module PHU 3400 110 Administrator 20 1 C Return TC process medium Sensor data Cal preset values 7 00 pH ORP rH value Delta function Input filter Block Cal preset values Administrator 20 1 C Abort Calibration timer Knick 2 00 4 01 Calimatic buffer 7 00 pH Cal tolerance band Drift check Knick DIN 19267 NIST standard NIST t...

Page 42: ...Yes Calculate rH with factor No entry of factor Delta function Off pH mV ORP or rH entry of delta value Parameter Setting of PHU 3400 X 110 TC process medium ORP rH value delta function Default settings and selection range Temperature compensation of process medium Linear temperature compensation reference temp fixed at 25 C pH 25 C pHM TC 100 25 C TM pH 25 C pH value compensated to 25 C pHM Measu...

Page 43: ...ures 0 C or 95 C the last table value is used for calculation If the delta function has been acti vated see Pg 42 simultaneously with temperature compensation the temperature is compensated first and then the delta value is subtracted When the TC correction for process medium is switched on TC appears in the display in measuring mode Module PHU 3400 110 Administrator 24 0 C Return TC process mediu...

Page 44: ...s the difference Output value measured value delta value The output value controls all outputs and is shown on the display When the delta function has been activated simultaneously with temperature compensation the temperature is compensated first and then the delta value is subtracted When delta function is switched on appears in the display in measuring mode ORP rH value Administrator 20 1 C Abo...

Page 45: ...Warning Limit LO Warning Limit HI Failure Limit HI rH value Off device limits max Variable limits Failure Limit LO Warning Limit LO Warning Limit HI Failure Limit HI Temperature Off device limits max Variable limits Failure Limit LO Warning Limit LO Warning Limit HI Failure Limit HI mV value Off device limits max Variable limits Failure Limit LO Warning Limit LO Warning Limit HI Failure Limit HI V...

Page 46: ...H Messages pH value Administrator 25 6 C Abort Monitoring 7 00 pH Variable limits OK Device limits max Off Messages Temperature Messages ORP value Messages pH value Messages mV value Messages rH value Messages Administrator 25 6 C 7 00 pH Warning Limit Hi Monitoring Failure Limit Lo Failure Limit Hi Warning Limit Lo 16 00 pH Variable limits 16 00 pH 02 00 pH 02 00 pH Return OK Diagnostics menu Whe...

Page 47: ...er settings The Excel file provides one worksheet for each module with columns for the following parameters Factory settings parameter set A parameter set B Enter your settings as parameter set A or B The gray cells in the parameter set B column cannot be modified since they contain sensor specific values which cannot be changed by parameter set switchover Here the values listed under parameter se...

Page 48: ...n the corresponding cells of the module worksheet Display The HOLD mode is active during parameter setting HOLD The NAMUR HOLD contact function check is active factory setting Module BASE Contact K2 N O contact Current output response is user defined Current meas The currently measured value appears at the current output Last usable value The last measured value is held at the current output Fixed...

Page 49: ...to the analyzer First the configuration data are written to the SmartMedia card These data can then be read and edited by the ProgaLog 3000 software 1 Save the configuration data at the Protos 3400 X Parameter setting System control Copy configuration With Save configuration the complete device configuration except the passcodes is written on the memory card 2 Close and remove the SmartMedia card ...

Page 50: ...a have been loaded the software lists the connected modules with all available configuration parameters The parameters are listed according to the modular device structure All configuration parameters except the Sensor data details which are deter mined by digital sensors can be edited at the PC After having finished the configuration save the data to the SmartMedia card ...

Page 51: ...os 3400 X Parameter setting System control Copy configuration Select Load configuration to write the complete device configuration except the passcodes to the Protos 3400 X ProgaLog 3000 Software for Configuration and Documentation Input errors are indicated by red highlighting Configuring the parameters e g relay contact usage 5 Save the configuration data to SmartMedia card ...

Page 52: ...Select your configuration from the modular system components offered in the left hand field 2 Click the right arrow to add the components or remove components by clicking 3 Now configure the parameters for the selected system components 4 Save the configuration You can save the configuration to a memory card that has been pre formatted in the Protos 3400 X and transfer them to analyzers with ident...

Page 53: ...ilure Log warning Yes No Yes Logbook Return 04 13 10 09 50 Measurement active 04 12 10 17 52 Measurement active 04 12 10 17 44 Parameter setting active 04 13 10 09 36 Parameter setting active 04 12 10 17 04 Measurement active 04 12 10 17 40 Wrong passcode 04 12 10 16 53 Diagnostics active Factory Setting Allows resetting the parameters to their factory setting When this menu is opened the analyzer...

Page 54: ... range of interest mA To configure current output Call up parameter setting Enter passcode Select Module BASE Select Output current I1 Configuring a Current Output Call up parameter setting Enter passcode Select Module BASE Select Output current Module BASE Administrator 19 2 C Return Contact K2 NAMUR HOLD Contact K4 NAMUR Failure Contact K3 NAMUR maintenance 7 00 pH Output current I2 Contact K1 L...

Page 55: ...near characteristic The process variable is represented by a linear output current curve Note Bilinear characteristic For a bilinear characteristic identical parameters are entered for the two vertices 1st vertex 2nd vertex Trilinear characteristic Two additional vertices must be entered Current Outputs Characteristics Select menu Parameter setting Module BASE ...

Page 56: ... resolution and high values with a low resolution Required Entering a value for 50 output current 100 50 Equation 1 K x 1 Kx E S 2 X50 X50 S K M S E S x S Start value at 4 mA X50 50 value at 12 mA output current range 4 to 20 mA E End value at 20 mA M Measured value Logarithmic output curve over one decade S 10 of maximum value X50 31 6 of maximum value E Maximum value Logarithmic output curve ove...

Page 57: ...utput level is at 63 after the time interval has been reached The time interval can be set from 0 to 120 sec If the time interval is set to 0 sec the current output follows the input Note The filter only acts on the current output and the current value of the second ary display not on the measurement display the limit values or the controller Time interval 0 120 sec Process variable 0 4 20 mA ...

Page 58: ... Air 22mA message Abort HOLD Fixed 22 mA Current meas Last usable value Message when the current range is exceeded As delivered the Maintenance request Warn message is generated when the current range is exceeded 3 8 mA or 20 5 mA This setting can be changed in the Parameter setting menu of the respective measuring module at Messages To generate a Failure message the limit value monitoring must be...

Page 59: ...ntion Warning is disabled during HOLD function check HOLD is active during calibration during maintenance current source meas point maintenance during parameter setting at the Operator level and the Administrator level during an automatic rinsing cycle As delivered the floating relay outputs of the BASE module are assigned to the NAMUR signals Failure Contact K4 normally closed signaling current f...

Page 60: ...cts are subject to electrical erosion Especially with inductive and capacitive loads the service life of the contacts will be reduced For suppres sion of sparks and arcing components such as RC combinations nonlinear resistors series resistors and diodes should be used Information concerning relay contacts As delivered the relay contacts are suitable for low signal currents down to approx 1 mA If ...

Page 61: ...mit value K1 K3 are user definable Usage NAMUR maintenance NAMUR HOLD Limit value Rinse contact Parameter set B active USP output COND module only KI rec active Sensoface Alarm control Menu Display Setting the relay contacts Relay Contacts Usage Open parameter setting Enter passcode Select Module BASE Select Contact Usage Fig Module BASE Alarm K4 K1 K2 K3 Contact K1 Administrator 19 2 C Return Hys...

Page 62: ...g Enter passcode Select Module BASE Select contact e g K1 Assign Sensoface message of desired measuring module to selected relay contact Contact K1 Administrator 19 2 C Return Hysteresis Variable Limit value 7 00 pH Usage Effective direction Contact type Limit value NAMUR maintenance NAMUR HOLD Sensoface Parameter set B active USP output Contact K1 Administrator 19 2 C Return OFF delay ON delay 7 ...

Page 63: ...ge Effective direction Contact type Limit value NAMUR maintenance NAMUR HOLD Rinse contact Parameter set B active USP output Rinse contact Contact K1 Administrator 19 2 C Return Rinse duration Rinse interval Rinsing lead time 7 00pH Usage Measurement lead time Contact type 0010 s Rinse contact 000 0 h 0010 s N O 0016 s Please note when configuring the Rinse contact function HOLD mode e g during pa...

Page 64: ...type Specifies whether the active contact is closed N O or open N C Contact K1 Administrator 19 2 C Return Hysteresis Variable Limit value 7 00 pH Usage Effective direction Contact type Limit value NAMUR maintenance NAMUR HOLD Rinse contact Parameter set B active USP output Hysteresis Tolerance band around the limit value within which the contact is not actuated Serves to obtain appropriate switch...

Page 65: ...ital inputs OK1 OK2 The following functions depending on the parameter setting can be started via a control signal OK1 Off or HOLD OK2 Select System control Function control matrix Off Parameter set A B Start KI recorder You must specify the switching level for the control signal active 10 30 V or active 2 V Module BASE OK1 OK2 OK1 OK2 OK Inputs OK1 OK2 Administrator 19 2 C Return OK2 usage 7 00 p...

Page 66: ... Parameter Set via Relay Contact Open parameter setting BASE module Select contact Usage Parameter set Selecting Parameter Set A B via OK2 Input Open parameter setting System control Function control matrix Select OK2 Connect Parameter set A B Contact K3 Administrator Abort 24 8 C Contact type OK NAMUR maintenance Usage ON delay NAMUR HOLD Limit value Rinse contact Parameter set B active USP outpu...

Page 67: ...V M S input 42 43 active 10 30 V or active 2 V A M input 40 41 active 10 30 V or active 2 V Output DCS 34 Measuring Alarm DCS outputs 31 34 N O N C Sensor detection On Off Immersion lock Off Sensocheck Glass el Access manual control Access code required All valves can be actuated separately Probe Probe type Ceramat SensoGate InTrac Others Move time max Adjustable default setting 0015 s Sealing wat...

Page 68: ...n the measured values displayed Cal Preset Values Unical 9000 Select pH module only if equipped with more than 1 pH module Select cal mode Adjustment The values determined by a calibration are taken over Calibration The values determined by a calibration are logged but not taken over Cal timer program Starts the selected program after cal timer expiry Return 25 6 C Cal Buffer 2 7 05 pH Module PHU ...

Page 69: ...Cal 1point Return 25 6 C Cal 2point 7 05 pH Clean User 2 Parking Monday Administrator Time of start 08 00 Return 25 6 C 03 Program 7 05 pH 01 Program Start 06 00 End 18 00 Int 002 0 h 02 Program Copy day Administrator Return 25 6 C 7 05 pH Weekday Copy Monday to Weekday Old day is overwritten Clean Cal 1point End User 3 0 00 6 00 12 00 18 00 24 00 Weekday View shows the configured program sequence...

Page 70: ...0002 s 05 Probe in MEASURE 0005 s 06 Program end Program step Probe Measure Probe Service Rinse water Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 Stroke 1 Stroke 2 Exposure time t s Cleaning continuous can also be started via a DCS input signal at input BIN1 of the Unical 9000 probe controller Message display Parameter setting Program flows Cleaning program ...

Page 71: ... 14 Program end Parameter Setting Program Flows Cal 2point Continuous Media Monitoring Off Program step Probe Measure Probe Service Rinse water Buffer 4 01 Pump I Buffer 7 00 Pump II Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 09 10 11 12 13 14 Stroke 1 Stroke 2 Exposure time Calibration with 1st buffer Calibration with 2nd buffer t s Cal 2point continuous can also...

Page 72: ...010 s 08 Rinse water 0002 s 09 Probe in MEASURE 10 Program end Parameter Setting Program Flows Cal 1point Continuous Media Monitoring Off Program step Probe Measure Probe Service Rinse water Buffer 4 01 Pump I Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 09 10 Stroke 1 Stroke 2 Exposure time Calibration with 1st buffer t s Message display ...

Page 73: ...the Wait position is reached There it remains until the signal status at the DCS inputs changes The program is started via the DCS inputs and remains in Wait position until the assignment of the DCS inputs changes DCS inputs BIN 1 BIN 3 of Unical 9000 The program is started by a short signal at the DCS inputs Wait position is skipped DCS inputs BIN 1 BIN 3 of Unical 9000 Notice If the programs are...

Page 74: ... water ON 0010 s 10 Rinse water OFF 0002 s 11 Probe in MEASURE 0005 s 12 Program end Parameter Setting Program Flows Parking Program step Probe Measure Probe Service Rinse water Buffer 4 01 Pump I Purge air AUX1 valve Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 09 10 11 Stroke 1 Stroke 2 Exposure time Wait t s Message display Wait position Parking is started via a ...

Page 75: ... s 09 Program end Parameter Setting Program Flows Measurement Short Time Media Monitoring Off Program step Probe Measure Probe Service Rinse water Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 Stroke 1 Stroke 2 Exposure time Probe in MEASURE short time t s Message display Measurement short time can also be started via a DCS input signal at input BIN1 of the Unical 90...

Page 76: ...nse water OFF 0002 s 11 Program end Parameter Setting Program Flows Cal 2point Short Time Media Monitoring Off Program step Probe Measure Probe Service Rinse water HOLD 01 02 03 04 05 06 07 08 09 t s Message display 10 Buffer 4 01 Pump I Buffer 7 00 Pump II Calibration with 1st buffer Calibration with 2nd buffer Cal 2point short time can also be started via a DCS input signal at input BIN2 of the ...

Page 77: ...nse water ON 0010 s 06 Rinse water OFF 0002 s 07 Program end Parameter Setting Program Flows Cal 1point Short Time Media Monitoring Off Program step Probe Measure Probe Service Rinse water HOLD DCS ML3 Program running 01 02 03 04 05 06 t s Message display Buffer 4 01 Pump I Calibration with 1st buffer Cal 1point short time ...

Page 78: ...in MEASURE 0005 s Service Measuring 11 Program end Parameter Setting Program Flows Service Program step Probe Measure Probe Service Rinse water HOLD DCS ML3 Program running 01 02 03 04 05 06 Message display Purge air AUX1 valve Part 1 Measure SERVICE Cleaning agent Pump III Stroke 1 Stroke 2 Exposure time 07 08 09 10 11 Part 2 SERVICE Measure Wait position Service can also be is started via a DCS ...

Page 79: ...tep above the selected program step and then allows selecting a function by editing the empty step Allows selecting a function Delete The program step is deleted Program flow Administrator Clean Abort 25 6 C Parking 7 05 pH Edit Service User 2 Copy Cal 2point approx 2 02 min Cal 1point approx 2 50 min approx 2 26 min User 2 Administrator 03 Rinse water ON 25 6 C 04 Rinse water OFF 7 05 pH 05 Buffe...

Page 80: ... can be edited Cal Buffer 1 Cal Buffer 2 Purge air On Text can be edited Purge air Off Text can be edited Aux medium On Text can be edited Aux medium Off Text can be edited Wait position Goto line ORP check Menu Display Configure function Activate monitoring Program flow Administrator 25 6 C 7 05 pH Blank step Function Cal Buffer 2 Cal Buffer 1 Purge air On Purge air Off Aux medium On Aux medium O...

Page 81: ...g Off Off Interval Continuous Default for interval 0001 0 h Rinse duration 05 s Check interval Off On Check after travels Maintenance interval Off On Maintenance after travels Rinse water Monitoring Off Process value Temperature Setpoint 07 00 pH Adm deviation 01 00 pH Media adapter Port I III Off Pump or Off Medium e g Buffer I Displaced volume 25 ml 50 75 100 ml Residual volume 250 ml 0 250 500 ...

Page 82: ...the process medium This method is applied when measuring aggressive or ther mally demanding process media which require short measurement times with long rest periods Menu Display Meas procedure External control via DCS Installation Administrator Access manual control Return 25 6 C Probe 7 05 pH Rinse water Meas procedure Ext control DCS Short time Sensor detection Continuous External Control via ...

Page 83: ...on Service O 33 Probe in SERVICE position Program runs O 32 Program running Level 0 1 0 1 0 1 0 1 0 1 Inputs Outputs of Unical 9000 X Passive contacts 24 V must be supplied externally or via DCS Signal duration at least 2 s passing contacts As delivered the signal output DCS 34 serves for probe position feedback as shown However you can also program this output as Alarm Then it sends a signal to t...

Page 84: ...am Request via M S The service program 7 stops all other running programs 1 6 immediately and erases stored requests For programs 1 6 the following applies When you start a new program the remaining steps of a currently running program are executed first Further requests are stored and executed subse quently When you control the Unical 9000 X via Protos 3400 X you can block the Bin 1 Bin 2 Bin 3 s...

Page 85: ...y adjusted depending on model Sealing Water Sealing water is switched on shortly before the probe movement is started to keep the rinsing chamber free from medium This is important for pro cesses containing fibrous or adhering media The sealing water pressure must be higher than the medium pressure Intrusion of medium is prevented by the counter pressure in the rinsing chamber which is caused by t...

Page 86: ... value or temperature of the media used buffer solutions cleaning solution rinsing water can be checked against a specified value in the calibration chamber This ensures that only correct media are used in the calibration chamber of the probe Exchanged or contaminated media or media with a wrong temperature are recognized In that case a message will be released If faulty media are recognized befor...

Page 87: ... Return 25 6 C Adm deviation 7 05 pH Additional medium 2 Medium Additional medium 1 Off On Monitoring Buffer I 07 00 pH 00 20 pH Purge air Process value Off On Installation Administrator Media adapter Return 25 6 C Additional media 7 05 pH Access manual control Start up Probe Yes Rinse water No Additional Media 2 Specifying the equipment On Off Designation of medium Monitoring Process value Temp S...

Page 88: ...es in the course of time particularly with long dwell times in one position System forecast and in Process position SensoGate in Service position The opening and closing times as well as the passing capacity of these valves can then be significantly changed Over time pneumatically controlled valves are also subject to changed switching times as a result of increasing friction fatty deposits or oth...

Page 89: ...7 c25 d33 e02 CM Auto New record Edit reference profile 12 21 16 12 37 P a09 b16 c26 d34 e02 CM Tolerances Active reference profile System forecast Administrator Auto 12 21 16 12 37 S a06 b17 c25 d33 e02 CM aXX eXX Records of separate travel times aXX Time 1 10 s from run command to response of air sensor bXX Time 1 10 s from run command until drop out of the exit limit position cXX Time 1 10 s fr...

Page 90: ...ference profile They are based on the following process conditions Process pressure 3 bar Compressed air 5 bar Unical hose length 5 m Temperature 20 C In the event of greater deviations in the process conditions you should create an individual User reference profile Return 25 6 C 07 00 pH Rinse water Additional media Start up Media adapter Probe System forecast System control Administrator Yes No ...

Page 91: ...ctive reference profile 12 21 16 12 37 P a09 b16 c26 d34 e02 CM Tolerances Auto New record System forecast Auto No Yes Edit reference profile Return 25 6 C 7 00 pH 01 01 00 00 00 S a00 b00 c00 d00 e00 X Auto 01 01 00 00 00 P a00 b00 c00 d00 e00 X Auto System forecast 12 21 16 12 37 S a06 b17 c25 d33 e02 12 21 16 12 37 P a09 b16 c26 d34 e02 Return 25 6 C 7 00 pH 12 21 16 12 37 S a06 b17 c25 d33 e02...

Page 92: ...on permissible deviations in the sep arate travel times can be set in the Tolerances menu The tolerances a e are permissible deviations from the active reference profile See next page The name User cannot be modified by the user The new profile is iden tifiable by the date and time of its recording Return 25 6 C 7 00 pH 12 21 16 12 37 S a06 b17 c25 d33 e02 CM Record new profile with Start softkey ...

Page 93: ...d in measuring mode if a tolerance limit is exceeded the corresponding message text can be viewed under Diagnostics Messages Return 25 6 C 7 00 pH 12 21 16 12 37 S a06 b17 c25 d33 e02 CM Monitoring Edit reference profile 12 21 16 12 37 P a09 b16 c26 d34 e02 CM Active reference profile Tolerances System control Administrator WA150 Off On Tolerances tol Input range a Probe valve switching time tol 0...

Page 94: ...sage text can be viewed under Diagnostics Messages The individual messages can be set to active or inactive switched off With Maintenance selected the icon is shown in measuring mode when a tolerance is exceeded With Failure selected the icon is shown in measuring mode when a tolerance is exceeded Return 25 6 C 7 00 pH U160 Pressure loss Air sensor Messages Maintenance U161 Probe valve not functio...

Page 95: ...erance lim its are exceeded in the probe travel profile the error number is displayed after the probe profile NOTICE In the Protos Unical system the last 200 travel cycles are recorded in vola tile memory i e the data is lost when the supply voltage is switched off Recording on a SmartMedia card is therefore recommended see follow ing page Return 25 6 C 7 00 pH 12 21 16 12 37 S a06 b17 c25 d33 e02...

Page 96: ...enu Parameter setting Probe control Installation System forecast System forecast Record on SmartMedia card Menu Display System forecast SmartMedia card Record on SmartMedia card If a SmartMedia card is installed probe travel times can be saved on it ASCII The recording capacity is limit ed only by the amount of memory on the card For this function use the final menu item in the system forecast Rec...

Page 97: ... switch PROCESS reacts too late after start of probe travel U172 SP Probe sluggish Probe sluggish limit position is reached U173 SP Probe is stuck during probe travel Probe is stuck during probe travel limit position is not reached U174 SP SERVICE position not functioning Limit switch SERVICE does not react after end of probe travel U175 SP PROCESS position not functioning Limit switch PROCESS doe...

Page 98: ...e 10 30 V or active 2 V Output DCS 34 Measuring Alarm DCS outputs 31 34 N O N C Sensor detection On Off Immersion lock Off Sensocheck Glass el Access manual control Access code required All valves can be actuated separately Probe Probe type SensoGate Ceramat others Move time max Adjustable default setting 0015 s Sealing water On Off Cavity rinsing Off Interval Continuous Check interval On Off On E...

Page 99: ...Module FRONT 3400 011 OK Return 25 6 C 7 05 pH Fixed interval Time control Week program Measuring module Cal mode Select Probe control Uniclean 900 Icons to assign the measured values displayed Measuring Module Select measuring module Select the pH module for evaluation with the Uniclean 900 controller only if equipped with more than 1 pH module Control Return 25 6 C Week program 7 05 pH Program f...

Page 100: ...n 25 6 C Clean 7 05 pH Rinse User 1 Parking Monday Administrator Time of start 08 00 Return 25 6 C 03 Program 7 05 pH 01 Program Start 06 00 End 18 00 Int 002 0 h 02 Program Copy day Administrator Return 25 6 C 7 05 pH Weekday Copy Monday to Weekday Old day is overwritten Clean Cal 1point End User 2 0 00 6 00 12 00 18 00 24 00 Weekday View shows the configured program sequences over the day Edit a...

Page 101: ...er OFF 0002 sec 04 Probe in MEASURE 0005 sec 05 Program end Program step Probe Measure Probe Service Rinse water HOLD DCS ML3 Program running 01 02 03 04 05 t s Cleaning continuous can also be started via a DCS input signal at input BIN1 of the Uniclean 900 probe controller Message display Parameter setting Program flows Rinse program ...

Page 102: ...r OFF 0002 sec 05 Probe in MEASURE 0005 sec 06 Program end Program step Probe Measure Probe Service Rinse water Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 Stroke 1 Stroke 2 Exposure time t s Cleaning continuous can also be started via a DCS input signal at input BIN1 of the Uniclean 900 probe controller Message display Cleaning program ...

Page 103: ... the Wait position is reached There it remains until the signal status at the DCS inputs changes The program is started via the DCS inputs and remains in Wait position until the assignment of the DCS inputs changes DCS inputs BIN 1 BIN 3 of Uniclean 900 The program is started by a short signal at the DCS inputs Wait position is skipped DCS inputs BIN 1 BIN 3 of Uniclean 900 Note If the programs ar...

Page 104: ...e water ON 0010 sec 09 Rinse water OFF 0002 sec 10 Probe in MEASURE 0005 sec 11 Program end Parameter Setting Program Flows Parking Program step Probe Measure Probe Service Rinse water Purge air AUX1 valve Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 09 10 Stroke 1 Stroke 2 Exposure time Wait t s Message display Wait position Parking is started via a DCS input signa...

Page 105: ...02 sec 09 Program end Parameter Setting Program Flows Measuring Short Time Program step Probe Measure Probe Service Rinse water Cleaning agent Pump III HOLD DCS ML3 Program running 01 02 03 04 05 06 07 08 Stroke 1 Stroke 2 Exposure time Probe in MEASURE short time t s Message display Measurement short time can also be started via a DCS input signal at input BIN1 of the Uniclean 900 probe controlle...

Page 106: ...0 Probe in MEASURE 0005 sec Service Measuring 11 Program end Parameter Setting Program Flows Service Program step Probe Measure Probe Service Rinse water HOLD DCS ML3 Program running 01 02 03 04 05 06 Message display Purge air AUX1 valve Part 1 Measure SERVICE Cleaning agent Pump III Stroke 1 Stroke 2 Exposure time 07 08 09 10 11 Part 2 SERVICE Measure Wait position Service can also be started via...

Page 107: ... in SERVICE Example 0020 sec Edit 02 Insert Delete Program name OK Configuring a Function Select a function using arrow keys confirm with enter Program end Probe in SERVICE Probe in MEASURE Rinse water On Rinse water Off Wait time Buffer I Text can be edited during installation Buffer II Text can be edited during installation Cleaning agent Text can be edited Cal Buffer 1 Cal Buffer 2 Purge air On...

Page 108: ...her Max move time 0015 sec Sealing water Off On Cavity rinsing Off Off Interval Continuous Check interval Off On Check after travels Maintenance interval Off On Maintenance after travels Media adapter Metering pump Off On or Off Medium e g Cleaning agent A Displaced volume 50 ml 25 50 75 100 ml Residual volume 250 ml 0 250 500 ml Additional media Additional medium 1 Off On then enter designation A...

Page 109: ...arily moved into the process medium This method is applied when measuring aggressive or thermally demanding process media which require short measurement times with long rest periods Menu Display Meas procedure External control via DCS Installation Administrator Access manual control Return 25 6 C Probe 7 05 pH Media adapter Meas procedures Ext control DCS Short time Sensor detection Continuous Ex...

Page 110: ...tion Service O 33 Probe in SERVICE position Program runs O 32 Program running Level 0 1 0 1 0 1 0 1 0 1 Inputs Outputs of Uniclean 900 X Passive contacts 24 V must be supplied externally or via DCS Signal duration at least 2 sec passing contacts As delivered the signal output DCS 34 serves for probe position feedback as shown However you can also program this output as Alarm Then it sends a signal...

Page 111: ... stored requests For programs 1 3 the following applies When you start a new program the remaining steps of a currently running pro gram are executed first Further requests are stored and executed subsequently When you control the Uniclean 900 X via Protos 3400 X you can block the Bin 1 Bin 2 Bin 3 signal lines as well as M S and A M to prevent conflicts Parameter setting Uniclean 900 Installation...

Page 112: ...lecting the retractable fitting Here the max move time is automati cally adjusted depending on model Sealing Water Sealing water is switched on shortly before the probe movement is started to keep the rinsing chamber free from medium This is important for processes containing fibrous or adhering media The sealing water pressure must be higher than the medium pressure Intrusion of medium is prevent...

Page 113: ...itoring Cleaning agent 07 00 pH 00 20 pH Purge air Process value Off On Installation Administrator Media adapter Return 25 6 C Additional media 7 05 pH Access manual control Start up Probe Yes Rinse water No Additional Media 2 Specifying the equipment On Off Designation of medium Monitoring Process value Temp Setpoint Start Up At the end of the parameter setting procedure a Start up line appears i...

Page 114: ...t a calibration is performed to detect the deviations of the electrode zero slope To do so the electrode is immersed in buffer solutions whose pH value is exactly known The measuring module measures the electrode voltages and the buffer solution temperature and automatically calculates the electrode zero and slope These data are stored in a calibration record By Adjustment the determined calibrati...

Page 115: ... AuditTrail continuous data recording and backup according to FDA 21 CFR Part 11 Adjustment Operator without administrator rights After calibration change to measur ing mode Inform Administrator When opening the menu Calibration respective module the Administrator sees all data of the last calibration and can take over the values or perform a new calibration Calibration data record Cal mode 25 6 C...

Page 116: ...here is great difference between the measured pH value and the electrode zero the pH measurement must be very accurate the electrode is exposed to extreme wear Three Point Calibration The electrode is calibrated with three buffer solutions Zero and slope are calculated using a line of best fit according to DIN 19268 Sensor Replacement First Calibration A First Calibration must be performed each ti...

Page 117: ...re Compensation The temperature of the buffer solution must be entered manually in the Parameter setting menu at Parameter setting pH module Sensor data Temp detection Cal temp manual Temperature measurement is performed using a glass thermometer for example Temp detection Administrator Return Temperature probe Measuring temp Cal temp 25 6 C 7 00 pH 025 6 C Proceed Manual There are two important r...

Page 118: ...to a week program The week program is defined in the Parameter setting menu It can automatically start up to 10 programs flows for each weekday Program Flows for One and Two Point Calibration The program flows for one and two point calibrations are preset but can be modified in the Parameter setting menu Probe Controller Start Programs The programs can be started directly from the Calibration menu...

Page 119: ...enu with different programs which have been defined in the Parameter setting menu During calibration the module is in HOLD mode Current outputs and relay contacts of the module behave as configured BASE module Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Calibration 25 6 C Return Info 7 00 pH Probe control Probe control 25 6 C Return Start manual cal proc Sensor replacement 7 0...

Page 120: ...ay Start manual Cal proc Open calibration Press menu key to select menu Select calibration using arrow keys confirm with enter passcode 1147 To change passcode select Parameter setting System control Passcode entry Pressing enter at Start manual cal process allows the selection of a calibration method During calibration the module is in HOLD mode Current outputs and relay contacts of the module be...

Page 121: ...e Start calibration Follow the instructions given in the display After end of calibration reinstall the electrode UNICAL 7 00 pH 25 6 C Probe in SERVICE position With the SERVICE program the probe is moved into SERVICE position The program steps are indicated in the display Program Service Water pressure OK 3 Rinse water ON UNICAL End Service 7 00 pH 25 6 C Service position by means of Probe maint...

Page 122: ...utputs during calibration Measuring Calibration Module A Module B Selecting the measuring module K2 contact HOLD is active Module A Calibration Module B Calibration End of calibration or abort Measuring The current output of the selected module is in HOLD mode indicated by ...

Page 123: ...ol Passcode entry Calibration Select PHU module Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Calibration 25 6 C Return Info 7 00 pH Module PHU 3400 110 Module PHU 3400 110 25 6 C Return Data entry premeasured electrodes Manual entry of buffer values Product calibration 7 00 pH Calimatic automatic calibration ORP calibration When you open the Calibration menu the analyzer automa...

Page 124: ...ted using a reference temperature of 25 C During calibration the module is in HOLD mode Current outputs and relay contacts of the module behave as configured BASE module Caution Only ever use fresh undiluted buffer solutions which belong to the selected buffer set Menu Display Automatic buffer recognition Remove and rinse the electrode Caution Do not rub Electrostatic hazard then immerse it in the...

Page 125: ...ly Immerse electrode in the second buffer solution Start with softkey or enter Calibration is performed with the second buffer Three point calibration is performed correspondingly with the third buffer Calimatic 0001s Drift check with 1st buffer running Zero correction Electrode potential 0000 mV Calibration temp 25 5 C 25 6 C 7 00 pH Nominal buffer value Response time Calimatic Dip sensor in 1st ...

Page 126: ...reference temperature of 25 C During calibration the module is in HOLD mode Current outputs and relay contacts of the module behave as configured BASE module Caution Only ever use fresh undiluted buffer solutions Menu Display Manual entry Manual entry Return Cal medium Buffer solution When changing sensors perform First cal for statistics Cal temp 25 6 C 7 00 pH 025 6 C Proceed First buffer soluti...

Page 127: ...nt calibration is performed correspondingly with the third buffer Manual entry Drift check with 1st buffer running Zero correction Electrode potential 0224 mV Calibration temp 25 6 C 25 6 C 4 00 pH 0018s Nominal buffer value Response time 04 00 pH End Manual entry Dip sensor in 1st buffer then Start calibration For one point calibration End procedure 25 6 C 7 00 pH End Start Second buffer solution...

Page 128: ...contacts of the module behave as configured BASE module Caution The pH value of the sample is temperature dependent Therefore the reference measurement should be performed at the sample temperature shown in the display Transport the sample in an insulated container The pH value may also be altered due to escaping of volatile substances Menu Display Product calibration Select module PHU 3400 110 Th...

Page 129: ...appears Enter reference value Lab value Confirm with OK or repeat calibration Product calibration Return Cal medium Product Cal by taking sample and input of pH value 25 6 C 7 00 pH Product calibration Step 1 Sampling Save the sample value Input lab value Measured value 25 0 C 7 00 pH 25 0 C Temperature 7 00 pH Input Save Product calibration Abort Step 2 Lab value Input sample lab value 25 6 C 7 0...

Page 130: ... HOLD mode Current outputs and relay contacts of the module behave as configured BASE module Menu Display Data entry Select Data entry of premeasured electrodes Remove electrode and connect premeasured electrode Call up Sensor replacement Enter the values for Zero Slope Isothermal potential Return with softkey Return to measurement with meas Data entry Return When changing sensors perform First ca...

Page 131: ...s comprehensive functions for monitoring proper calibration performance and the electrode condition This allows documentation for quality management to ISO 9000 and GLP GMP Sensocheck monitors the electrode condition by measuring the glass and reference electrode impedances Regular calibration can be monitored by the cal timer Adaptive cal timer automatically reduces the calibration interval when ...

Page 132: ...n reduction potential measured ORP mVmeas direct electrode potential ORP input see Sensor monitor mV delta value determined during calibration ORP related to the standard hydrogen electrode SHE The oxidation reduction potential can also be calibrated automatically with respect to the standard hydrogen electrode SHE To do so you must first select the reference electrode used see Parameter setting T...

Page 133: ...stment Return Reference electrode 25 6 C 200 mV Ag AgCl KCl 1m 25 5 C Temperature ORP input 200 mV 200 mV ORP setpoint ORP adjustment Abort Reference electrode 25 6 C 200 mV Ag AgCl KCl 1m 25 5 C Temperature ORP input 200 mV ORP setpoint 0220 mV OK ORP adjustment Reference electrode 25 6 C 220 mV Ag AgCl KCl 1m 25 5 C Temperature ORP input 220 mV 200 mV ORP setpoint Return End Temperature C Ag AgC...

Page 134: ...ch time a new sensor is connected to adjust the operating point The adjustment for that sensor remains stored in the analyzer Afterwards you should perform a two point calibration using one of the following methods Calimatic automatic calibration Manual entry of buffer values Data entry premeasured electrodes During calibration the module is in HOLD mode Current outputs and relay contacts of the m...

Page 135: ... 6 C 7 00 pH Nominal buffer value Response time Electrode voltage Calibration temperature s mV C pH 10 122 7 00 25 6 ISFET zero adjustment At the end of the adjustment proce dure the ISFET zero based on 25 C is displayed This is not the real sensor value The actual value must be determined afterwards by a complete two point calibration To abort you can press the End softkey However this reduces ad...

Page 136: ... the process temperature is precisely measured using a cali brated reference thermometer The measurement error of the reference thermometer should be less than 0 1 C Adjustment without precise measurement might result in consid erable deviations of the measured value display Sensor Monitor for validation of sensor and complete measured value processing Menu selection Return to meas 22 3 C Select e...

Page 137: ...robe maintenance With the Unical SERVICE program the probe is moved into SERVICE position The individual program steps are indicated in the display 01 Probe in SERVICE 02 Cleaning agent 0020 sec 03 Rinse water ON 0060 sec 04 Rinse water OFF 0002 sec 05 Purge air ON 0005 sec 06 Purge air OFF 0002 sec 07 Wait position 08 Rinse water ON 0010 sec 09 Rinse water OFF 0002 sec 10 Probe in MEASURE 0005 se...

Page 138: ...n menu Default 2958 Unical manual control End Service 7 00 pH 25 6 C Manual Control via Protos 3400 X Maintenance Probe control Menu Menu Display Maintenance ON Warning for Use of Manual Control Make sure that the probe is separated from the process Manual control via Protos 3400 X allows actuating the probe controller for servicing Rinsing water media supply and valve functions can be tested indi...

Page 139: ... Cleaner 0020 sec 03 Rinse water ON 0060 sec 04 Rinse water OFF 0002 sec 05 Probe in MEASURE 0005 sec 06 Program end Manual control Yes 25 6 C Start program 7 00 pH No Single step control UNICAL Safety prompt Execute function Please select End 01 Probe in SERVICE 02 Cleaner 0020 s 03 Rinse water ON 0060 s 25 6 C 7 00 pH Clean Single step 04 Rinse water OFF 0004 s Program status OK Single step Retu...

Page 140: ...ividual interval for each counter After expiry of this interval a message is generated You can reset the counters in the maintenance menu Probe Wear Maintenance Probe control Menu Menu Display Maintenance Probe wear Probe wear 7 00 pH 25 6 C Reset check counter 750 of 100000 Probe travel total Reset maintenance counter Yes 2101 No Maintenance counter Check counter 750 of 20000 Yes No ...

Page 141: ...ended logbook SmartMedia card SW 3400 104 Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Diagnostics Return 25 6 C Set favorite 7 00 pH Logbook Message list Device description Module FRONT Module BASE Diagnostics Point of meas description Return 25 6 C 7 00 pH Note Tank_2 Measurement point Point of Meas Description Allows entering a tag number and a note Select position left righ...

Page 142: ...dard output signals Test possibilities Module diagnostics Input output status Example Module BASE input output status Device description Return 22 7 C 7 00 pH pH C and probe control Module PHU 3400 110 Serial number 0000313 BASE Module FRONT Module FRONT Return 22 7 C 7 00 pH Display test Keypad test Module diagnostics Module BASE Return 22 7 C 7 00 pH Input output status Set favorite Module diagn...

Page 143: ... control Function control matrix Module Diagnostics Internal function test Sensor Monitor Shows the values currently measured by the sensor Important function for diagnostics and validation Menu selection Return to meas 22 3 C Select enter Lingua Module PHU 3400 110 22 3 C Return Cal record Sensor monitor 7 00 pH 7 00 pH Sensor network diagram Statistics Set favorite Module diagnostics Sensor moni...

Page 144: ...tolerance ranges for zero and slope over the time If the values determined by a calibration exceed the tolerance limits an adjustment can be executed automatically Display can be graphical or as a listing The tolerance band for zero and slope is configured during parameter setting Module PHU 3400 110 Cal preset values Adaptive cal timer 22 3 C 7 00 pH T band recorder Return Zero 22 3 C 7 00 pH Slo...

Page 145: ...fo softkey Statistics Indication of sensor data for the First Calibration adjustment and the last 3 calibrations compared to the First Calibration Date and time of First Calibration zero and slope impedance of glass and reference electrode response time Cal record Return Active adjustment 24 2 C 7 00 pH 05 04 10 09 34 08151234 Serial number Sensor type Data entry Cal mode 057 7 mV pH 07 00 pH Zero...

Page 146: ... control 22 3 C Return Unical network diagram 7 00 pH 7 00 pH Set favorite Unical status Unical status Return Communication 24 2 C 7 00 pH ok ok Water pressure Compressed air ok Buffer 7 00 ok Buffer 4 01 ok Unical Status The media ports at the media adapter are checked During installation you can enter texts specifying the media here for example Buffer 7 00 Unical network diagram Return 24 1 C 7 ...

Page 147: ...ng mode using a softkey To configure Parameter setting System control Function control matrix Menu selection Return to meas 22 3 C Select enter Lingua Probe control 22 3 C Return 7 00 pH 7 00 pH Set favorite Uniclean status Uniclean status Return Communication 24 2 C 7 00 pH ok ok Compressed air Flash check sum ok Water pressure 569 of 9999 ok Cleaning agent Wear counter ok Uniclean Status The med...

Page 148: ...xceeded in the probe travel profile the error number is displayed after the probe profile NOTICE In the Protos Unical system the last 200 travel cycles are recorded in non volatile memory i e the data are lost when the supply voltage is switched off Recording on a SmartMedia card is therefore recommended see following page Return 25 6 C 7 00 pH 07 21 10 12 37 S a06 b17 c25 d33 e02 CM Load probe mo...

Page 149: ...Diagnostics functions can be called directly from the measuring mode using a softkey The table on the next page explains how to select favorites Secondary displays 1 Here additional values are displayed in the measuring mode according to the factory setting When the respective softkey 2 is pressed the process variables measured by the modules plus date or time are displayed In addition you can use...

Page 150: ...have been set as Favorite can be directly called from the measuring mode Menu Display Select favorites Favorites menu Diagnostics functions can be called directly from the measuring mode using a softkey The Favorites are selected in the Diagnostics menu Select favorites Press menu key to select menu Select diagnostics using arrow keys confirm with enter Then select module and confirm with enter 09...

Page 151: ...rently activated warning or failure messages in plain text Menu selection Return to meas 7 00 pH 25 6 C Select enter Lingua Diagnostics Return 23 7 C Set favorite 7 00 pH Logbook Message list Device description Module FRONT Message list Return 25 6 C 7 00 pH Warn Module BASE 8 messg Point of meas description Warn Temp alarm HI Saturation Air Alarm HI Fail Wrong ISM sensor Warn Tolerance band Warn ...

Page 152: ...l 1 2 Sensor connection F086 ComFu E Channel 1 1 Battery empty F087 ComFu E Channel 1 2 Battery empty F090 ComFu E Channel 2 2 No sensor F091 ComFu E Channel 2 3 No sensor F092 ComFu E Channel 2 2 Communication interrupted F093 ComFu E Channel 2 3 Communication interrupted F094 ComFu E Channel 2 2 Sensor connection F095 ComFu E Channel 2 3 Sensor connection F096 ComFu E Channel 2 2 Battery empty F...

Page 153: ...ext F222 Parameter setting active Text F223 Diagnostics active Text F225 Measurement active Text F226 Power supply OFF Text F227 Power supply ON Text F228 Software update Text F229 Wrong passcode Text F230 Factory setting Text F231 Configuration changed Text F232 Module equipment Ex non Ex FAIL F233 Module equipment Ex FAIL ...

Page 154: ...lure Firmware Flash check sum FAIL B070 Current I1 Span WARN B071 Current I1 0 4 mA WARN B072 Current I1 20 mA WARN B073 Current I1 Load error FAIL B074 Current I1 Parameter WARN B075 Current I2 Span WARN B076 Current I2 0 4 mA WARN B077 Current I2 20 mA WARN B078 Current I2 Load error FAIL B079 Current I2 Parameter WARN B200 Rinsing program active Text B254 Module reset Text ...

Page 155: ... FAIL P016 Temperature Alarm LO_LO FAIL P017 Temperature Alarm LO WARN P018 Temperature Alarm HI WARN P019 Temperature Alarm HI_HI FAIL P020 ORP range FAIL P021 ORP Alarm LO_LO FAIL P022 ORP Alarm LO WARN P023 ORP Alarm HI WARN P024 ORP Alarm HI_HI FAIL P025 rH range WARN P026 rH Alarm LO_LO FAIL P027 rH Alarm LO WARN P028 rH Alarm HI WARN P029 rH Alarm HI_HI FAIL P030 Zero range WARN P035 Slope r...

Page 156: ...D Sensor wear User defined P071 SENSOFACE SAD ISFET leakage current User defined P090 Buffer offset specifiable buffer table WARN P091 Zero offset ORP WARN P092 Tolerance band WARN P110 CIP counter User defined P111 SIP counter User defined P112 Autoclaving counter User defined P113 Sensor operating time duration of use User defined P114 ISFET characteristic User defined P115 Membrane body changes...

Page 157: ... PH messages Message type A010 pH Diff Range FAIL A011 pH Diff Alarm LO_LO FAIL A012 pH Diff Alarm LO WARN A013 pH Diff Alarm HI WARN A014 pH Diff Alarm HI_HI FAIL A015 Temperature Diff Range FAIL A016 Temperature Diff Alarm LO_LO FAIL A017 Temperature Diff Alarm LO WARN A018 Temperature Diff Alarm HI WARN A019 Temperature Diff Alarm HI_HI FAIL A020 ORP Diff Range FAIL A021 ORP Diff Alarm LO_LO FA...

Page 158: ... status FAIL U224 Probe control flooded FAIL U225 Probe control Probe valve defective FAIL U226 Probe Limit position switch FAIL U227 Probe Limit position SERVICE FAIL U228 Probe cylinder untight WARN U229 Sensor dismount guard defective WARN U230 Probe Limit position MEASURE FAIL U231 Probe Move time MEASURE WARN U233 Probe control Switch water pressure WARN U234 Probe move time SERVICE WARN U235...

Page 159: ...r WARN U245 Check Add medium 1 WARN U246 Check Add medium 2 WARN U248 Probe control Water valve WARN U249 Proble check counter WARN U250 Proble maintenance counter WARN U251 Probe control Calibration error WARN U252 Probe control Communication error WARN U253 Probe control WARN Messages ...

Page 160: ...160 ...

Page 161: ...tch PROCESS reacts too late after start of probe travel U172 SP Probe sluggish Probe sluggish limit position is reached U173 SP Probe is stuck during probe travel Probe is stuck during probe travel limit position is not reached U174 SP SERVICE position not functioning Limit switch SERVICE does not react after end of probe travel U175 SP PROCESS position not functioning Limit switch PROCESS does no...

Page 162: ...q Alarm MAINT REQ active Probe move time SERVICE U234 MAINT REQ active Probe Move time MEASURE U231 FAIL active active Probe limit position SERVICE U227 FAIL active active Probe Limit position MEASURE U230 FAIL active active Compressed air switch U220 FAIL active active UNICAL Probe valve defective U225 FAIL active active UNICAL flooded U224 ...

Page 163: ...obe defective Probe sticky MEASURE limit switch defective Probe valve defective Pilot valve defective None message only By next smooth probe movement MEASURE limit position was not reached even after several trials Media adapter untight Failure in compressed air supply Pressure too low P E converter defective Safety valve defective shut None message only Automatic as soon as pressure is provided P...

Page 164: ...2 MAINT REQ active Safety valve defective U235 MAINT REQ active Sensor dismount guard defective U229 MAINT REQ active Buffer almost empty Err text from medium description U190 U191 FAIL active active Buffer empty Err text from medium description U194 U195 MAINT REQ active Cleaner almost empty Err text from medium description U192 FAIL active active Cleaner empty Err text from medium description U1...

Page 165: ...use of defect Filling level below minimum Float switch stuck Check back error line interrupted or short circuited Bottle untight None message only Automatic when buffer solution is topped up above min level Start immediately when intervals have expired Residual bottle contents used up Float switch stuck Check back error line interrupted or short circuited All programs requiring buf fer solution ar...

Page 166: ...ter pressure U220 MAINT REQ active Probe cylinder untight U228 MAINT REQ active Proble check counter Proble maintenance counter U249 U250 MAINT REQ active Media monitoring Err texts from medium description U241 U246 MAINT REQ active active UNICAL Calibration error U251 Can only be detected with SERVICE switch function Error messages of probe control ...

Page 167: ...c as soon as cause of trouble removed Probe cylinder or probe lines untight Maintenance required Counter expired None message only Manual reset in maintenance menu Wrong medium Wrong medium temp Media mixed System untight Probe untight None message only Automatic as soon as medium OK Buffers interchanged Identical buffers Buffer unknown Cal temp Sensor unstable Zero too low high Slope too low high...

Page 168: ... req Alarm MAINT REQ active Probe move time SERVICE U234 MAINT REQ active Probe move time MEASURE U231 FAIL active active Probe limit position SERVICE U227 FAIL active active Probe limit position MEASURE U230 FAIL active active Compressed air switch U220 FAIL active active Probe valve defective U225 FAIL active active UNICLEAN flooded U224 ...

Page 169: ...be defective Probe sticky MEASURE limit switch defective Probe valve defective Pilot valve defective None message only By next smooth probe movement MEASURE limit position was not reached even after several trials Media adapter untight Failure in compressed air supply Pressure too low P E converter defective Safety valve defective shut None message only Automatic as soon as pressure is provided Pi...

Page 170: ...ssage with Ceramat only MAINT REQ active Sensor dismount guard defective U229 Message with Ceramat only MAINT REQ active Cleaner almost empty U192 FAIL active active Cleaner empty U196 MAINT REQ active UNICLEAN switch Water pressure U220 MAINT REQ active Probe cylinder untight U228 MAINT REQ active Proble check counter Proble maintenance counter U249 U250 ...

Page 171: ...sage only Automatic when clean ing solution is topped up above min level Start immediately when intervals have expired Residual bottle contents used up Float switch stuck Check back error line interrupted or short circuited All programs requiring clean ing solution are blocked Automatic when cleaning solution is topped up Start immediately when intervals have expired No water Water pressure too lo...

Page 172: ...200 kΩ Measurement error pH value 0 02 TC 0 001 pH K display ORP value 1 mV TC 0 05 mV K l l Temperature input Pt 100 Pt 1000 NTC 30 kΩ NTC 8 55 kΩ Ex ia IIC 2 wire connection adjustable Measuring range MR 20 150 C Pt 100 Pt 1000 NTC 30 kΩ 10 130 C NTC 8 55 kΩ Mitsubishi Resolution 0 1 C Measurement error 0 2 meas val 0 5 K 1 K with NTC 100 C l l Temp compensation Reference temp 25 C media depende...

Page 173: ...Ciba 2 06 4 00 7 00 10 00 Reagecon 2 00 4 00 7 00 9 00 12 00 Manually enterable buffer set with max three buffer tables Additional function SW3400 002 Nom zero pH 0 14 calibration range pH 1 Nom slope 25 C 25 61 mV pH calibration range 80 103 Viso 1000 1000 mV l l Calibration record Recording of zero slope Viso response time calibration method with date and time l l Statistics Recording of Zero sl...

Page 174: ...djustment tolerance limits adjustable Additional function SW3400 005 graphical recording of zero point and slope of the last 40 calibrations adjustments l l Sensor monitoring Criteria for sensor network diagram Sensoface adjustable and NAMUR messages individually adjustable l l RS 485 Vo Vi 5 V Io Ii 250 mA Ri 20 Ω Ex ia IIC Transfer rate 1200 Bd for UNICAL 8 data bits 1 stop bit parity odd Record...

Page 175: ...NAMUR NE 21 and EN 61326 1 EN 61326 2 3 Class B residential area Industry Lightning protection EN 61000 4 5 Installation Class 2 Nominal operating conditions Ambient temperature 20 55 C Ex max 50 C Rel humidity 10 95 not condensing Transport Storage temperature 20 70 C Screw clamp connector Single wires and flexible leads up to 2 5 mm2 ...

Page 176: ...SE module basic device or by communication modules e g OUT PID The corresponding parameters must be set there The minimum current span shall prevent that the resolution limit of the measurement technology 1 count is seen in the current PHU 3400 X 110 Module pH 1 00 ORP 100 0 C 10 0 mV 100 0 rH 1 00 F 10 0 Calculation Block PH PH Diff pH 1 00 Diff ORP 100 0 Diff C 10 0 ...

Page 177: ...177 Appendix Buffer Table Mettler Toledo ...

Page 178: ... 12 39 10 2 01 4 02 7 04 9 11 12 26 15 2 00 4 01 7 02 9 05 12 13 20 2 00 4 00 7 00 9 00 12 00 25 2 00 4 01 6 99 8 95 11 87 30 2 00 4 01 6 98 8 91 11 75 35 2 00 4 01 6 96 8 88 11 64 40 2 00 4 01 6 96 8 85 11 53 50 2 00 4 01 6 96 8 79 11 31 60 2 00 4 00 6 96 8 73 11 09 70 2 00 4 00 6 96 8 70 10 88 80 2 00 4 00 6 98 8 66 10 68 90 2 00 4 00 7 00 8 64 10 48 ...

Page 179: ...179 Appendix Buffer Table DIN 19267 ...

Page 180: ...ificate of an accredited laboratory This certifi cate is supplied with the respective buffer materials Only these pH S values shall be used as standard values for the secondary reference buffer materials Correspondingly this standard does not include a table with standard pH values for practical use The table above ony provides examples of pH PS values for orientation ...

Page 181: ...181 Appendix Buffer Table Techn Buffers to NIST ...

Page 182: ...182 Appendix Buffer Table Hamilton ...

Page 183: ...183 Appendix Buffer Table Kraft ...

Page 184: ...184 Appendix Buffer Table Hamilton A ...

Page 185: ...185 Appendix Buffer Table Hamilton B ...

Page 186: ...186 Appendix Buffer Table HACH ...

Page 187: ...6 2 06 2 05 2 08 2 07 2 07 2 04 2 02 2 03 2 04 2 05 4 00 4 02 4 00 4 00 4 01 4 02 4 00 4 01 4 02 4 03 4 04 4 05 4 10 4 10 4 11 4 13 4 15 4 17 4 20 4 22 7 10 7 08 7 05 7 02 6 98 6 98 6 96 6 95 6 94 6 93 6 93 6 91 6 93 6 92 6 92 6 92 6 93 6 95 6 97 6 99 10 30 10 21 10 14 10 06 9 99 9 95 9 89 9 85 9 81 9 77 9 73 9 68 9 66 9 61 9 57 9 54 9 52 9 47 9 43 9 38 extrapoliert Puffertabellen Extrapolated ...

Page 188: ...99 8 95 11 81 35 C 2 00 4 02 6 98 8 90 11 63 40 C 2 01 4 03 6 97 8 86 11 47 45 C 2 01 4 04 6 97 8 83 11 39 50 C 2 00 4 05 6 96 8 79 11 30 55 C 2 00 4 07 6 96 8 77 11 13 60 C 2 00 4 08 6 96 8 74 10 95 65 C 2 00 4 10 6 99 8 70 10 95 70 C 2 00 4 12 7 00 8 67 10 95 75 C 2 00 4 14 7 02 8 64 10 95 80 C 2 00 4 16 7 04 8 62 10 95 85 C 2 00 4 18 7 06 8 60 10 95 90 C 2 00 4 21 7 09 8 58 10 95 95 C 2 00 4 24...

Page 189: ...n parameter setting System control Select Buffer table Select buffer to be entered Return 25 6 C 7 20 pH Point of measurement Logbook Concentration table Release of options Calculation Blocks Buffer table System control Administrator Return 25 6 C 7 10 pH Buffer 2 Buffer 3 Buffer 1 Buffer table Administrator Return 25 6 C 7 10 pH Nominal buffer value pH value at 10 C pH value at 15 C pH value at 0...

Page 190: ... Register recorder Decimal separator Card full Format Menu only appears with SmartMedia Card inserted Make sure that it is a memory card not an update card Commercially available SmartMedia cards must be formatted in the analyzer before they can be used as memory card Copy configuration The complete configuration of an analyzer can be written on a SmartMedia card This allows transferring all devic...

Page 191: ...nual Signal outputs and inputs contacts BASE module Contact K4 Contact type ON delay OFF delay NAMUR failure Contacts K3 K2 K1 Usage Maintenance request HOLD function check Limit value adjustable Rinse contact adjustable Parameter set B active USP output KI recorder active Sensoface Controller alarm alarm output Unical Uniclean Contact type ON OFF delay Factory setting K3 Maintenance request K2 HO...

Page 192: ...play Select Selection for Measurement Calibration Cal preset values Calimatic buffer Knick Mettler Toledo Merck Riedel DIN 19267 NIST standard technical Hamilton Kraft Hamilton A B HACH Ciba Reagecon Table Drift check Cal timer Cal tolerance band ORP check TC process medium Select Off linear ultrapure water table ORP rH value Reference electrode ORP conversion to SHE Calculate rH with factor Delta...

Page 193: ...gramming Installation Meas procedure External control DCS DCS inputs 36 39 M S input 42 43 A M input 40 41 DCS output 34 DCS outputs 31 34 Sensor detection Immersion lock Access manual control Probe Probe type Max move time Sealing water Cavity rinsing Check interval Maintenance interval Rinse water Monitoring For first start up or change of configuration Continuous probe always in the process Sho...

Page 194: ...pH default Start up Yes No Makes sure that the tubings between media adapter and probe are filled with calibration medium Media adapter Port II Medium Displaced volume Residual volume Monitoring Setpoint Adm deviation Usage Metering pump Off Buffer 4 01 25 50 75 100 ml 0 250 500 ml Process value Temperature Off 7 00 pH default 00 50 pH default Port III Medium Displaced volume Residual volume Monit...

Page 195: ...diagnostics Input output status PHU 3400 X 110 Module Module diagnostics Sensor monitor Cal record Cal record ORP Sensor network diagram PH Statistics Internal function test Shows the values currently measured by the sensor Data of last adjustment calibration Data of last ORP adjustment calibration Graphical representation of the sensor parameters Displays first calibration and deviations of last ...

Page 196: ...ion Calimatic 124 Automatic temperature compensation 117 B BASE module 17 Behavior during messages 58 Buffer sets to be entered 189 Buffer tables 177 Buffer table specifiable 189 Buffer values manual entry for calibration 126 C Cable glands 14 Calibration 114 Calibration by entering data from premeasured electrodes 130 Calibration methods 116 Calibration procedures 118 Calibration timer diagnostic...

Page 197: ...program 107 Configure measurement display 28 Configure program flow Unical 9000 79 Configure program flow Uniclean 900 107 Connecting the probe controller 25 Connecting the sensor 23 Contacts 54 Contact type 64 Continuous calibration Unical program 71 Control programs Unical 9000 84 Control programs Uniclean 900 111 Control via process control system Unical 9000 83 Control via process control syst...

Page 198: ...me Unical 9000 79 Error messages 152 Error messages of Unical 9000 X 162 Error messages of Uniclean 900 X 168 Error messages system forecast 97 Explosion protection 175 External control via DCS Unical 9000 82 External control via DCS Uniclean 900 109 F Factory setting 53 Failure signal 59 Favorites 149 FDA 21 CFR Part 11 9 First Calibration 116 Fixed interval Unical program 69 Fixed interval Unicl...

Page 199: ... in the measurement display 64 Linear characteristic 55 Lock icon 32 Locking a function 32 Logarithmic output curve 56 Logbook diagnostics 141 Logbook parameter setting 53 M Maintenance 136 Maintenance counter 140 Maintenance interval Unical program 85 Maintenance interval Uniclean 900 112 Maintenance request signal 59 Manual electrode calibration 120 Manual entry of buffer values 126 Manual tempe...

Page 200: ...ssages default settings and selection range 45 Messages overview 152 Messages response of current outputs 58 Messages system forecast 94 Message when the current range is exceeded 58 Minimum spans for current outputs 176 Modular concept 13 Module equipment 17 Modules 16 Module software 11 Monitoring functions for calibration 131 Monitoring the behavior of retractable fittings 88 N NAMUR signals cu...

Page 201: ...ameter setting Unical 9000 67 Parameter setting Uniclean 900 98 Parking Unical program 74 Parking Uniclean program 104 Park program Unical 9000 73 Park program Uniclean 900 103 Passcode entry 27 Passcode lost 27 Point of meas description 141 Probe controller connection 25 Probe controller icons 209 Probe control Unical menu 68 Probe control Uniclean menu 99 Probe maintenance 137 Probe travel profi...

Page 202: ...an 900 104 Program flow Rinsing continuous Uniclean 900 101 Program flow Service Unical 9000 78 Program flow Service Uniclean 900 106 Program flows Unical 9000 70 Program flows Uniclean 900 101 Protective wiring 60 R Reference profile Auto system forecast 91 Reference profiles messages 94 Reference profile User system forecast 92 Relay contacts protective wiring 60 Relay contacts Sensoface message...

Page 203: ...5 Sensor detection Uniclean parameter setting 112 Sensor monitor 143 Sensor monitor maintenance menu 136 Sensor network diagram 145 Sensor replacement 116 Serial number 11 Service Unical program 78 Service Uniclean program 106 Settings documentation 47 Settings of sensor data 34 Shield 22 Short description 14 Short time cal 1point Unical program 77 Short time cal 2point Unical program 76 Signaling...

Page 204: ...tolerances 93 T Table of contents 3 Tag number 141 Temperature compensation during calibration 117 Temperature dependence of commonly used reference systems measured against SHE 133 Temp probe adjustment 136 Terminal compartment 17 Terminal plate 21 Terminal plates of hidden modules 16 Three point calibration 116 Time control fixed interval Unical 9000 69 Time control fixed interval Uniclean 900 1...

Page 205: ...Unical network diagram 146 Unical parameter setting 67 Unical status 146 Uniclean 900 X connection 25 Uniclean 900 X error messages 168 Uniclean 900 X single step control 139 Uniclean parameter setting 98 Uniclean status 147 V Viewing level 31 W Wait position Unical program 73 Wait position Uniclean program 103 Week program Unical 9000 69 Week program Uniclean 900 100 Wiring examples 23 Index ...

Page 206: ...206 Index ...

Page 207: ...207 Index ...

Page 208: ...the plaintext display in front of a menu line Access to next menu level with enter In the plaintext display in front of a menu line when it has been blocked by the Administrator against access from the Operator level Designates the module slot 1 2 or 3 allowing the clear assignment of measured value parameter displays in the case of identical module types Indicates the active parameter set The ana...

Page 209: ...r active Metering pump at media adapter port I active Metering pump at media adapter port II active Additional medium 1 activated Additional medium 2 activated Metering pump at media adapter port III active Valve at port III active Probe in SERVICE position Probe changes position Probe in MEASURE position PROCESS Overview of icons Overview of icons ...

Page 210: ...tic automatic calibration 124 Calibration with manual entry of buffer values 126 Product calibration 128 Data entry premeasured electrode 130 ORP calibration 132 ISFET zero adjustment 134 Maintenance 136 Sensor monitor 136 Temperature probe 136 Diagnostics 141 Setting diagnostics messages as favorite 149 Message list 151 Error messages 152 Error messages of system forecast 161 Error messages of Un...

Page 211: ...m 100 Parameter setting Program flows 101 Rinse program 101 Cleaning program 102 Park program 103 Measuring program short time 105 Service Program 106 Parameter setting Installation 108 Control via process control system 110 Uniclean 900 X diagnostics 147 Uniclean status 147 System forecast 148 Error messages of Uniclean 900 X 168 Overview of icons 209 ...

Page 212: ...g Program flows 70 Cleaning program 70 Calibration program 71 Park program 73 Service program 78 Parameter setting Installation 81 Control via process control system 83 Configuring media monitoring 86 Maintenance of Unical 9000 X Uniclean 900 X 137 Probe maintenance 137 Manual control 138 Single step control 139 Probe wear 140 Diagnostics of Unical 9000 X 146 Unical status 146 Unical network diagr...

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