Inficon HAPSITE Smart, Operating Manual

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HAPSITE Smart Operating Manual
3.7.1 Quick Reference SOP —
GC/MS Mode with HSS and Sample Loop in Portable Mode
1
From the Front Panel highlight Run Method , then press SEL .
2
Highlight GC/MS , then press SEL .
3
Select the Headspace folder from the GC/MS menu.
4
Select HSS 15 Min Loop method
5
Place the headspace needle in the 40mL vial that contains the sample.
6
When prompted, press the Run button on the front panel of the HAPSITE.
7
When prompted, place the headspace needle in the purge vial and press SEL .
8
Review results.
3.8 GC/MS Mode with Headspace Sampling System and
Concentrator in Portable Mode
This method is used for analyzing samples with concentration levels in the low part
per trillion range. This method is used when the loop method fails to detect a
chemical. Refer to
Chapter 6, Methods for additional information on GC/MS
methods.
CAUTION
The concentrator feature is designed to enhance
HAPSITE sensitivity when analyzing low concentration
samples. The accumulated sample VOCs are transferred
from the concentrator adsorbent bed to the HAPSITE as
a concentrated sample. Care should be taken to avoid
overloading the HAPSITE and causing excessive
carryover of VOCs in subsequent runs.
1
Refer to Chapter 13, Headspace Sampling System for more information on the
Headspace System. Refer to 2.6, HAPSITE Components and Assemblies for
assembly instructions.
2
Follow the instructions in Section 2.9.3, Installing the Tri-Bed Concentrator, on
page 2-29 or Section 2.9.4, Installing the Tenax or Carbopack Concentrator, on
page 2-31 to install the concentrator tube.
3
To cleanout out the concentrator tube, follow the instructions in Section 3.5.1,
Quick Reference SOP — Tri-Bed Concentrator Cleanout, on page 3-32 ; or
Section 3.6.1, Quick Reference SOP — Tenax Cleanout, on page
3-35
;depending on the type of concentrator installed.