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Summary of Contents for 5061-3378

Page 1: ... underutilized and idle equipment along with credit for buybacks and trade ins Custom engineering so your equipment works exactly as you specify Critical and expedited services Leasing Rentals Demos In stock Ready to ship TAR certified secure asset solutions Expert team I Trust guarantee I 100 satisfaction All trademarks brand names and brands appearing herein are the property of their respective ...

Page 2: ...0 Series Variable Wavelength Detector Installation and Maintenance Guide ABCDE HP Part No 79853 90009 Printed in FRG Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 3: ...see W arranty Statement in Chapter 5 For details of safety see Safety Information in Chapter 5 L The apparatus is marked with this symbol when the user should refer to the instruction manual in order to protect the apparatus against damage M Indicates dangerous voltages K Indicates a protected ground terminal Hewlett P ackard GmbH Hewlett P ackard Strasse 8 W 7517 Waldbronn 2 Federal Republic of G...

Page 4: ...ther error symptom Here you will be directed to Chapter 4 when it is necessary to replace a part Chapter 5 gives supplementary information about your detector What Other Handbooks Are Available Your detector comes complete with 2 further handbooks The User s Guide describes each of your detector s functions Getting it all Together is intended for chromatographic systems comprising only HP 1050 Ser...

Page 5: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 6: ...r 1 6 Removing the Locking Screws 1 7 Waste Drain 1 9 Solvent Inlet and Outlet 1 11 Analog Output 1 11 Remote Control 1 12 Line Voltage 1 14 Fuses 1 14 Power Cord 1 16 Ground Connector 1 17 Installing HP IB Board 1 17 Checking Out Your Detector 1 19 Preparing the Detector 1 20 Preparing the Pump 1 20 Preparing the Recording Device 1 20 Starting a Run 1 21 Contents 1 Artisan Technology Group Qualit...

Page 7: ...bance After Injection 3 8 Air Bubbles in Flow Cell 3 8 Removing Air Bubbles 3 9 4 Maintaining Your Detector Changing Deuterium Lamp 4 2 Stage 1 Removing Lamp 4 2 Stage 2 Inserting New Lamp 4 4 Stage 3 Calibrating Zero Order Light 4 4 Calibrating Wavelength Accuracy 4 5 Removing the Flow Cell 4 5 Cleaning Standard Flow Cell 4 6 Removing Standard Flow Cell 4 6 Disassembling Standard Flow Cell 4 6 Cl...

Page 8: ...oducts 5 1 Limitation of Warranty 5 2 Limitation of Remedies and Liability 5 3 Responsibilities of the Customer 5 3 Responsibilities of Hewlett P ackard 5 4 Safety Information 5 5 General 5 5 Operation 5 5 Safety Symbols 5 6 Solvent Information 5 9 Flow Cell 5 9 Solvents 5 9 Use of Solvents 5 10 Important 5 11 Acids 5 11 Bases 5 11 Salts 5 11 Organic Solvents 5 12 BuÀer Solutions 5 12 Degassing So...

Page 9: ...5 19 Response Time 5 19 Spectra 5 19 Light Source 5 20 Flow Cells 5 20 Control 5 20 Parameters 5 20 Analog Output 5 20 Communications 5 20 Safety Aids 5 20 Environment 5 20 Dimensions 5 20 Printing History 5 21 Your Comments Are Welcome 5 23 Your Comments Are Welcome 5 25 Index Contents 4 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 10: ...4 2 Position of Flow Cell Cassette Screws 4 5 4 3 Standard Flow Cell 4 6 4 4 Semi Micro Flow Cell 4 8 4 5 Preparative Flow Cell 4 10 4 6 High Pressure Flow Cell 4 12 Tables 1 1 Packing List 1 2 1 2 Accessories 1 3 1 3 Signal Cables 1 11 1 4 APG Remote Control Cables 1 12 1 5 APG Remote Control Connector Functions 1 13 1 6 Fuses 1 15 1 7 Integrator Scaling Factors 1 21 5 1 Warranty Services 5 4 Con...

Page 11: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 12: ...osen to install your detector meets requirements below Dimensions 325 mm 133 mm 545 mm 12 8 inch 5 2 inch 21 5 inch width height depth Leave adequate space at least 80 mm 3 inch at rear for access to connectors Weight 14 kg 31 lb Environment Temperature 5 to 55ΠC 40 to 131 ΠF Humidity 95 non condensing Line Power 100 to 120 V AC 10 or 220 to 240 V AC 10 Installing Your Detector 1 1 Artisan Techn...

Page 13: ... List Description Hewlett Packard Part Number Check Power cord as ordered Signal cable as ordered Remote cables as ordered Instruction kit handbooks 79853 90008 Leak interface kit 79853 68731 Start up kit including 79853 68701 One Pozidriv screwdriver 1 8710 0899 One wrench 1 4 and 5 16 inch 8710 0510 Three 2 amp fuses 2110 0002 Three 3 amp fuses 2110 0003 1 2 Installing Your Detector Artisan Tech...

Page 14: ...m lamp 79883 60002 Standard Õow cell stainless steel 79853 60008 Standard Õow cell titanium 79853 60011 Semi micro Õow cell stainless steel 79853 60010 High pressure Õow cell stainless steel 79853 60009 Preparative Õow cell titanium 79853 60012 Installing Your Detector 1 3 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 15: ...5 79853 68722 Cell screw 79853 27201 Cell rings pack of 2 79853 27202 Springs pack of 10 79853 27203 Parts for semi micro Õow cell Semi micro Õow cell kit including 2 windows 2 gaskets 1 and 2 gaskets 2 79853 68723 Windows quartz pack of 2 79853 68719 Gaskets 1 PTFE pack of 10 79853 68720 Gaskets 2 PTFE pack of 10 79853 68724 Cell screw 79853 27201 Cell rings pack of 2 79853 27202 Springs pack of ...

Page 16: ...ell Preparative Õow cell kit including 1 window 1 1 window 2 1 gaskets 1 4 gaskets 2 1 of each size and 1 gasket 3 79853 68725 Window kit including 1 window 1 and 1 window 2 79853 68726 Windows 1 quartz pack of 2 79853 68719 Gaskets 1 PTFE pack of 10 79853 68720 Gaskets 2 PTFE 1 of each size 79853 68727 Gaskets 3 PTFE pack of 5 79853 68732 Cell screw 79853 27201 Springs pack of 10 79853 27203 Comm...

Page 17: ...ector A TTENZIONE Assicuratevi che il cavo di alimentazione sia scollegato prima di installare il Variable Wavelength Detector WAARSCHUWING Zorg dat het netsnoer is losgekoppeld voordat de Variable Wavelength Detector wordt geinstalleerd Note If you have more than one HP 1050 Series module see Getting it all Together which recommends suitable arrangements of the diÀerent modules Each detector is i...

Page 18: ... spacers using a Pozidriv 1 screwdriver see Figure 1 1 Figure 1 1 Position of Locking Screws and Spacers 3 Screw locking screws and spacers in holes on rear panel as shown in Figure 1 2 You will need the screws and spacers again if you want to transport your detector Installing Your Detector 1 7 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 19: ... and Spacers Line power Switch Flow Cell Cassette Waste Outlet Leak Interface Keyboa rd Status Lamps Outlet Inlet Display Figure 1 3 Front of Detector 1 8 Installing Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 20: ...n in Figure 1 5 Waste Drain Lever Figure 1 5 Position of Waste Drain and Lever The waste line of your detector contains a small reservoir with a leak sensor thermistor to detect leaks When a leak is detected a shut down signal is sent from the REMOTE connector which is used to stop your pump Installing Your Detector 1 9 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www ...

Page 21: ...kann Losungsmittelabfall oder durch ein Leck austretendes Losungsmittel zu den elektronischen Teilen der Module gelangen CUID ADO Al apilar los m odulos aseg urese de que las superÃcies de apoyo del m odulo superior se asienten correctamente en la ranura del m odulo inferior Si los m oulos no est an bien alineados pueden penetrar sobrantes o fugas de disolvente en las partes electr onicas de los m...

Page 22: ... 2 Place the outlet capillary of the Õow cell in a suitable waste container Analog Output The ANALOG OUT connector provides either a 100 mV or a 1 V maximum signal output To select the output voltage use the control 11 function see User s Guide Check that you have the correct signal cable The part number is in a sheath around the cable Table 1 3 Signal Cables From Detector To Part Number Check HP ...

Page 23: ...a sheath around the cable Table 1 4 APG Remote Control Cables From Detector To Hewlett Packard Part Number Check Any HP 1050 Series module 5061 3378 HP 3390A Integrator 01046 60203 HP 3392A or HP 3393A Integrator 01046 60206 HP 3394A Integrator 01046 60210 HP 3396A Integrator 03394 60600 HP 18652A A D Converter 01046 60204 HP 35900A A D Converter 5061 3378 Universal 01046 60201 Push the metal plug...

Page 24: ...nals carried on each pin are shown in Table 1 5 The colors refer to wires of the remote cable part number 01046 60201 Table 1 5 APG Remote Control Connector Functions Pin Signal Wire Color Activity 1 Digital ground white none 2 Prepare run brown low 3 Start gray low 4 Shut down blue low 5 Not used pink none 6 Power on yellow high 7 Ready red high 8 Stop green low 9 Start request black low Installi...

Page 25: ...s connect e avant de changer la tension d alimentation A TTENZIONE Assicuratevi che il cavo di alimentazione sia scollegato prima di spostare il selettore di voltaggio WAARSCHUWING Zorg dat de voedingskabel losgekoppeld is voordat de voedingsspanning wordt veranderd To change setting 1 Insert tip of small screwdriver in slot on switch 2 Slide switch to correct position Fuses Check that the correct...

Page 26: ...vant de changer un fusible ATTENZIONE Assicuratevi che il cavo di alimentazione sia scollegato prima di installare o sostituire un fusibile WAARSCHUWING Zorg dat de voedingskabel losgekoppeld is voordat een zekering wordt geplaatst of vervangen To install a fuse 1 Loosen screw that secures power supply cover and remove cover 2 Use a screwdriver to push fuse cap inwards and then turn counterclockwi...

Page 27: ...erde verbindet sobald der Stecker in eine passende Steckdose gesteckt wird CUID ADO El Variable Wavelength Detector debe ser conectada a una toma de tierra para protegerle durante su operaci on El Variable Wavelength Detector y cualquier otro instrumento conectado a ella deben operar desde una fuente de energ a de tres contactos con el contacto de tierra conectado con certeza a tierra P dale a un ...

Page 28: ...r is aangesloten Schakel een elekticien in om te controleren of de voeding op de juiste wijze geaard is Ground Connector If you have a measuring instrument that has a safety ground connector connect the grounding cable from your instrument to the ground connector on the rear panel of your detector Installing HP IB Board The HP IB board allows communication between your detector and a ChemStation c...

Page 29: ...ne Bauteile auf der Karte an Legen Sie die Karte nicht auf PlastikoberÕ achen PRECA UCION La tarjeta contiene componentes electr onicos que son sensibles a las el ectricas No intente instalar esta tarjeta a no ser que utilize un equipo portable de puesta a tierra No toque ninguno de los componentes de la tarjeta No coloque la tarjeta sobre ninguna superÃcie de plastico o plastiÃcada AD VERTISSEMEN...

Page 30: ...om rear panel see Figure 1 4 3 Insert HP IB board and connect HP IB ribbon cable to J12 on DCB board 4 Replace detector top cover Checking Out Your Detector The noise and drift speciÃcations of your detector are 1 5 x 10 5 AU and 5 x 10 4 AU h respectively Note Allow a minimum time of one hour for the detector to stabilize before verifying the performance To check this speciÃcation you need a pump...

Page 31: ...TER ƒENTER ƒ ƒ ENTER 5 Set output voltage to 1 V press ƒCLEAR ƒCTRL ƒ 1 ƒ 1 ƒENTER ƒENTER ƒ 1 ƒENTER Preparing the Pump 1 Prime the pump and ensure there are no air bubbles in the system 2 Thoroughly degas about 300 ml of bidistilled water 3 Set pump to deliver bidistilled water at a Õow rate of 1 ml min Preparing the Recording Device 1 Set the attenuation to about 100 to 200 V full scale 2 Set an...

Page 32: ...The HP 3390A HP 3392A and HP 3393A have a full scale deÕection of 75 mm The HP 3394A and the HP 3396A have a full scale deÕection of 150 mm they also have an attenuation range between 8 and 36 Table 1 7 Integrator Scaling Factors Attenuation mV Full Scale mA U Full Scale 3 0 125 0 25 2 0 25 0 5 1 0 5 1 0 1 2 1 2 4 2 4 8 3 8 16 4 16 32 5 32 64 6 64 128 7 128 256 8 256 512 9 512 1024 10 1024 2048 In...

Page 33: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 34: ...ins installation instructions and information for accessories and upgrades Installing the Leak Interface High Pressure Flow Cells Installing Accessories 2 1 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 35: ...2 This page is intentionally blank 2 2 Installing Accessories Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 36: ...can occur This organization gets you to the source of a problem fast without having to read through long lists of error messages Whenever you must make a repair or replace a part we will reference the appropriate procedure in Chapter 4 Troubleshooting Your Detector 3 1 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 37: ...wn Turn on line power follow display ON YES message j displayed NO power cord NO connect connected power cord j YES contact Hewlett P ackard ROMTEST FIM failed at U4 ROM test failed Contact Hewlett P ackard RAMTEST CMP failed at XXXXH RAM test failed Contact Hewlett P ackard 3 2 T roubleshooting Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg c...

Page 38: ...tween pins 1 and 7 of the REMOTE connector The detector makes this connection for as long as the not ready condition exists When the not ready condition is removed the connection is broken and the detector operates again A not ready condition can pause automated operation which will only continue when the not ready condition is removed Troubleshooting During Operation The following errors messages...

Page 39: ...ng Deuterium Lamp in Chapter 4 N NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN DATA UNDERFLOW Flow cell window dirty Clean Õow cell window see Cleaning Standard Flow Cell in Chapter 4 NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN DATA OVERFLOW Flow cell incorrectly positioned Adjust Õow cell position NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN ADC DATA OVERFLOW Too much li...

Page 40: ...NNNNNNNNNNNNNNNN EEROM DATA LOST 1 Data lost from EEROM 1 NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN EEROM DATA LOST 2 Data lost from EEROM 2 NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN EEROM DATA LOST 3 Data lost from EEROM 3 NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN FILTER ERROR Beam cut Ãlter Troubleshooting the Chromatogram The quality of your chromatographic r...

Page 41: ...ution strength 4 Chemical reaction between sample and stationary phase Use another type of column Areas Not Reproducible Unstable Õow Check Õow system to improve Õow stability Gas bubbles in pump Shake all bubbles from solvent inlet Ãlters degas thoroughly and prime pump Leaks Disconnect detector and check pressure tightness of other modules Injection not reproducible Check performance of your inj...

Page 42: ...itable solvents or add a mechanical mixer Baseline Drift Non conditioned or new column Flush column with solvent of high elution strength Sample impurities that elute slowly Flush column with solvent of high elution strength Gradient with dirty or UV absorbing solvents Use pure solvents or change wavelength Leaks Disconnect detector and check pressure tightness of other modules Detector Õow cell c...

Page 43: ...lution strength than mobile phase Use solvent for sample with lower elution strength than mobile phase Excessive Baseline Disturbance After Injection High pressure drop after injection Check performance of your injector Air Bubbles in Flow Cell Before you start to check the other modules we recommend you check the Õow cell of your detector Air bubbles in the Õow cell are a common cause of chromato...

Page 44: ...ubbles from the Õow cell by increasing the Õow to 5 ml min Ensure that the maximum Õow cell pressure does not exceed 20 bar and the increased pressure does not aÀect your column If an air bubble is in the Õow cell the sample photocurrent is lowered because the light passes through the bubble so reducing the amount of light reaching the photodiode Using the control 16 function you can check the sam...

Page 45: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 46: ...ische Bauteile die gegen elektrostatische Entladung empÃndlich sind Verwenden Sie daher bei der Installation der Karte immer ein Elektrostatisches Erdungskit Teilenummer 9300 0794 Fassen Sie keine Bauteile auf der Karte an Legen Sie die Karte nicht auf PlastikoberÕ achen PRECA UCION La tarjeta contiene componentes electr onicos que son sensibles a las el ectricas No intente instalar esta tarjeta a...

Page 47: ...atsbare aardingsset onderdeelnummer 9300 0794 Geen van de componenten van het board mag ooit worden aangeraakt Het board mag nooit op een plastic of een met plastic gecoate ondergrond worden geplaatst Note Any adjustments calibrations or maintenance described in this handbook are not covered by warranty Changing Deuterium Lamp When as necessary Deuterium lamp part number 79883 60002 Stage 1 Removi...

Page 48: ...or Top Cover WARNING If detector has been in use the lamp may be hot If so wait for 5 to 10 minutes until lamp cools WARNUNG Wenn die Detektorlampe eingeschaltet war kann die Lampe sehr heiŸ sein Lassen Sie bitte die Lampe 5 bis 10 Minuten abk uhlen bevor Sie diese anfassen PRECA UCION Si el detector se ha estado usando la l ampara puede estar caliente Esp erese 5 10 minutes hasta que la l ampara ...

Page 49: ... Inserting New Lamp 1 Insert lamp into lamp housing and secure it with the screws 2 Connect lamp connector 3 Replace top cover Stage 3 Calibrating Zero Order Light 1 Turn on line power 2 Turn on lamp press ƒLAMP ON OFF ƒENTER 3 Select control function 20 to calibrate the zero order light of the grating Press ƒCTRL ƒ 2 ƒ 0 ƒENTER ƒENTER to display NNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNNN...

Page 50: ... to continue the calibration and then wait about 30 seconds 3 Press ƒENTER and the detector will store the step number in its electronic memory 4 Press ƒCLEAR Removing the Flow Cell When as necessary 1 Unscrew screws on Õow cell cassette and remove cassette see Figure 4 2 Screws Figure 4 2 Position of Flow Cell Cassette Screws Maintaining Your Detector 4 5 Artisan Technology Group Quality Instrume...

Page 51: ...ell 1 Cell screw 2 Spring 3 Ring 4 Gasket 1 5 Window 6 Gasket 2 7 Gasket 3 1 Unscrew cell screw using a Õat blade screwdriver see Figure 4 3 2 Remove springs O ring and gasket 1 using a pair of tweezers 3 Attach adhesive tape to window and remove window by lifting tape 4 6 Maintaining Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 52: ... gaskets supplied in standard Õow cell kit Reassembling Standard Flow Cell 1 Hold Õow cell cassette horizontally and place gasket 3 in position Ensure both cell holes can be seen through slot of gasket 3 2 Place gasket 2 on gasket 3 3 Place window on gasket 2 4 Place gasket 1 on window 5 Place ring on gasket 1 6 Place springs on ring Note Make sure conical springs point towards window Otherwise ti...

Page 53: ...Micro Flow Cell Figure 4 4 Semi Micro Flow Cell 1 Cell screw 2 Spring 3 Ring 4 Gasket 1 5 Window 6 Gasket 2 1 Unscrew cell screw using a Õat blade screwdriver see Figure 4 4 2 Remove springs ring and gasket 1 using a pair of tweezers 4 8 Maintaining Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 54: ...e cloth Note Replace old gaskets with new gaskets supplied in semi micro Õow cell kit Reassembling Semi Micro Flow Cell 1 Hold Õow cell cassette horizontally and place gasket 2 in position Ensure both cell holes can be seen through slot of gasket 2 2 Place window on gasket 2 3 Place gasket 1 on window 4 Place ring on gasket 1 5 Place springs on ring Note Make sure conical springs point towards win...

Page 55: ...ll 1 Cell screw 2 Spring 3 Ring 4 Gasket 1 5 Window 1 6 Gasket 2 7 Window 2 8 Gasket 3 1 Unscrew cell screw using a Õat blade screwdriver see Figure 4 5 2 Remove springs ring and gasket 1 using a pair of tweezers 3 Attach adhesive tape to window 1 and remove window by lifting tape 4 10 Maintaining Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg...

Page 56: ...n standard Õow cell kit Reassembling Preparative Flow Cell 1 Hold Õow cell cassette horizontally and place gasket 3 in position Ensure both cell holes can be seen through holes of gasket 3 2 Place window 2 on gasket 3 Ensure both cell holes can be seen through holes of window 2 3 Place gasket 2 on window 2 Ensure both cell holes can be seen through slit of gasket 2 4 Place window 1 on gasket 2 5 P...

Page 57: ...ing the Flow Cell Disassembling High Pressure Flow Cell Figure 4 6 High Pressure Flow Cell 1 Cell screw 2 Ring 3 Window 4 Gasket 1 5 Gasket 2 1 Unscrew cell screw using a Õat blade screwdriver see Figure 4 5 2 Remove ring using a pair of tweezers 4 12 Maintaining Your Detector Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 58: ...trasonic cleaner for several minutes dry them with a piece of lint free cloth Note Replace old gaskets with new gaskets supplied in standard Õow cell kit Reassembling High Pressure Flow Cell 1 Hold Õow cell cassette horizontally and place gasket 2 in position Ensure both cell holes can be seen through holes of gasket 2 2 Place gasket 1 on gasket 2 3 Place window on gasket 1 4 Place ring on window ...

Page 59: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 60: ...warranted from the installation date all others from the ship date If Buyer schedules or delays installation more than 30 days after delivery then warranty period starts on 31st day from date of shipment 60 and 61 days respectively for products shipped internationally HP warrants that its software and Ãrmware designed by HP for use with a CPU will execute its programming instructions when properly...

Page 61: ...n in eÀect only if the customer purchases additional inspection or installation services at the new site The foregoing warranty shall not apply to defects resulting from 1 Improper or inadequate maintenance adjustment calibration or operation by Buyer 2 Buyer supplied software hardware interfacing or consumables 3 Unauthorized modiÃcation or misuse 4 Operation outside of the environmental and elec...

Page 62: ...personnel 3 Access to and use of all information and facilities determined necessary by Hewlett P ackard to service and or maintain the products Insofar as these items may contain proprietary or classiÃed information the customer shall assume full responsiblity for safeguarding and protection from wrongful use 4 Routine operator maintenance and cleaning as speciÃed in the Hewlett P ackard Operatin...

Page 63: ...w of your country Please consult your local HP oŒce for the period of the warranty for shipping instructions and for the applicable wording of the local warranty 2 Warranty services are included as speciÃed for Analytical products and options purchased concurrently provided customer is located within a HP deÃned travel area HP warranty service provides for 8 am to 5 pm on site coverage Monday thro...

Page 64: ...s and devices connected to it must be connected to a protective earth via a ground socket Any interruption of the protective earth grounding will cause a potential shock hazard that could result in serious personal injury Whenever it is likely that the protection has been impaired the instrument must be made inoperative and be secured against any intended operation Make sure that only fuses with t...

Page 65: ...ng serious personal injury are present in this instrument Use extreme caution when handling testing and adjusting Safety Symbols Below you will Ãnd some symbols that are used on the instrument and throughout the documentation Symbol Description L The apparatus is marked with this symbol when the user should refer to the instruction manual in order to protect the apparatus against damage M Indicate...

Page 66: ...le une pr ecaution quant a une proc edure ou une pratique qui si elle n est pas correctement suivie peut r esulter en une blessure ou m eme en un risque pour la vie S assurer d avoir rempli toutes les conditions indiqu ees avant de continuer ATTENZIONE La scritta ATTENZIONE indica un pericolo Essa richiama l attenzione su una situazione che pu o portare a danni anche gravi per le persone Non prose...

Page 67: ...ION denota un riesgo Remite a un procedimiento o pr actica que de no ser llevada a cabo correctamente podr a resultar en un da no o destruccion parcial o total del equipo No continue cuando exista un signo de precauci on hasta que las condiciones indicadas hayan sido completamente entendidas y satisfechas A TTENTION Le signe ATTENTION d enote un risque Il appelle une pr ecaution quant a une proc e...

Page 68: ... Always Ãlter solvents small particles can permanently block the capillaries Avoid the use of the following steel corrosive solvents Solutions of alkali halides and their respective acids for example lithium iodide potassium chloride and so on High concentrations of inorganic acids like nitric acid sulfuric acid especially at higher temperatures replace if your chromatography method allows by phos...

Page 69: ...ith pH below 2 3 should not contain acids which attack stainless steel The materials in contact with the mobile phase include stainless steel titanium gold sapphire ruby quartz Ãlled TeÕon R Õ TeÕon R Õ and ceramic The HP 1050 Stainless Steel Series autosampler also contains a VESPEL R Õ rotor seal An optional TEFZEL R Õ rotor seal is available to extend the pH range to 12 5 The HP 1050 Ti Series ...

Page 70: ...ne TEA and phosphate buÀers generally cause no problems If you use solutions of pH 9 5 we recommend you replace the VESPEL R Õ rotor seal of the injection valve in the HP 1050 Stainless Steel Series with a TEFZEL R Õ rotor seal No modiÃcations are necessary with the HP 1050 Ti Series Solutions of pH 11 may also attack quartz impairing optical properties of Õow cells Salts Alkali halides for exampl...

Page 71: ...iments and look for precipitation Do not operate at or near the solubility limit determined in this way Oversaturated solutions are easily obtained in a batch experiment and will crystallize quickly on a suitable crystallization seed for example a capillary connection Moreover solubility might decrease with increasing temperature causing plugging of the capillaries in the heated parts of your chro...

Page 72: ...inbau der Option f ur die kontinuierliche Hinterkolbensp ulung Falls Sie ein Modul der Ti Serie t aglich verwenden ist es vertretbar die PuÀerl osung uber Nacht stehen zu lassen Vergewissern Sie Sich aber daŸ die WaschÕasche Losungsmittel enth alt Falls Module der Edelstahl oder Ti Serie f ur eine langere Zeit auŸer Betrieb sind sollten Sie die Losungsmittelkan ale mit destilliertem Wasser und dan...

Page 73: ...manent de piston Si le module HP 1050 Ti Series est utilis equotidiennement il est permis de le laisser pendant la nuit dans une solution saline ou une solution tampon Il convient cependant de contr oler dans ce cas que le r eservoir de rin ÿ cage de piston contienne un agent de rin ÿ cage Si les modules HP 1050 Stainless Steel ou Series Ti ne sont pas utilis es pour une dur ee prolong ee tous les...

Page 74: ...en regelmatig zoutoplossingen worden gebruikt adviseren wij de permanente afsluitspoelvloeistof optie te installeren Indien een moduul uit de HP 1050 Ti Serie dagelijks wordt gebruikt is het toegestaan deze gedurende de nacht in zout of een buÀer te laten liggen Wees er echter van overtuigd dat het afsluitspoelvloeistofreservoir voldoende spoeloplossinge bevat Indien de HP 1050 Stainless Steel of ...

Page 75: ...nd Measurement If test and measurement equipment is operated with equipment unscreened cables and or used for measurements on open set ups the user has to assure that under operating conditions the radio interference limits are still met within the premises Hersteller bescheinigung Hiermit wird bescheinigt dass dieses Ger at System in Ubereinstimmung mit den Bestimmungen von Postverf ugung 1046 84...

Page 76: ... operator position 70 dB Sound Pressure Lp 70 dB A At Operator Position Normal Operation According to ISO 7779 1988 EN 27779 1991 Type Test Hersteller bescheinigung Diese Information steht im Zusammenhang mit dem Anforderungen der Maschinenl arminformationsverordung vom 18 Januar 1991 Schalldruckpegel Lp 70 dB A Am Arbeitsplatz Normaler Betrieb Nach ISO 7779 1988 EN 27779 1991 Typpr ufung Suppleme...

Page 77: ...e Wavelength Detector conforms to the following product speciÃcations Safety IEC 348 CSA C22 2 No 151 EMC EN50082 1 1991 IEC 801 2 10kV AD IEC 801 3 3V m IEC 801 4 2kV power lines 1kV signal lines RFI EN 55011 Class B Group 1 Supplementary information Waldbronn December 1991 Location Date Signature QA Manager 5 18 Supplementary Information Artisan Technology Group Quality Instrumentation Guarantee...

Page 78: ...gth A ccuracy 2 nm Wavelength Reproducibility 0 3 nm Bandwidth 6 5 nm Linear Absorbance Range Better than 1 up to 1 5 AU using acetone at 254 nm Response Time 0 25 1 or 4 s 10 to 90 user selectable Spectra One spectrum at a time during a run scan rate 10 nm sec range from 190 to 600 nm selectable plotting speed selectable from 1 to 50 nm s background corrected spectrum Supplementary Information 5 ...

Page 79: ...e from 0 001 to 4 AU user selectable For integrator 100 mV for every 2 AU full scale or 1 V for every 2 AU full scale user selectable Communications Outputs ready signal and two external outputs one 24 V relay and one 100 Vmax contact closure both with 0 1 A Inputs and outputs start stop and shut down signals Optional interface for HP IB Safety Aids Extensive diagnostics error detection and displa...

Page 80: ... was printed on an HP LaserJet Series III printer and reproduced using standard oÀset printing techniques This handbook is for the C revision of the HP 1050 Series Variable Wavelength Detector and corresponds to model number 79853C see label on rear panel of detector VESPEL R Õ TEFZEL R Õ and TeÕon R Õ are registered trademarks of DuP ont Supplementary Information 5 21 Artisan Technology Group Qua...

Page 81: ...5 This page is intentionally blank 5 22 Supplementary Information Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 82: ...nically accurate Yes No Index 1 2 3 Are the instructions clear and complete Yes No Tabs 1 2 3 Are there enough examples and illustrations Yes No Glossary 1 2 3 Are concepts explained clearly Yes No Illustrations 1 2 3 Examples 1 2 3 Readability 1 2 3 Comments Name Title Company A ddress Country Phone Please tear out and mail in HP 1050 Series Variable Wavelength Detector Installation and Maintenan...

Page 83: ... Learning Products Group Hewlett P ackard Strasse 8 W 7517 Waldbronn 2 Federal Republic of Germany Fold here Fold here 5 24 Supplementary Information Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 84: ...te Yes No Index 1 2 3 Are the instructions clear and complete Yes No Tabs 1 2 3 Are there enough examples and illustrations Yes No Glossary 1 2 3 Are concepts explained clearly Yes No Illustrations 1 2 3 Examples 1 2 3 Readability 1 2 3 Comments Name Title Company A ddress City and State Country Postal Code Phone Please tear out and mail in HP 1050 Series Variable Wavelength Detector Installation ...

Page 85: ...5 Fold here Fold here 5 26 Supplementary Information Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 86: ...led water 1 19 D DAC TROUBLE 3 5 data underÕow 3 4 deuterium lamp 1 5 4 2 display 1 9 drift speciÃcations 1 19 E EEROM DATA LOST 3 5 environment 1 1 error messages 3 3 F FIL TER ERROR 3 5 Õow cell 2 1 5 9 Õow cell cassette 1 9 fuses 1 9 1 14 Index 1 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 87: ... 4 leak detected 3 4 leak interface 1 9 1 10 2 1 leak sensor 1 10 line power 1 1 line power socket 1 9 line power switch 1 9 line voltage selector 1 14 locking screw 1 8 low illumination 3 4 M micro Õow cell 1 5 N noise speciÃcations 1 19 not ready conditions 3 3 O outlet capillary 1 9 1 11 output voltage 1 11 Index 2 Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www ar...

Page 88: ... 2 S safety 5 5 symbols 5 6 safety ground connector 1 17 sawtooth baseline 3 9 self tests 3 2 SENSOR TROUBLE 3 5 solvents 5 9 spiking 3 9 spring 4 6 4 8 4 10 4 12 standard Õow cell 1 5 status lamps 1 9 T thermistor 1 10 transportation 1 8 V VOLTAGE ERROR 3 5 voltage selection switch 1 9 W warranty 5 1 waste drain 1 9 waste outlet 1 9 window 4 6 4 8 4 10 4 12 W SET ERROR 3 5 Index 3 Artisan Technol...

Page 89: ...Artisan Technology Group Quality Instrumentation Guaranteed 888 88 SOURCE www artisantg com ...

Page 90: ...quipment Have surplus equipment taking up shelf space We ll give it a new home Learn more Visit us at artisantg com for more info on price quotes drivers technical specifications manuals and documentation Artisan Scientific Corporation dba Artisan Technology Group is not an affiliate representative or authorized distributor for any manufacturer listed herein We re here to make your life easier How...

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