Hanna Instruments HI 83205 Instruction Manual Download Page 6

10

11

Pay attention to push the cuvette completely down in the holder.

• In order to avoid reagent leaking and to obtain more accurate measure-

ments, close the cuvette first with the supplied HDPE plastic stopper 
and then the black cap.

• Each time the cuvette is used, the cap must be tightened to the same degree.
• Whenever the cuvette is placed into the measurement cell, it must be dry

outside, and free of fingerprints, oil or dirt. Wipe it thoroughly with

HI 731318

  or a lint-free cloth prior to insertion.

• Shaking the cuvette can generate bubbles in the sample, causing higher

readings. To obtain accurate measurements, remove such bubbles by
swirling or by gently tapping the cuvette.

• Do not let the reacted sample stand too long after reagent is added, or

accuracy will be lost.

• It is possible to take multiple readings in a row, but it is recommended to

take a new zero reading for each sample and to use the same cuvette for

zeroing and measurement when possible (for most precise results follow the
measurement procedures carefully).

• Discard the sample immediately after the reading is taken, or the glass might become permanently

stained.

• All the reaction times reported in this manual are at 20°C (68°F). As a general rule of thumb, they

should be doubled at 10°C (50°F) and halved at 30°C (86°F).

REAGENT BLANK CORRECTION

• Some methods require a “reagent blank correction”. The blank and the sample are prepared exactly

in the same way, only the blank is deionized water instead of sample.
A blank cuvette may be used more than once: stability and storing conditions are described for each
method in the related chapter.

INTERFERENCES

• In the method measurement section the most common interferences that may be present in an average

wastewater matrix have been reported. It may be that for a particular treatment process other
compounds do interfere with the method of analysis.

METHOD REFERENCE TABLE

HI 83205 - BOILERS & COOLING TOWERS

Method

Method

Page

description

1

Aluminum

17

2

Ammonia MR

19

3

Ammonia LR

21

      4

Bromine

23

5

Free Chlorine

25

6

Total Chlorine

28

7

Chlorine Dioxide

31

8

Chromium VI HR

34

9

Chromium VI LR

36

10

Copper HR

38

11

Copper LR

40

12

Hydrazine

42

Method

Method

Page

description

13

Iron HR

44

14

Iron LR

46

15

Molybdenum

49

16

Nitrate

52

17

Nitrite HR

54

18

Nitrite LR

56

19

Dissolved Oxygen

58

20

pH

60

21

Phosphate HR

62

22

Phosphate LR

64

23

Silica

66

24

Zinc

69

HEALTH & SAFETY

The chemicals contained in the reagent kits may be hazardous if improperly handled. Read the
Material Safety Data Sheet (MSDS) before performing tests.

Safety equipment:  Wear suitable eye protection and clothing when required, and follow instructions carefully.
Reagent spills: If a reagent spill occurs, wipe up immediately and rinse with plenty of water.
If reagent contacts skin, rinse the affected area thoroughly with water. Avoid breathing released vapors.

Summary of Contents for HI 83205

Page 1: ...1 Instruction Manual HI 83205 Multiparameter Bench Photometer for Boilers and Cooling Towers w w w h a n n a i n s t c o m This Instrument is in Compliance with the CE Directives...

Page 2: ...0 Windows Compatible Software helps users manage all their results Dear Customer Thank you for choosing a Hanna product Please read this instruction manual carefully before using the instrument This m...

Page 3: ...are optically identical to provide the same measurement conditions Most of methods use the same cuvette for both so it is important that measurements take place in the same optical point The instrumen...

Page 4: ...elect method menu Press to move up in a menu or a help screen to increment a set value to access second level functions Press to move down in a menu or a help screen to decrement a set value to access...

Page 5: ...mounts may cause interference they should be removed by treatment with active carbon and filtration Ensure the cuvette is filled correctly the liquid in the cuvette forms a convexity on the top the bo...

Page 6: ...ods require a reagent blank correction The blank and the sample are prepared exactly in the same way only the blank is deionized water instead of sample A blank cuvette may be used more than once stab...

Page 7: ...g and deleting You can view and delete the data log by pressing the RCL key Deleting is based on the LIFO last in first out scheme Additionally you can delete the data records all at once CHEMICAL FOR...

Page 8: ...n enabled a short beep is heard every time a key is pressed A long beep alert sounds when the pressed key is not active or an error condition is detected Press the functional key to enable disable the...

Page 9: ...05 offers an interactive contextual help mode that assists the user at any time To access help screens pressHELP The instrument will display additional information related to the current screen To rea...

Page 10: ...into the holder and close the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measurement AMMONIA MEDIUM RANGE Aluminum Add the content of one packet of HI 93712C 0...

Page 11: ...ide various aliphatic and aromatic amines Ammonia LR SPECIFICATIONS Range 0 00 to 3 00 mg L Resolution 0 01 mg L Accuracy 0 04 mg L 4 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten l...

Page 12: ...se the lid Press ZERO key The display will show 0 0 when the meter is zeroed and ready for measurement 10 mL Ammonia LR Remove the cuvette Add 4 drops of HI 93700A 0 First reagent 6 drops for seawater...

Page 13: ...tte with 10 mL of unreacted sample up to the mark and replace the cap Place the cuvette into the holder and close the lid Free Chlorine FREE CHLORINE 10 mL Remove the cuvette and add the content of on...

Page 14: ...ey The meter will show 0 0 when the meter is zeroed and ready for measurement Remove the cuvette Powder reagents procedure Add the content of one packet of HI 93701 0 DPD reagent Replace the cap and s...

Page 15: ...instrument x 3 x 3 x 1 Total Chlorine TOTAL CHLORINE SPECIFICATIONS Range 0 00 to 3 50 mg L Resolution 0 01 mg L Accuracy 0 03 mg L 3 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten l...

Page 16: ...rk with the sample Add 0 5 mL of HI 93738A 0 Chlorine Dioxide Reagent to each cylinder 1 2 close them and invert several times to mix 2 25 ml 1 25 ml 1 2 1 2 Press TIMER and the display will show the...

Page 17: ...t above 25 C 78 F agitation and exposure to light must be avoided INTERFERENCES Interferences may be caused by strong oxidants 10 mL 2 2 Chlorine Dioxide 1 Add the content of one packet of HI 93738B 0...

Page 18: ...g L Accuracy 5 g L 4 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the ASTM Manual of Water and Environmental Tech...

Page 19: ...g L Accuracy 1 g L 4 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 525 nm Method Adaptation of the ASTM Manual of Water and Environmental Techn...

Page 20: ...5 00 mg L Resolution 0 01 mg L Accuracy 0 02 mg L 4 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the EPA meth...

Page 21: ...0 to 1000 g L Resolution 1 g L Accuracy 10 g L 5 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the EPA method The r...

Page 22: ...sten lamp with narrow band interference filter 420 nm Method Adaptation of the ASTM Manual of Water and Environmental Technology method D1385 88 p Dimethylaminobenzaldehyde method The reaction between...

Page 23: ...rference filter 525 nm Method Adaptation of the EPA Phenantroline method 315B for natural and treated waters The reaction between iron and reagents causes an orange tint in the sample REQUIRED REAGENT...

Page 24: ...IONS Range 0 to 400 g L Resolution 1 g L Accuracy 10 g L 8 of reading Typical EMC 1 g L Deviation Light Source Tungsten lamp with narrow band interference filter 575 nm Method Adaptation of the TPTZ M...

Page 25: ...ccessories see page 73 MEASUREMENT PROCEDURE Select the Molybdenum method using the procedure described in the Method Selection section see page 12 Fill the cuvette with 10 mL of unreacted sample up t...

Page 26: ...r above 10 mg L Iron above 50 mg L Nickel above 50 mg L Nitrite as NO2 Sulfate above 200 mg L Highly buffered samples or with extreme pH may exceed the buffering capacity of the reagents Fill one grad...

Page 27: ...amines Chloride above 100 ppm Chlorine above 2 ppm Copper Iron III Strong oxidizing and reducing substances Sulfide must be absent Nitrate SPECIFICATIONS Range 0 0 to 30 0 mg L Resolution 0 1 mg L Ac...

Page 28: ...sten lamp with narrow band interference filter 575 nm Method Adaptation of the Ferrous Sulfate method The reaction between nitrite and the reagent causes a greenish brown tint in the sample REQUIRED R...

Page 29: ...Nitrite LR SPECIFICATIONS Range 0 00 to 0 35 mg L Resolution 0 01 mg L Accuracy 0 02 mg L 4 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp with narrow band interference filter...

Page 30: ...eading Typical EMC 0 1 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 420 nm Method Adaptation of the Standard Methods for the Examination of Water and Wastewater 18th...

Page 31: ...scription Quantity HI 93710 0 Phenol Red Indicator 5 drops REAGENT SETS HI 93710 01 Reagents for 100 pH tests HI 93710 03 Reagents for 300 pH tests For other accessories see page 73 MEASUREMENT PROCED...

Page 32: ...RANGE SPECIFICATIONS Range 0 0 to 30 0 mg L Resolution 0 1 mg L Accuracy 1 mg L 4 of reading Typical EMC Dev 0 1 mg L Light Source Tungsten lamp with narrow band interference filter 525 nm Method Ada...

Page 33: ...cy 0 04 mg L 4 of reading Typical EMC Dev 0 01 mg L Light Source Tungsten lamp with narrow band interference filter 610 nm Method Adaptation of the Ascorbic Acid method The reaction between phosphate...

Page 34: ...mg L Accuracy 0 03 mg L 3 of reading Typical EMC 0 01 mg L Deviation Light Source Tungsten lamp with narrow band interference filter 610 nm Method Adaptation of the ASTM Manual of Water and Environme...

Page 35: ...HI 93731 01 Reagents for 100 tests HI 93731 03 Reagents for 300 tests For other accessories see page 73 MEASUREMENT PROCEDURE Select the Zinc method using the procedure described in the Method Select...

Page 36: ...be caused by Aluminum above 6 mg L Cadmium above 0 5 mg L Copper above 5 mg L Iron above 7 mg L Manganese above 5 mg L Nickel above 5 mg L Zinc Place the cap and insert the cuvette into the instrumen...

Page 37: ...eropolyBlue Zinc 0 00 to 3 00 mg L Zincon ACCESSORIES REAGENT SETS HI 93700 01 100 ammonia LR tests HI 93700 03 300 ammonia LR tests HI 93701 01 100 free chlorine tests powder HI 93701 03 300 free chl...

Page 38: ...r Service Center nearest to you To find the Hanna Office in your vicinity check our home page at www hannainst com RecommendationsforUsers Before using these products make sure that they are entirely...

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