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StamoLys CA 71 MN

Trouble-shooting

Hauser

37

9.3

Process errors without messages

Error message

Possible cause

Tests and / or corrective measures

Measured values 
always the same

Reagents 
contaminated or aged

Simple check: Add about 20 ml of standard solution with about 1 ml of reagent in a vessel. If it 
does not change colour after max. 10 min, replace the reagents .

No sample, no 
reagents

Make sure sample and reagents are supplied, check level monitor and clean if necessary

System blocked

Flush with 12.5% bleaching lye (monthly maintenance)

Measured values 
inaccurate

Incorrect 
concentration of 
standard 

Check the concentration in the laboratory. Adjust the standard accordingly 
("PARAMETER ENTRY", "Calibration solution") or replace the standard.

Reagents 
contaminated or aged

Simple check: Add about 20 ml of standard solution with about 1 ml of reagent in a vessel. If it 
does not change colour after max. 10 min, replace the reagents.

Reagent blank value 
too high

After replacing the reagents, carry out an offset calibration and then a calibration 
(CONFIGURATION, "Offset calibration")

Wrong dimension

Check the setting in the CONFIGURATION menu, "Measuring unit".

Wrong optical cell

Check the setting in the CONFIGURATION menu, "Photometer"

Sample suction time 
too short

Increase the suction time (CONFIGURATION, "Delay to sample")

Matrix effects
(substances that 
interfere with the 
photometric methods)

Detect interfering substances (see Technical Information, "Measuring principle"), 
possibly use sample conditioning

Standard is dosed to 
the sample

Check the valves and valve settings. Replace valve hoses if necessary.

Filter life too long

Take counter sample at analyzer inlet and check the concentration in the laboratory. If the 
analyzer measured values have no deviations, clean ultrafiltration modules or backflush filters 
more frequently.

System block or 
contaminated

Flush with 12.5% bleaching lye (monthly maintenance)

Dosing

Replace pump hoses.

Optical cell dirty

Flush with 12.5% bleaching lye first and then with 5% hydrochloric acid

Counter sample in the 
laboratory delivers 
deviating measured 
values

Sample ageing

Shorten time between sampling and analysis.

Measured value 
transfer errored

Wrong size of analog 
output

Check the setting (CONFIGURATION, "Analog output 1"  " 2").

Incorrect measuring 
range

Adjust measuring range (PARAMETER ENTRY, "Measuring range")

Background noise

Check line for interference from strong sources of induction.

Analyzer will not 
switch on

No power

Check the electrical connection and ensure power supply.

Fuse

Replace fuse F1 (time-lag 0.5 A)

Analyzer is running 
but display reading is 
garbled or off

Initialisation failed

Switch the analyzer off and after approx. 30 seconds back on.

Pumps fail to run

Leak

See "Spillage error" error message

Leak sensor 
bypassed

Interrupt contact between two leak sensors (pins 67-66)

Fuse

Check all fuses and replace if necessary.

Pump defective

E+H-Service

Measurement does 
not start

Leak on photometer

E+H-Service

Summary of Contents for StamoLys CA 71 MN

Page 1: ...Quality made by Endress Hauser ISO 9001 BA 363C 07 en 01 03 51512330 Valid of Software version 5 0 StamoLys CA 71 MN Manganese Analyzer Operating Instructions...

Page 2: ......

Page 3: ...eration 20 5 4 Calibration 27 6 Commissioning 29 6 1 Function check 29 6 2 Switch on 29 7 Maintenance 31 7 1 Maintenance schedule 31 7 2 Replacing reagents 32 7 3 Replacing pump hoses 33 7 4 Replacing...

Page 4: ...rical cables and hose connections are not damaged Do not operate damaged products and secure them against unintentional commissioning Mark the damaged product as being defective Measuring point faults...

Page 5: ...symbol alerts you to hazards They can cause serious damage to the instrument or to persons if ignored Caution This symbol alerts you to possible faults which could arise from incorrect operation They...

Page 6: ...cation Sample transfer 1 Sample transfer from one measuring point one channel version 2 Sample transfer from two measuring points two channel version Power supply 0 Power supply 230 V AC 50 Hz 1 Power...

Page 7: ...6 4 x 3 2 mm 0 25 x 0 12 an interference suppressor for the current output 4 edge covers a quality certificate Operating Instructions english Note Reagents please order separately 2 3 Certificates and...

Page 8: ...eck that the scope of delivery is complete and agrees with your order and the shipping documents The packaging material used to store or to transport the product must provide shock protection and humi...

Page 9: ...11 08 00 xx 001 eps Fig 4 Collecting vessel at analyzer optionally 1 Ventilation 2 Sample inlet from sampling 3 Collecting vessel 4 Electrical connections 5 Analyzer sample inlet C07 CA71xxx 06 08 02...

Page 10: ...n or no adjusting pin Fig 6 and Fig 7 position 2 2 Pull the marked pipe position 3 downwards due to your application 1 2 or 3 analyzers E H Collecting vessel at CA 71 with or without level measurement...

Page 11: ...age treatment plant From a sedimentation tank or after microfiltration this is practical for media containing flocculants e g in an activated sludge basin Sample conditioning using ultrafiltration for...

Page 12: ...ple available for both analyzers Observe this when selecting maintenance intervals for CAT 430 and when setting the buffer volume on the collecting vessel C07 CA71xxx 11 08 00 xx 007 eps Fig 9 Install...

Page 13: ...onnel must have read and understood the instructions in this manual and must adhere to them Ensure before beginning the connection work that there is no voltage at the power cable 4 1 1 Quick wiring g...

Page 14: ...y To start measurement the voltage must stay at 0 V for at least 5 seconds Function Designation Terminal without cooling device Terminal with cooling device Mains L 3 3 N 2 2 PE 1 1 Alarm value 1 chan...

Page 15: ...l version place the cable cores of all cables data cables to analog output 1 and to analog output 2 through the interference suppressor 4 2 2 One channel version C07 CA71xxx 03 08 00 xx 001 eps Fig 12...

Page 16: ...ult Retrieves error message using operation menu Channel or measurement end1 1 Alternative selection Displays active channel Displays Measurement finished 5 s Analog output l 1 channel 1 0 or 4 mA mea...

Page 17: ...g commands can be sent from the PC in order to read out data D Data memory Measured values C Data memory Calibration factors S Setup parameter entry configuration F Frequency current Connection Termin...

Page 18: ...e check the terminal assignment for analogue output 1 or 2 Device status and specifications Note Is the analyzer or cable externally undamaged Visual inspection Electrical connection Note Does the sup...

Page 19: ...rial interface RS 232 4 Operating keys and control LEDs 5 3 Local operation The operating keys and the integrated indicator LEDs have the following functions RS 232 ENDRESS HAUSER STAMOLYS CA 71 M CE...

Page 20: ...as not yet expired Note Measuring flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample collector or the sample conditioning unit Selec...

Page 21: ...he standard see PARAMETER ENTRY calibration solution The deviation results from factors such as reagent ageing ageing of constructive components etc The calibration factor compensates for these effect...

Page 22: ...er contact for alarm value 2 channel 1 works as NO current or NC current contact Alarm value AV 1 2 Two channel version only Setting for whether contact for alarm value 1 channel 2 works as NO current...

Page 23: ...teresis 2 of alarm value Alarm value AV 2 1 MN A 1 150 g l 150 g l MN B 10 2000 g l 2000 g l Concentration threshold value limit relay 2 channel 1 differential hysteresis 2 of alarm value Alarm value...

Page 24: ...on Recommended calibration interval of 48 72 h Calibration solution MN A 1 150 g l 100 g l MN B 10 2000 g l 500 g l Concentration of the calibration standard Select a standard whose concentration is i...

Page 25: ...y to enter the menu Option Display Info Pumps and valves Virtual switching board Various valve and pump combinations can be selected The setting options are Valve 1 P sample or S standard Pump 1 and p...

Page 26: ...ncentration measured values with date and time If there are no values available Empty set appears Browse through the data sets by pressing the Vand Wkeys Serial output You can output all data sets in...

Page 27: ...calibration is now carried out automatically Caution After the calibration has finished the analyzer automatically goes into measuring mode You now have to set the time of the 1st calibration back int...

Page 28: ...nfigured and calibrated the measuring cycle starts automatically Entering parameters is no longer necessary To perform initial start up or to readjust the device parameters proceed as follows 1 Plug i...

Page 29: ...R or S with V and then switch the P1 sample pump on Leave the pump running until you can tell that there is cleaning agent at the T connector Switch P1 back off 7 Now switch the valves to passage for...

Page 30: ...f the reagents Period of time Duty Note weekly Check and note calibration factor for service purposes CONFIGURATION every 2 weeks Check concentration of the calibration standard in the laboratory Adju...

Page 31: ...ee Trouble shooting instructions the reagents are too old the reagents have been spoilt by incorrect storage conditions or environmental influences Reagents check a Check the standard solution concent...

Page 32: ...the reagent canisters in order to prevent contamination of the reagents 4 Loosen the hose cassette Now you can remove the hoses 5 Replace the new pump hoses in the reverse sequence of operations Do no...

Page 33: ...left of the mixer 4 Remove the old mixer from the clip and insert the new one 5 Connect the new mixer to the hoses again 6 Attach the photometer housing and screw it down 7 After installation refill...

Page 34: ...er housing proceed as follows Stainless steel housing stainless steel SS 1 4301 AISI 304 with a lint free cloth and Glittol RG 10 51 GFR housing with a damp cloth or with tenside based alkaline cleani...

Page 35: ...olution 0 1 mg l Mn order no CAY845 V10C10AAE Standard solution 0 5 mg l Mn order no CAY845 V10C50AAE Note Please note the disposal instructions in the safety data sheets of the reagents 8 3 Hose clea...

Page 36: ...ngly PARAMETER ENTRY Calibration solution or replace the standard Reagents contaminated or aged Simple check Add about 20 ml of standard solution with about 1 ml of reagent in a beaker If it does not...

Page 37: ...tric methods Detect interfering substances see Technical Information Measuring principle possibly use sample conditioning Standard is dosed to the sample Check the valves and valve settings Replace va...

Page 38: ...he current date Interval not expired or 0 h Change parameters Leak on Photometer Device or discharge blocked Remove blockage E H Service Blockage deposits in device Water hardness Lime deposits can by...

Page 39: ...mple collector 51504114 122 Hose made of C Flex 6 4 mm 51504115 123 Hose made of C Flex 1 5 mm 51512535 130 Hose adapter 1 6 mm x 1 6 mm 51506495 131 Hose adapter T 1 6 mm x 1 6 mm x 1 6 mm 51506490 1...

Page 40: ...m Contacts 2 limit contacts per channel 1 system alarm contact optionally end of measurement with two channel version display of channel no available Load max 500 Serial interface RS 232 C Load capaci...

Page 41: ...e selectable from 20 to 300 s standard 80 s Rinse again time 30 s Filling time 25 s Maintenance interval 6 month typically Servicing requirements 15 minutes week typically Ambient temperature 5 40 C 4...

Page 42: ...sample Deutsch English Fran ais Italiano Nederlands Suomi Magyar Polski Error messages Pumps and valves Frequency Mixture Measured values Output Clear data Measuring range start Alarm value 1 Calibra...

Page 43: ...ys CA 71 MN Appendix Endress Hauser 43 Analog output Alarm value 1 Alarm value 2 Error contact act Date time Frequency offset Standard solution Flushing interval Flushing time 1st Flushing Calibrate o...

Page 44: ...s Suomi Magyar Polski Error messages Pumps and valves Frequency Mixture Measured values Output Clear data Measuring range start1 Calibration Measuring Flushing Waiting PARAMETER ENTRY AUTO MEASURING L...

Page 45: ...m value 1 2 Calibration solution 1st Flushing act Date time Frequency offset Calibrate offset Error contact Alarm value 2 2 Alarm value 2 1 Analog output 2 Flushing interval Flushing time n Channel 1...

Page 46: ...nactive 1 l MN1 MN2 MN3 each CAY844 V10AAE Cleaning agent 1 l CAY845 V10C10AAE Standard solution 0 1 mg l Mn CAY845 V10C50AAE Standard solution 0 5 mg l Mn Chemicals for Ultra filtration Quantity Orde...

Page 47: ...7 5 m C Flex hose ID 6 4 mm 51504115 123 1 m C Flex hose ID 1 5 mm 51512535 130 10 Hose adapter 1 6 mm x 1 6 mm 51506495 131 10 Hose adapter T 1 6 mm x 1 6 mm x 1 6 mm 51506490 132 10 Hose adapter 3 2...

Page 48: ...output 0 20 mA 4 20 mA AV 1 normally closed normally open AV 2 normally closed normally open Fault signal normally closed normally open Frequency offset Hz Ground line demineralised water without reag...

Page 49: ...gain Filling time Reaction time U min K floating mean N Points C1 mg l g l F 1 Hz C2 mg l g l F 2 Hz C3 mg l g l F 3 Hz C4 mg l g l F 4 Hz C5 mg l g l F 5 Hz C6 mg l g l F 6 Hz C7 mg l g l F 7 Hz C8 m...

Page 50: ...ith pressurised water disposable syringe Remove hose holder unit from the pump Done KW 1 KW 3 KW 5 KW 7 KW 9 KW 11 KW 13 KW 15 KW 17 KW 19 KW 21 KW 23 Date Done KW 25 KW 27 KW 29 KW 31 KW 33 KW 35 KW...

Page 51: ...StamoLys CA 71 MN Appendix Endress Hauser 51...

Page 52: ...Appendix StamoLys CA 71 MN 52 Endress Hauser...

Page 53: ...s 6 safety symbols 6 Incoming acceptance 9 Input 41 Installation 5 9 12 Examples 13 Interference suppressor 16 L LANGUAGE 26 M Main menu 21 Maintenance 31 Schedule 31 Mechanical construction 42 Menu A...

Page 54: ...reening 16 Serial interface 18 SERVICE 26 Signal connection 16 Spare parts 39 Standard solution 36 Storage 9 Switching contacts 17 Switch on 29 Symbols 6 T Technical data 41 42 Terminal assignment 15...

Page 55: ...f health o biological hazardous o inflammable o safe Please mark the appropriate warning hints 5HDVRQ IRU UHWXUQ BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB BBBBBBBBBBB...

Page 56: ...San Jose Euro Tec Costa Rica S A Tel 2 20 28 08 Fax 2 96 15 42 Ecuador Quito Insetec Cia Ltda Tel 02 2 26 91 48 Fax 02 2 46 18 33 El Salvador San Salvador Automatizacion y Control Industrial de El Sal...

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