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Spare Parts

Waltron User Manual 101-016-B.3

3041 Silica Analyzer

SPARE PARTS

Table 10.1: Routine Maintenance Parts Listing.

Description

Part Number

Annual Consumables Kit

W3040-101

Pinch Valve Drain Tubing

W3040-055

Sample Pump Tubing

W3040-046

Sample Line Tubing

W3040-099

Colorimetric Cell O-Ring

W3040-074

Peristaltic Reagent Pump Kit (tubing, fittings, rollers)

W3040-091

Table 10.2: Standards and Reagents Parts Listing.

Description

Part Number

Silica Reagent #1

W1234-096E

Silica Reagent #2

W1234-097E

Silica Reagent #3

W1234-098E

Silica Calibration Standard (200 ppb)

W1234-099E

Table 10.3: Spare Parts Listing.

Description

Part Number

Pump Head 7016

– Sampling Pump

W9040-007

Pump motor 70-80 rpm 24 Vdc

W3040-015

External Reservoir - Fast loop with level switch

W3040-003

Peristaltic pump for reagents

W3040-057

Reaction quartz cell 26 mm

W3040-006A

Reaction quartz cell 16 mm

W3040-005A

Adapter for 16 mm reaction cell

W3040-126

Reaction cell block

W3040-117

Heater

W3040-009

Mixing pump

W3040-013A

Drain Pinch Valve

W3040-014

Flowcell Cap with Tubing and Fittings (3 Reagents)

W3040-056

3 Ways Valve (D351)

W3040-096

Sample Selection Block with 1 Valve (Single Stream Unit)

W3040-064

Sample Selection Block with 2 Valves (Dual Stream Unit)

W3040-065

Power supply

– 24 Vdc

W3040-021

Touchscreen

W3040-022A

Preamplifier photometer board

W3040-026

Led 850 nm

W3040-331

Electronics, Complete

W3040-097

Содержание 3041

Страница 1: ...101 016 B 3 EXPERTS IN WATER CHEMISTRY SINCE 1903 3041 Silica Analyzer User Manual...

Страница 2: ...5546 www waltron net Please be ready to provide the following information Date analyzer was purchased Analyzer model and serial number Recent maintenance history Calibration slope values and detailed...

Страница 3: ...iners packages and chemicals Only qualified personnel should be involved in the installation operation and servicing of the analyzer Follow safety precautions when operating analyzer in conditions of...

Страница 4: ...al Service Department Customer name address and department Name and telephone number of the individual responsible for returning items for repair Brief problem description Ship to Waltron service cent...

Страница 5: ...g and shipping needs Check all items received against those on the packing list Chemicals are usually shipped in a separate package and will be itemized accordingly Verify that the number of packages...

Страница 6: ...1 2 1 General Information 10 1 2 2 List of Warnings and Potential Dangers 11 1 2 3 Reagents 12 1 2 4 Sample 12 1 2 5 Waste Disposal 12 1 2 6 Analyzer General Hazards 12 2 Introduction 15 2 1 Analyzer...

Страница 7: ...2 Chart 35 5 6 3 Manual Step 35 5 7 Data Logger 36 5 7 1 Save to USB 36 5 8 Program Menu 37 5 8 1 Settings Menu 37 5 8 2 Calibration Menu 38 5 9 Service Menu 39 6 Operation 40 6 1 Reagents Prime 40 6...

Страница 8: ...3 2 Reccomended complete system installation 26 Figure 3 3 Electrical connections for user connections and power connections 28 Figure 3 4 Mounting schematics for the reagent holding bracket 29 Figur...

Страница 9: ...etermination 18 Table 3 1 Terminal block pin locations 28 Table 5 1 User password 31 Table 5 2 Menu access level with password 31 Table 5 3 Analyzer operating statuses 32 Table 5 4 Main menu button de...

Страница 10: ...or 4 configurable alarm relays Reproducibility 1 ppb or 2 of reading whichever is greater Degree of Protection IP55 NEMA 4 Wet section IP65 NEMA 4x Electronics Required Maintenance Monthly replenish r...

Страница 11: ...ritten on this manual The user has the responsibility to read and understand the information contained in this manual and to abide by all applicable employee health and safety regulations Use maintena...

Страница 12: ...ltic pump motor input terminal mixing pump heater Hazard of chemical burns This symbol is used to indicate the potential hazard of severe burns and serious injury due to hazardous chemicals All handli...

Страница 13: ...erials of construction listed below Table 1 2 List of materials used in Waltron 3041 Analyzer Pump tubing Silicon or Norprene Fittings PP Connection tubing Norprene Silicon Colorimetric cell Glass Mix...

Страница 14: ...been designed built and located in a closed enclosure with a special key Inside the enclosure these parts have protective covers to avoid any contact and physical injuries to users HAZARD Hazard of b...

Страница 15: ...ctrocution have been designed built and located in an enclosure with a special key Inside the enclosure these parts have protective covers with warning labels to avoid contact and serious injuries or...

Страница 16: ...colorimetric method The analyzer is assembled in an enclosure with a lockable door The LIQUIDS enclosure includes all the components involved in sample and reagent flows as well as mixing and reactio...

Страница 17: ...is measured at a specific wavelength The absorbance is related to sample concentration according to Beer s law The Lambert Beer law is an empirical relationship that relates the absorption of light t...

Страница 18: ...ges from 0 to 1 but it can go higher An absorbance of 0 at some wavelength means that no light of that particular wavelength has been absorbed The intensities of the sample and reference beam are both...

Страница 19: ...wait functions Following the addition of Reagent 2 the mixing pump is activated and the liquid is pumped from the lower part to the upper part of the colorimetric cell The waiting time is programmed...

Страница 20: ...4 2 FLOW DIAGRAM Figure 2 4 Flow diagram 2 4 3 ANALYZER OPERATIONS The Waltron 3041 Silica Analyzer performs several operations throughout a cycle A list of common operations is shown below Rinse 1 Ri...

Страница 21: ...mple circulation to avoid accumulation of suspended solids The sample flow should be adjusted to allow continuous sample overflow to waste through the U shaped stainless steel tube Inside the reservoi...

Страница 22: ...Introduction 21 Waltron User Manual 101 016 B 3 3041 Silica Analyzer Figure 2 6 Mounting dimensions for the fast loop reservoir 10 36 259 mm 5 84 146 mm 5 24 131 mm 5 20 130 mm 0 26 6 5 mm...

Страница 23: ...ample inlet s and calibration standard inlet pass through the housing enclosure on the right hand side of the unit and are connected to the 3 way valve Colorimetric Reaction Cell The colorimetric reac...

Страница 24: ...s a constant level of few cm of liquid on the colorimetric cell 2 7 ELECTRONICS The microprocessor and its PCB assembly are located in the electronic section It provides control for the entire analyzi...

Страница 25: ...tive humidity If the temperature could fall below 5 C the analyzer should be installed in a heated cabinet Because of chemicals and waste gases it is necessary to have a well ventilated location for t...

Страница 26: ...t 8 20 cm on either side and about 40 100 cm in the front Sufficient space for the reagent containers should be provided on the side or beneath the analyzer The reagent containers should be positioned...

Страница 27: ...26 Waltron User Manual 101 016 B 3 3041 Silica Analyzer Installation Figure 3 2 Reccomended complete system installation Note Single channel analyzers will only have one Fast Loop Reservoir...

Страница 28: ...fficiency of the analyzer s grounding Users and qualified maintenance personnel must proceed as follows Be aware of electrical shock and or electrocution labels placed on the analyzer Always isolate p...

Страница 29: ...labels starting with pin 1 on the left Figure 3 3 Electrical connections for user connections and power connections Table 3 1 Terminal block pin locations Pin Number Terminal Label Description 1 Inpu...

Страница 30: ...below to mount the reagent bracket below the analyzer NOTE Mount the bracket below the analyzer so that the base of the bracket is at least 14 inches 40 cm below the analyzer but no more than 30 inch...

Страница 31: ...gle channel analyzers connect the sample to connection 1 on the inlet block and the standard to connection 2 b For dual channel instruments connect sample 1 to connection 1 sample 2 to connection 2 an...

Страница 32: ...ressing the touchscreen buttons Figure 5 1 User interface main display screen 5 2 USER PASSWORD Table 5 1 User password First Level Password service 1111 Second Level Password admin Contact Waltron Ta...

Страница 33: ...ROGRAM menu Analysis Cycle and started when the START ON LINE button has been pressed As soon as the analyzer completes an analysis cycle it will restart with a new analysis This condition is identifi...

Страница 34: ...vel falls below a value of 4 the analyzer goes into FAULT status and stops automatically The alarm message will be displayed in the main menu and the FAULT contact will be activated Every time the rea...

Страница 35: ...de and wait for the user s next command CH 2 available on dual stream units only This command will perform a single analysis cycle on stream 2 At the end of the cycle the analyzer will go into stand b...

Страница 36: ...ted Blank shows the most recent blank value Led shows the led supplied Valid it shows the validation value in compared to the calibration value Current operation this window displays the current analy...

Страница 37: ...results in memory Figure 5 6 Data logger screen of the user interface 5 7 1 SAVE TO USB To export the stored results in the data log to a csv file 1 Insert a USB memory stick into the bottom of the t...

Страница 38: ...to set the ratio of the analysis cycles versus the extra cycles the alarm value low or high and to enable or disable the loss of sample alarm and the 4 20 mA output CALIBRATION MENU This function is...

Страница 39: ...een analysis cycles when the analyzer is in on line mode Result alarm Programs the low high value alarm The alarm is expressed in of full scale Output Signal Enables disables the 4 20 mA output Datalo...

Страница 40: ...ange of the analyzer This setting only applies to dual stream analyzers Configuring Relay 1 2 3 and 4 There are 4 cells on the service screen to configure Relay 1 Relay 2 Relay 3 and Relay 4 Touch one...

Страница 41: ...ion for 20 seconds 4 Select ADD REAG 1 2 3 functions for 60 seconds each in order to prime the three reagent lines Visually confirm that reagent is being drawn into the lines and into the flowcell If...

Страница 42: ...od of extended shut down The recommended and default setting for automatic calibration is approximately once per week 1 Login with the 1st level service password 1111 2 Connect the CAL tube to the cal...

Страница 43: ...w to the fast loop reservoir 2 Check that the sample fills the fast loop reservoir so that the float switch rises and sample is being discharged from the overflow drain 3 Put the analyzer into online...

Страница 44: ...r user command 7 When the user is finished with the grab sample analysis make sure to reconnect the sample tubiing to the fast loop resevoir 8 Turn on sample flow to the fast loop resevoir 9 Put the a...

Страница 45: ...enance work all necessary precautions regarding personal safety protective clothing safety glasses etc are to be taken into consideration Always be sure to label and rinse all connected tubing with wa...

Страница 46: ...nintenance reference chart Scheduled Maintenance Frequency Daily Monthly Quarterly Annually Visual check of FAULT alarm indicator X Visual check of liquids enclosures for leakages detection X Visual c...

Страница 47: ...s 7 Place the pump half containing the rotor in one hand and place the rollers in the 2 6 and 10 o clock positions Place tubing in the outer port and against the two rollers as shown keeping your thum...

Страница 48: ...drain tubing into the drain valve pinch mechanism 9 Feed the drain tubing through the bottom of the enclosure 10 Connect the drain tubing to the T fitting 11 Perform a manual command of sample 1 for...

Страница 49: ...first pump roller into the open space 9 From the manual commands menu perform an add reagent 1 command for 1 second This should rotate the first pump roller into place against the tubing and open a s...

Страница 50: ...eriod please proceed as follows 1 Replace the reagents in the container with distilled water and perform a priming of all the pumps with DI water a Login with the 1st level service password 1111 b Pre...

Страница 51: ...cell Loss of Sample 1 The sample to stream 1 is lost Check the flow of Sample 1 Loss of Sample 2 The sample to stream 2 is lost Check the flow of Sample 2 Dual stream analyzers only Emergency Stop So...

Страница 52: ...are Parts Listing Description Part Number Pump Head 7016 Sampling Pump W9040 007 Pump motor 70 80 rpm 24 Vdc W3040 015 External Reservoir Fast loop with level switch W3040 003 Peristaltic pump for rea...

Страница 53: ...52 Waltron User Manual 101 016 B 3 3041 Silica Analyzer Spare Parts Display Cable W3040 093 Output Cable for User Connections W3040 094...

Страница 54: ...Appendix A Panel Mount Schematics 53 Waltron User Manual 101 016 B 3 3041 Silica Analyzer APPENDIX A PANEL MOUNT SCHEMATICS...

Страница 55: ...54 Waltron User Manual 101 016 B 3 3041 Silica Analyzer Appendix A Panel Mount Schematics...

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