Thermo Scientific ISQ, Руководство пользователя

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4
Creating a Method
Creating a Method for the GC
50 ISQ User Guide Thermo Scientific
7. When you are finished creating methods for each component in your GC/MS system,
select File | Save As... from the main menu or click the icon.
Figure 37. Saving a TRACE 1300 or TRACE 1310 Method
Creating a Method for the TRACE GC Ultra
 To create a method for the TRACE GC Ultra
1. Click the Oven tab to set the oven temperatures. There is always at least one temperature
and time in any GC temperature program. In the Initial row, enter the initial
temperature, which must be 4 °C above room temperature and less than the maximum
operating temperature of your GC column. If you set the initial temperature to a value
below this limit, the GC will not reach the initial temperature. If you set the temperature
above the limit, the GC column will get damaged. You can set the initial hold time to a
value between 0 and 999.99 minutes. The typical initial temperature is at least 10 °C
above the boiling point of your sample solvent and the initial time is usually long enough
for the solvent to move through the column.
Note This process only covers the left SSL, but the process is the same for the right SSL.
For information on how to use the other injector types, consult the TRACE GC Ultra
documentation.