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ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide

Page 12

1.3

Reference Documentation

In addition to this operating manual, other documentation is available
for reference.

Hardware Documentation

Additional hardware documentation includes the following:

•

ISQ EC and ISQ EM Mass Spectrometer Operating Manual

Operating manuals

for the other modules of the LC or IC system

TIP

Electronic versions of these manuals are available as PDF (Portable

Document Format) files. To open and read the PDF files, Adobe™
Reader™ or Adobe™ Acrobat™ is required.

Software Documentation

Additional software documentation includes the following:

•

Chromeleon™ 7 Help and documents

The

Chromeleon 7 Help

provides extensive information and

comprehensive reference material for all aspects of the software.
For basic information about device installation and configuration,
refer to the

Installation Guide

; for specific information about a

certain device, refer to the

Instrument Configuration Manager Help.

In Chromeleon 7, devices are called modules.
For information about the main elements of the user interface and
step-by-step guidance through the most important workflows, refer
to the

Quick Start Guide

For a concise overview of the most important workflows, refer to
the

Reference Card

TIP

The

Chromeleon

Help and documents are included in the software

shipment. The ISQ EC and ISQ EM do not support Chromeleon software
versions before 7.2.6.

Содержание ISQ EC

Страница 1: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide 1R120591 0001 Revision B October 2018 ...

Страница 2: ...written authorization of Thermo Fisher Scientific Inc This manual is provided as is The contents of this manual are subject to being changed without notice in future revisions Thermo Fisher Scientific Inc makes no representations that this document is complete accurate or error free Thermo Fisher Scientific Inc assumes no responsibility and will not be liable for any errors omissions damage or los...

Страница 3: ...r Scientific sales organization For contact information go to Contact Us on http www thermofisher com Technical Assistance For technical support for HPLC products contact your local Thermo Fisher Scientific support organization For contact information go to Contact Us on http www thermofisher com Legal Manufacturer Address Thermo Finnigan LLC a part of Thermo Fisher Scientific 355 River Oaks Parkw...

Страница 4: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 4 ...

Страница 5: ...d Signal Words 15 2 1 1 Safety Symbols and Signal Words in This Manual 15 2 1 2 Observing this Manual 16 2 1 3 Safety Symbols on the Detector 16 2 2 Intended Use 18 2 3 Safety Precautions 19 2 3 1 General Safety Information 19 2 3 2 Qualification of the Personnel 19 2 3 3 Personal Protective Equipment 20 2 3 4 Electrical Safety Precautions 21 2 3 5 General Residual Hazards 21 2 4 Solvent and Addit...

Страница 6: ...ration 47 3 8 1 Standard Installation 47 3 9 Receiving Requirements 48 3 10 What Happens Next 49 4 Appendix 50 4 1 Compliance Information 51 4 1 1 Declarations of Conformity 51 4 1 2 WEEE Compliance 52 4 1 3 FCC Compliance 53 4 1 4 Regulatory Compliance 54 4 1 5 Low Voltage Safety Compliance 54 4 1 6 Notice on Lifting and Handling of Thermo Scientific Instruments 54 4 1 7 Notice on the Proper Use ...

Страница 7: ...r Preinstallation Requirements Guide Page 7 1 Using this Manual This chapter provides information about this manual the conventions used throughout the manual and the reference documentation that is available in addition to this manual ...

Страница 8: ... detailed instructions to prepare your site for installation of a Thermo Scientific ISQ EC or a Thermo Scientific ISQ EM mass spectrometer This manual also contains safety messages precautionary statements and special notices that can prevent personal injury damage to the detector or loss of data when followed properly ...

Страница 9: ... which they apply Safety messages that apply to only a particular section or procedure appear in the section or procedure to which they apply They appear different from the main flow of text Safety messages are often preceded by an alert symbol and or alert word The alert word appears in uppercase letters and in bold type Make sure that you understand and follow all safety messages presented in th...

Страница 10: ...rs in bold type Input that you enter by the keyboard or that you select with the mouse Buttons that you click on the screen Commands that you enter by the keyboard Names of for example dialog boxes properties and parameters For brevity long expressions and paths appear in the condensed form for example Click Start All Programs Thermo Chromeleon 7 Services Manager Start Instrument Controller Refere...

Страница 11: ...ant words in the main flow of text appear italicized Electronic Manual Version PDF The electronic version PDF of the manual contains numerous links that you can click to go to other locations within the manual These include Table of contents entries Index entries Cross references in blue text for example to sections and figures ...

Страница 12: ... includes the following Chromeleon 7 Help and documents The Chromeleon 7 Help provides extensive information and comprehensive reference material for all aspects of the software For basic information about device installation and configuration refer to the Installation Guide for specific information about a certain device refer to the Instrument Configuration Manager Help In Chromeleon 7 devices a...

Страница 13: ...entation Refer also to the user documentation provided by the manufacturers of third party components and materials for example Safety Data Sheets SDSs Third party documentation includes the user documentation for the optional gas supply as applicable User documentation for the nitrogen generator ...

Страница 14: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 14 2 Safety This chapter provides general and specific safety information and informs about the intended use of the detector ...

Страница 15: ...using the detector The safety symbols and signal words in this manual include the following Always be aware of the safety information Do not proceed until you have fully understood the information and consider the consequences of what you are doing CAUTION Indicates a hazardous situation that if not avoided could result in minor or moderate injury WARNING Indicates a hazardous situation that if no...

Страница 16: ...afety messages and precautionary statements presented in this manual 2 1 3 Safety Symbols on the Instrument The table lists the safety symbols that appear on the instrument or on labels affixed to the instrument Follow the safety notices in this manual to prevent the risk of operator injury or damage to the instrument Symbol Description Indicates a potential hazard Refer to this manual to avoid th...

Страница 17: ...d or might occur Alerts you to carefully read your instrument s documentation to ensure your safety and the instrument s operation ability Failing to carefully read the documentation could or might put you at risk for a physical injury Indicates that physical injury could or might occur if two or more people do not lift an object ...

Страница 18: ...nded for laboratory research use only It is not intended for use in diagnostic procedures Laboratory Practice Thermo Fisher Scientific recommends that the laboratory in which the MS system is used follow best practices for LC MS and IC MS analyses This includes among others Using appropriate standards Regularly running calibration Establishing shelf life limits and following them for all consumabl...

Страница 19: ... for the detector by Thermo Fisher Scientific Perform only the procedures that are described in this operating manual and in supporting documents for the detector Follow all instructions step by step and use the tools recommended for the procedure Open the enclosure of the detector and other components only if specifically instructed to do so in this manual Thermo Fisher Scientific cannot be held ...

Страница 20: ...ctor and the substances they are using All users should observe the related Safety Data Sheets SDSs 2 3 3 Personal Protective Equipment Wear personal protective equipment and follow good laboratory practice to protect you from hazardous substances The appropriate equipment depends on the hazard For advice on the hazards and the equipment required for the substances you are using refer to the mater...

Страница 21: ...gh voltages are present inside the device that could cause an electric shock or damage to the device Do not make any changes to the electrical or grounding connections If you suspect any kind of electrical damage disconnect the power cord and contact Thermo Fisher Scientific Technical Support for assistance Do not open the housing or remove protective panels unless specifically instructed to do so...

Страница 22: ... refer to the Safety Data Sheet SDS of the manufacturer Observe the guidelines of Good Laboratory Practice GLP Be sure that you know the properties of all substances that you are using Avoid exposure to harmful substances If you have any doubt about a substance handle the substance as if it is potentially harmful Wear personal protective equipment as required by the hazard and follow good laborato...

Страница 23: ...olvents with a self ignition temperature below 150 C might ignite when in contact with a hot surface for example due to leakage in the chromatography system Avoid the use of these solvents WARNING Hazardous Vapors Install the LC MS or IC MS system in a well ventilated laboratory If the mobile phase or sample includes volatile or flammable solvents do not allow them to enter the workspace If the mo...

Страница 24: ...ature on the chemical resistance of PEEK CAUTION Fused silica is used in flow cells and capillaries To avoid personal injury always wear safety glasses when handling fused silica tubing for example when cutting fused silica tubing to length CAUTION Allergic Reaction Some capillaries in the HPLC system are made of MP35N a nickel cobalt based alloy Individuals with sensitivity to nickel cobalt may s...

Страница 25: ...EM Mass Spectrometer Preinstallation Requirements Guide Page 25 CAUTION Instrument Damage Clean tubing cutters with methanol prior to use Otherwise tubing may be contaminated with oil and grease from packing material ...

Страница 26: ...ment observe these recommendations on the use of solvents and additives Use only solvents and additives that are compatible with all parts in the flow path Follow any specific recommendations presented in other sections of this manual Refer also to the operating manuals for all modules in the LC or IC system They may provide additional guidelines and information ...

Страница 27: ...s manual For details see 4 1 Changes that you make to the device may void compliance with one or more of these EMC and safety standards Changes to the device include replacing a part or adding components options or peripherals not specifically authorized and qualified for the product by Thermo Fisher Scientific To ensure continued compliance with EMC and safety standards replacement parts and addi...

Страница 28: ...efore the Thermo Fisher Scientific representative arrives to install the ISQ EC or ISQ EM mass spectrometer NOTICE For the ISC EC and ISQ EM mass spectrometers only These instructions are for the ISQ EC and ISQ EM mass spectrometers only You will also need to follow the specific preinstallation requirements for the LC or IC which will be connected ...

Страница 29: ... 95 cm 37 5 in 2 Make sure you have enough room to move boxes around corners into elevators or through doorways Table 1 contains the dimensions and weight of shipping boxes so that you can make accommodations 3 The calibrant solution and optional computer are shipped separately Box Contents Length Width Height Weight ISQect infusion cm In cm in cm in kg lbs ISQ EC ISQ EM 112 44 95 37 5 107 42 1500...

Страница 30: ...ISQ EC or ISQ EM system Note Review site preparation requirements guides for additional system components such as IC or LC instrument Box Contents Length Width Height Weight ISQect infusion cm In cm in cm in kg lbs ISQ EC ISQ EM 91 36 42 16 5 52 20 5 71 156 Foreline Pump1F 2 47 18 5 20 8 26 10 28 62 Computer2F 3 42 16 5 18 7 37 14 5 7 5 17 Monitor2 19 7 5 54 21 44 17 5 5 12 Keyboard2 23 9 46 18 5 ...

Страница 31: ...he bench front or back is acceptable The foreline hose exits at the rear of the instrument and is connected to the foreline pump The hose can be moved to exit to the right the left or back The foreline pump is placed on the floor below or next to the system The foreline hose is 250 cm long measured from the back of the MS It cannot be extended because that will adversely affect the pressure in the...

Страница 32: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 32 Figure 2 ISQ EC or ISQ EM system front view Figure 3 ISQ EC or ISQ EM system back view ...

Страница 33: ...in mind additional instruments add to the totalweight 4 Ensure that your work area is stable and free of vibration from nearby equipment The ISQ EC or ISQ EM mass spectrometer is a sensitive instrument For this reason the foreline pumpmust be placed on the floor below or next to the system It is quiet at only 48 dB A See Figure 4 Figure 4 ISQ EC Bench Setup ...

Страница 34: ...following guidelines to ensure your site has the proper lighting to run an ISQ EC or ISQ EM system 1 Ensure that the work area is properly lit You might need an overhead lamp to light your work area 2 You might need a small high intensity lamp when you clean the ISQ EC or ISQ EM system or work on the foreline pump ...

Страница 35: ...Additional circuits may be needed for other equipment Equipment Circuit Max Current A at 120 V AC Max Current A at 230 V AC Maximum Power VA ISQ EC or ISQ EM MS3F 4 4F 5 1 11 7 6 1 1400 LC or IC 6 2 See instrument specifications See instrument specifications See instrument specifications Computer5F 6 2 5 2 6 600 Monitor 6 2 2 1 240 Table 3 Power requirements The power quality supplied to your syst...

Страница 36: ...on should be less than 6 Slow changes are gradual long term changes in average root mean square RMS voltage level with typical durations greater than 2 s Sags and swells are slow changes in average root mean square RMS voltage level with typical durations between 50 ms and 2 s Transients even of a few microseconds duration cause electronic devices to fail or to degrade and significantly shorten th...

Страница 37: ... cord or buy an additional cord you may use any brand of power cord as long as it is appropriate for your region The power cords are designed to match the wall socket requirements of the country in which they are used The end of the power cords that plugs into the power socket on the device is identical for all power cords The end of the power cords that plugs into the wall socket is different Reg...

Страница 38: ...allation Requirements Guide Page 38 Region Thermo Scientific Part Number C13 for PC monitors LC and IC Thermo Scientific Part Number C19 for MS Australia 250V China 250V Europe Schuko 250V United Kingdom 250V Denmark 250V Italy 250V Israel 250V ...

Страница 39: ...trometer Preinstallation Requirements Guide Page 39 Region Thermo Scientific Part Number C13 for PC monitors LC and IC Thermo Scientific Part Number C19 for MS India 250V Argentina 250V Table 4 Power Cord Identification by Region ...

Страница 40: ... performance is only confirmed for these temperatures For best performance the operating temperature should be constant Use Table 5 to calculate the amount of heat your system will generate and ensure your air conditioning system can handle that amount of heat IMPORTANT If you are not operating the ISQ EC or ISQ EM MS it is safe to leave the instrument powered on in a room with a temperature betwe...

Страница 41: ...ger than this amount dust can accumulate on electronic components This accumulation reduces their ability to cool off properly and could cause them to overheat If your environment is particularly dusty we recommend that you purchase the optional dust filter for your system 4 Ensure that your site is free of electrostatic discharge ESD which may damage the electronic components of your system Ensur...

Страница 42: ...ecifications for the gas supplied to the instrument have major impact on the instrument performance Observe the following notes If the gas supply pressure is varying or dropping below the specified pressure range it can impair the performance of the instrument Non volatile hydrocarbons such as compressor oils in the gas supplied to the system can cause permanent damage to the instrument If the sup...

Страница 43: ...OD Teflon tubing If connecting multiple instruments to one nitrogen line ensure the minimum pressure is delivered to each instrument when all are consuming the maximum amount of gas The system should be placed close to the nitrogen gas source since gas pressure decreases as the length of tubing increases Options for delivering nitrogen are in order of convenience A nitrogen generator These are ava...

Страница 44: ...f rate is a function of the ambient temperature In general a Dewar will go empty in 2 3 weeks even if not used NOTICE There are different types of liquid nitrogen Dewars some are rated to supply liquid and some are rated to supply liquid or gas Ensure that the Dewar used with the system is rated to supply high pressure gas Dewars rated to a higher pressure are better at maintaining pressure when u...

Страница 45: ...ory Consult your local Environmental and Safety Regulations for information about how to properly exhaust fumes from your laboratory 1 1 1 Foreline Pump Exhaust Must handle up to 1 L min Connection to top of pump is 25 4 mm 1 in i d 305 cm of flexible tubing is provided in the installation kit This tubing can be cut to any length needed 1 1 2 Ion Source Exhaust Must handle up to 30 L min Connectio...

Страница 46: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 46 Figure 5 Ion source exhaust tubing ...

Страница 47: ...t one of the following solvents must available Solvents should be new and un opened for best results during installation Recommended solvent quality for installation Methanol Optima LC MS grade Fisher Scientific A456 4 or equivalent Water Optima LC MS grade Fisher Scientific W6 4 or equivalent Water Ultrapure Type 1 18 Mohm resistance degassed Acetonitrile Optima LC MS grade Fisher Scientific A955...

Страница 48: ...ing of delicate equipment Occasionally however equipment is inadvertently damaged in transit If you notice evidence of external damage do not refuse shipment Instead call Customer Service 2 Once you are finished inspecting your shipment move the cartons to a protected location preferably the installation site Leave the boxes as complete as possible and do not unpack or open the boxes without a The...

Страница 49: ...irements Guide Page 49 3 10 What Happens Next A Thermo Fisher Scientific Representative will contact you to schedule the installation of your system It is important to confirm that all the requirements in this guide are met BEFORE scheduling an installation ...

Страница 50: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 50 4 Appendix This chapter provides additional information about compliance ...

Страница 51: ...at the product is compliant with the directive China RoHS regulations Measures for Administration of the Pollution Control of Electronic Information Products One of following logos may be present on the device if applicable The green logo marks items that do not contain the hazardous substances identified by the regulations The orange logo including a one digit or two digit number mark items that ...

Страница 52: ...te Electrical Electronic Equipment WEEE Directive 2002 96 EC It is marked with the following symbol Figure 6 WEEE symbol Thermo Fisher Scientific has contracted with one or more recycling or disposal companies in each European Union EU Member State and these companies should dispose of or recycle this product For further information contact Thermo Fisher Scientific ...

Страница 53: ...e reasonable protection against harmful interference when the equipment is operated in a commercial environment This equipment generates uses and can radiate radio frequency energy and if not installed and used in accordance with the instructions may cause harmful interference to radio communications Operation of this equipment in a residential area is likely to cause harmful interference in which...

Страница 54: ...cement parts and additional components options and peripherals must be ordered from Thermo Fisher Scientific or one of its authorized representatives 4 1 5 Low Voltage Safety Compliance This device complies with Low Voltage Directive 2014 35 EU and harmonized standard EN 61010 1 2001 4 1 6 Notice on Lifting and Handling of Thermo Scientific Instruments For your safety and in compliance with intern...

Страница 55: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 55 phones in close proximity to the instrument For manufacturing location see the label on the instrument ...

Страница 56: ...ISQ EC and ISQ EM Mass Spectrometer Preinstallation Requirements Guide Page 56 4 1 9 Manual Release History Revision Released Covering A August 2017 ISQ EC MS B October 2018 ISQ EC MS and ISQ EM MS ...

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