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A-96.250.671 / 070222

AMI Silica

Material Safety Data sheets

96

10. Material Safety Data sheets

10.1. Reagents

Download

MSDS

The current Material Safety Data Sheets (MSDS) for the above listed 

Reagents are available for downloading at 

www.swan.ch

.

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 1a for AMI Silica 

Ammonium heptamolybdate tetrahydrate

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 1b for AMI Silica 

Sodium hydroxide pellets

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 2 for AMI Silica 

Sulfuric acid 25 %

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 3 for AMI Silica 

Oxalic acid dihydrate

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 4a for AMI Silica 

Sulfuric acid 25 %

Catalogue No.:

Product name:

Part of Article No. A - 85.420. 560

OXYCON ON-LINE SILICA 

Reagent 4b for AMI Silica 

Ammonium iron(II) sulfate hexahydrate

Catalogue No.:

Product name:

A85.142.400

Silica Standard 100ppm 100ml

Содержание AMI Silica

Страница 1: ...Operator s Manual Firmware V6 22 and higher AMI Silica A 96 250 671 070222 ...

Страница 2: ...r nearest Swan representative or the manufacturer Swan Analytische Instrumente AG Studbachstrasse 13 8340 Hinwil Switzerland Internet www swan ch E mail support swan ch Document Status Title AMI Silica Operator s Manual ID A 96 250 671 Revision Issue 00 Nov 2011 First edition 01 Nov 2013 Mainboard V2 4 update to firmware release 5 40 02 Okt 2014 Update to firmware release 5 41 installation of 2nd ...

Страница 3: ...22 3 5 Install the 2nd Sample Stream Option 23 3 6 Install the AMI Sample Sequencer 26 3 6 1 Sample connection with 2nd sample stream 26 3 7 Electrical Connections 27 3 7 1 Connection Diagram 29 3 7 2 Power Supply 30 3 8 Relay Contacts 31 3 8 1 Input 31 3 8 2 Alarm Relay 31 3 8 3 Relay 1 and 2 32 3 9 Signal Outputs 34 3 9 1 Signal Output 1 and 2 Current Outputs 34 3 10 Interface Options 34 3 10 1 ...

Страница 4: ... 6 7 Cleaning the Photometer 56 6 8 Cleaning the solenoid valve 57 6 9 Tube Replacement 59 6 9 1 Replace the Pump Tubes 59 6 9 2 Tube Numbering 61 6 10 Fill or Flush Reagent System 62 6 11 Longer Stop of Operation 62 7 Troubleshooting 63 7 1 Slope Error 63 7 2 Grab Sample 65 7 3 Error List 66 7 4 Opening the peristaltic pump housing 70 7 5 Replacing Fuses 71 8 Program Overview 72 8 1 Messages Main...

Страница 5: ...A 96 250 671 070222 AMI Silica 5 10 Material Safety Data sheets 96 10 1 Reagents 96 11 Default Values 97 12 Index 99 13 Notes 101 ...

Страница 6: ...ructions are given throughout this manual at the re spective locations where observation is most important Strictly fol low all safety instructions in this publication Target audience Operator Qualified person who uses the equipment for its intended purpose Instrument operation requires thorough knowledge of applications instrument functions and software program as well as all applicable safety ru...

Страница 7: ...tion instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the equipment minor injury malfunctions or incorrect process values can be the consequence if such warnings are ig nored Follow the prevention instructions carefully Mandatory Signs The mandatory signs in this manual ha...

Страница 8: ...71 070222 AMI Silica Safety Instructions 8 Warning Signs The warning signs in this manual have the following meaning Electrical shock hazard Corrosive Harmful to health Flammable Warning general Attention general ...

Страница 9: ...li ty for any claim resulting from unauthorized modification or alter ation WARNING Electrical Shock Hazard If proper operation is no longer possible the instrument must be disconnected from all power lines and measures must be taken to prevent inadvertent operation To prevent from electrical shock always make sure that the ground wire is connected Service shall be performed by authorized personne...

Страница 10: ...ctions in this manual as well as the Material Safety Data Sheets MSDS Reagent 1 Ammoniummolybdate consists of Reagent 1a Ammonium molydate Tetrahydrate Reagent 1b Sodium hydroxide pellets Reagent 2 Sulfuric acid 25 Reagent 3 Oxalic acid Reagent 4 Ammonium Ferrous Sulfate consists of Reagent 4a Sulfuric acid 25 Reagent 4b Ammonium iron II sulfate hexahydrate Silica Standard 100 ppm 100 ml Download ...

Страница 11: ...e chemical reactions has been finished Grab sample The measuring mode grab sample allows the measurement of sam ples from remote locations Second sample stream If required the AMI Silica can be equipped with the optional second sample stream module Sample sequencer If measurement of more than two sample streams is required the AMI Silica can be connected to a Sample Sequencer which allows to measu...

Страница 12: ...ting valve so that always a small part of the sample flows through the overflow tube B into the waste I This adjustment ensures a sufficient sam ple flow through the measuring chamber of the photometer F If no measurement takes place the sample flows through the pho tometer outlet E where it will be aerated through air inlet S to gen erate bubbles Then the sample flows through the bubble counter H...

Страница 13: ...ube Solenoid valve Sample inlet photometer Sample outlet Photometer Magnetic stirrer Bubble counter Waste Reagent 1 K L M N O P Q R S Reagent 2 Reagent 3 Reagent 4 6 way valve Peristaltic pump Loop Flow regulating valve Sample inlet Air Inlet 1 2 3 4 5 6 7 Level D B A C G H I J K L M O P Q R S E N F ...

Страница 14: ... 6 way valve in position 5 sample is sucked into the loop the whole quantity of the reagents is pushed into the photometer 5 The reagents are mixed with the magnetic stirrer the first reac tion starts After 150 sec 6 6 way valve in position 3 the reagent 3 is sucked from the container L 7 6 way valve in position 5 sample is sucked into the loop the whole quantity of the reagent is pushed into the ...

Страница 15: ... photometer A measuring cycle takes 10 minutes The diagram below shows the process of a measuring cycle in the time axis 150 sec 90 sec 90 sec 6 5 4 3 2 1 1 2 3 4 5 6 7 7 5 min 2 5 min 8 9 10 11 12 13 14 X Y X Measuring steps on time axis Reagent 2 Y 6 way valve position Reagent 3 Solenoid valve closed Reagent 4 Solenoid valve open Loop Zero point measurement Reaction time Sample measurement Flush...

Страница 16: ...X 10 to 50 C 30 to 85 C 10 90 rel non condensing backlit LCD 75 x 45 mm Sample requirements Flow rate Sample pressure inlet Temperature min 10 l h 0 15 2 bar 2 28 PSI up to 50 C 122 F Silica measurement Measuring method Measuring range Reproducibility Max PO4 concentration colorimetric molybdosilicate method 1 to 5 000 ppb 1 ppb or 5 whichever is greater 10 ppm On site The analyzer site must permi...

Страница 17: ... Product Description 17 Dimensions Panel Dimensions Screw diameter Weight stainless steel 400 x 850 x 160 mm 8 mm 16 0 kg Level Exit Enter AMI Silica 13 mm 0 51 4 x dia 10 mm 0 39 850 mm 33 46 824 mm 32 44 374 mm 14 72 400 mm 15 75 ...

Страница 18: ...ter Panel 6 way valve control box 6 way valve Peristaltic pump Reagent 1 Reagent 2 Reagent 3 Reagent 4 Constant head K L M N O P Flow regulating valve Solenoid valve Sample inlet with sample switch 2nd sample stream option Photometer with magnetic stirrer Bubble counter Waste A B C D E F G H I J K L M N O P ...

Страница 19: ...all external devices like limit switches current loops and pumps Install the 2nd Sample Stream Option p 23 if available Install the AMI Sample Sequencer p 26 if available Connect the power cord see Power Supply p 30 Reagents Prepare the reagents see Refill or replace Reagents p 49 Insert suction lances see Instrument Setup p 37 Power up Activate the Peristaltic Pump p 37 Prepare Reagents p 37 Esta...

Страница 20: ...ust only be installed by trained personnel Mount the instrument in vertical position For ease of operation mount it so that the display is at eye level For the installation a kit containing the following installation ma terial is available 4 Screws 8x70 mm 4 Dowels 4 Washers 8 4 24 mm Mounting re quirements The instrument is only intended for indoor installation For dimensions see 17 ...

Страница 21: ...ds the waste funnel 2 Fit the constant head tube B into the flow cell block E 3 Put the constant head cover A onto the constant head tube 4 Adjust the overflow tube C so that it is at the lower level mark A B C D E F G Constant head cover Constant head tube Overflow tube O Ring Flow cell block Flow regulating valve Solenoid valve Level A B C E G F D ...

Страница 22: ...he sample line Mounting of SERTO fitting 3 4 2 Sample Outlet Connect the 1 2 tube E to the hose nozzle D and place it into a pressure free drain with sufficient capacity A B C D Screw connection Compression ferrule Knurled nut Flexible tube B C D A A B C D E Tube from constant head Tube from photometer Waste funnel Hose nozzle 1 2 tube B E D A C ...

Страница 23: ...main sample tap A B C D E F G H Block housing Connecting piece 2 O rings Blind Plug Flow regulating valve Flow cell block Sample inlet Elbow union Solenoid valve cable I J K L M N X Sample stream 1 Sample stream 2 Waste 15x20 mm Fixing screws Solenoid valve Sample inlet tube Detail view Exit Enter AMI SILICA SiO2 Process Analyzer Level A F G X L J I N M E D D H K A B C ...

Страница 24: ...ore of the flow cell block F 8 Insert the connecting piece B into the bore of the flow cell block 9 Slide the block housing A over the connecting piece and press it against the flow cell block F while screwing the block housing with the 2 fixing screws L onto the panel 10 Push a 15 x 20 mm tube K not included in the installation set over the hose nozzle of the block housing and put the end of the ...

Страница 25: ...the PG7 cable glands to feed the cable of the solenoid valve into the AMI transmitter housing 1 Remove the plug A from the cable gland B 2 Open the transmitter housing 3 Feed the cable of the solenoid valve through the cable gland B into the AMI transmitter housing 4 Connect the wires to the terminals in the AMI transmitter according to the Connection Diagram p 29 B A ...

Страница 26: ...e Sequencer 3 6 1 Sample connection with 2nd sample stream If an AMI Sample Sequencer is connected to an AMI Silica with a second sample stream option A sample inlet 2 will be automatically switched off and only sample inlet 1 will be active Connect the sample outlet of the Sample Sequencer to sample inlet 1 E of the second sample stream option A B C D E F Second sample stream option Blind plug Fl...

Страница 27: ...rate the instrument from an power outlet which has a ground connection Make sure the power specification of the instrument corre sponds to the power on site Cable thicknesses In order to comply with IP66 use the following cable thicknesses Note Protect unused cable glands Wire For power and relays Use max 1 5 mm2 AWG 14 stranded wire with end sleeves For signal outputs and input Use 0 25 mm2 AWG 2...

Страница 28: ...ure that the devices connected to the following contacts are disconnected from the power before resuming installation relay 1 relay 2 alarm relay WARNING To prevent from electrical shock do not connect the instrument to the power unless the ground wire PE is connected WARNING The mains of the AMI Transmitter must be secured by a main switch and appropriate fuse or circuit breaker ...

Страница 29: ...tion 29 3 7 1 Connection Diagram CAUTION Use only the terminals shown in this diagram and only for the mentioned purpose Use of any other terminals will cause short circuits with possible corresponding consequences to material and personnel ...

Страница 30: ...ound has to be connected to the grounding terminal Installation requirements The installation must meet the following requirements Mains cable to comply with standards IEC 60227 or IEC 60245 flammable rating FV1 Mains equipped with an external switch or circuit breaker near the instrument easily accessible to the operator marked as interrupter for AMI Silica A B C D Power supply connector Neutral ...

Страница 31: ... Max load 1 A time lag 250 VAC Alarm output for system errors Error codes see Troubleshooting p 63 Programming see menu 5 3 1 p 87 Note With certain alarms and certain settings of the AMI transmitter the alarm relay does not switch The error however is shown on the display 1 usual use Terminals Description Relay connection NC1 Normally Closed 10 11 Active opened during normal operation Inactive cl...

Страница 32: ...tus of the relays described below For programming see Menu Installation 5 3 2 and 5 3 3 p 88 Relay config Terminals Jumper pos Description Relay configuration Normally Open 6 7 Relay 1 8 9 Relay 2 Inactive opened during normal operation and loss of power Active closed when a programmed function is executed Normally Closed 6 7 Relay 1 8 9 Relay 2 Inactive closed during normal operation and loss of ...

Страница 33: ...n paral lel to the load A snubber circuit is not necessary if an AMI relaybox is used Resistive load Resistive loads max 1 A and control signals for PLC impulse pumps and so on can be connected without further measures Actuators Actuators like motor valves are using both relays One relay contact is used for opening the other for closing the valve i e with the 2 re lay contacts available only one m...

Страница 34: ... isolator Signal output 1 Terminals 14 and 13 Signal output 2 Terminals 15 and 13 Programming see menu 5 2 Signal Outputs p 83 3 10 Interface Options The slot for interfaces can be used to expand the functionality of the AMI instrument with either an additional signal output a Profbus or Modbus connection a HART connection an USB Interface A B C AMI Transmitter Slot for interfaces Screw terminals ...

Страница 35: ...nstallation instruction Note Max burden 510 Ω Third signal output 0 4 20 mA PCB 3 10 2 Profibus Modbus Interface Terminal 37 PB Terminal 38 PA To connect several instruments by means of a network or to config ure a PROFIBUS DP or a MODBUS connection consult the PROFI BUS MODBUS manual Use appropriate network cable Note The switch must be ON if only one instrument is installed or on the last instru...

Страница 36: ...onsult the HART manual HART Interface PCB 3 10 4 USB Interface The USB Interface is used to store Logger data and for Firmware upload For detailed information see the corresponding installation instruction The optional third signal output 0 4 20 mA PCB B can be plugged onto the USB interface and used in parallel USB Interface A USB Interface PCB B Third signal output 0 4 20 mA PCB A B ...

Страница 37: ...from sticking together at the pressure points 1 Turn the occlusion frame B clockwise to activate the peristaltic pump The peristaltic pump is ready 4 2 Prepare Reagents See Refill or replace Reagents p 49 1 Insert the suction lances into the containers Make sure that the numbers on the suction lances correspond to the numbers on the containers A B C D Turn clockwise to activate Occlusion frame Rot...

Страница 38: ...nnel instrument With a single channel instrument proceed as follows 1 Switch on power 2 Adjust the sample flow using the flow regulating valve D on the flow cell block of the constant head 3 Start Fill system see Fill or Flush Reagent System p 62 4 Check tube connections and flow cell for leaks and repair if necessary 5 Let the instrument run in for one hour A B C D Cover Outer tube Flow cell bloc...

Страница 39: ...t the sample flow using the flow regulating valves D of the second sample stream option 3 Start Fill system see Fill or Flush Reagent System p 62 4 Check tube connections and flow cell for leaks and repair if necessary 5 Let the instrument run in for one hour A B C D E Cover Outer tube Blind plug Flow regulating valves Second sample stream option Level E D 2 1 C A B ...

Страница 40: ...ead 3 Adjust the sample flow using the flow regulating valves F of the AMI Sample Sequencer 4 Start Fill system see Fill or Flush Reagent System p 62 5 Check tube connections and flow cell for leaks and repair if necessary 6 Let the instrument run in for one hour A B C D Cover Outer tube Flow cell block of the constant head Flow regulating valve E F Flow cell blocks of sample streams 1 6 Flow regu...

Страница 41: ... stream option is installed make the following settings Set the number of channels to 2 See 5 1 5 p 81 Select the channel switching mode See 5 1 6 p 82 If an AMI Sample Sequencer is installed make the following settings On the AMI Sample Sequencer navigate to Installation Sequence and select AMI On the AMI Silica select the number of available channels and the channel selection mode See 5 1 5 p 81...

Страница 42: ...vious menu level B to move DOWN in a menu list and to decrease digits C to move UP in a menu list and to increase digits to scroll the measuring values if a Sample Sequencer is con nected D to open a selected sub menu to accept an entry Exit Enter B C D A 32 B s RUN 25 4 C 14 10 45 R1 0 42 ppb R2 1 Installation Operation Diagnostics Messages Maintenance Main Menu Enter Exit ...

Страница 43: ...gnal outputs B ERROR Error Fatal error C Reagent low D Transmitter control via Profibus E Time F Process values with time stamp G Sample flow in bubbles per second H Sample temperature I Relay status upper lower limit not yet reached upper lower limit reached control upw downw no action control upw downw active dark bar indicates control intensity motor valve closed motor valve open dark bar indic...

Страница 44: ...error C Reagent low D Transmitter control via Profibus E Time F Process values with time stamp Si1 sample stream 1 Si2 sample stream 2 Channel active No sample flow n Measurement not valid not visible in this example x Only visible if a Sample Sequencer is connected to the AMI Silica Indicates that the sample stream is inactive G Sample flow in bubbles per second H Sample temperature I Relay statu...

Страница 45: ...ight need to be modified during daily routine Normally password protected and used by the process operator Subset of menu 5 Installation but process related Menu Installation 5 For initial instrument set up by SWAN authorized person to set all instrument parameters Can be protected by means of password 1 Messages Operation Maintenance Diagnostics Main Menu Installation 1 1 Pending Errors Messages ...

Страница 46: ...e new parameter is set 5 1 2 Sensors Sensor type FOME Temperature NT5K Standards Disinf Free chlorine 4 4 1 Logger Log interval 30 min Clear logger no 4 1 3 Logger Clear logger no Log interval 30min 1 Hour Interval 5 min 30 min 10 min 4 1 3 Logger Log interval 10 min Clear logger no 4 1 3 Logger Log interval Clear logger no No Save Yes 1 Select the value you want to change 2 Press Enter 3 Set requ...

Страница 47: ...Grab Sample 2 Follow the instructions on the screen Note The measured value of the grab sample is not stored If an AMI Sample Sequencer is installed the flow regulating valve B on the flow cell block of the constant head must be closed during the grab sample measurement Otherwise the grab sample may flow back into the sample feed line A B Flow cell block of the constant head Flow regulating valve ...

Страница 48: ...ump has stopped 4 Stop sample flow 5 Wait until the constant head is empty 6 Put suction lances into an empty bucket 7 Shut off power of the instrument Weekly Check sample supply for dirt Check sample flow Monthly Check reagent level Every 6 months Exchange reagent pump tube By occurrence E020 FOME dirty Cleaning the Photometer p 56 E022 Reagent empty Refill or replace Reagents p 49 E065 Reagents ...

Страница 49: ...ous chemicals are al lowed to prepare the reagents Canister setup Container almost empty Maintenance E065 Reagents low and the remaining reagent volume in starting at 17 340 ml Container empty Error E022 Reagent empty A B C D E F G H I Suction lance without level detector containers 1 3 Suction lance with level detector container 4 Level detector 2 L mark Container 1 Ammonium molybdate Container 2...

Страница 50: ...all containers well with demineralized water 2 Fill the container to 3 4 of its final level with demineralized water 3 Carefully add the chemicals See Reagent 1 p 51 Reagent 2 p 51 Reagent 3 p 51 Reagent 4 p 51 4 Screw the cover onto the container and mix well 5 Fill the container to its final level and mix again 6 Put container into the holder number 1 to 4 from left to right 7 Insert suction lan...

Страница 51: ...lways replace the reagent filters included with each reagent set when preparing new reagents Insert suction lances into the containers Make sure that the numbers on the suction lances correspond to the numbers on the containers Personal protective equipment Reagent 3 H302 Harmful if swallowed H312 Harmful in contact with skin H315 Causes skin irritation H318 Causes serious eye damage H373 May caus...

Страница 52: ...rification procedure Basically follow the dialog in menu Maintenance Service Verification 3 2 1 Note Start any time if a measuring cycle is in progress wait for next prompt 1 Stop sample flow by closing the flow regulating valve Wait for next prompt Constant head will be drained and an automatic zero will be defined 2 Open cuvette of the photometer and insert the verification filter Enter to conti...

Страница 53: ...s Standard To prepare a 100 ppb standard solution dilute 1 ml of stock solution with 1 l of demineralized water Calibration 1 Navigate to Maintenance Calibration 2 Follow the instructions on the screen Note If an AMI Sample Sequencer is installed the flow regulating valve B on the flow cell block of the constant head must be closed during the calibration Otherwise the standard solution may flow ba...

Страница 54: ...olvents or scrubbing materials to clean acrylic glass parts Use soft detergent and rinse well Eliminate lime deposits with a common household deliming agent in standard concentra tion Do not drop the constant head tube 6 6 1 Disassemble the Constant Head The flow cell can be disassembled easily Before disassemble the flow cell switch off the instrument according to instructions in Stop of Operatio...

Страница 55: ...ottle cleaner and soapy water 4 Replace all O rings before reassembling the flow cell Note A film of teflon paste e g Fomblin from Solvay Solexis on the O rings improves tightness and life time Assemble the Constant Head according to Install the Constant Head p 21 A B C D E F G Constant head cover Constant head tube Overflow tube O Ring Flow cell block Flow regulating valve Solenoid valve Level A ...

Страница 56: ...ructions in Stop of Operation for Maintenance p 48 Material Small brush Procedure 1 Close the flow regulating valve A 2 Wait until the sample flow through the photometer has stopped 3 Unscrew the cover B from the photometer C 4 Clean the Photometer with a small brush D 5 Screw the cover to the photometer 6 Open the flow regulating valve A B C D Flow regulating valve Photometer cover Photometer Bru...

Страница 57: ...onstant head The sole noid valve should be disassembled if it does not switch anymore or if it is clogged 1 Switch off the instrument according to instructions in Stop of Op eration for Maintenance p 48 2 Loosen the nut A 3 Remove the solenoid coil B from the valve body C 4 Loosen the fixing screws of the valve body with a 2 5 mm allen key D A B C D ...

Страница 58: ... Note The O rings inside the valve body may stick on the flow cell and fall down if the valve body is removed 5 Remove the valve body from the flow cell 6 Remove the white plate G with a screw driver size 0 F The membrane H is now visible 7 Clean base plate G and mem brane H with clean water E F G H ...

Страница 59: ...of reagents possible If the occlusion frames are opened during operation already mixed reagents will flow back into the reagent canisters and pol lute the reagents Never open the occlusion frames if the instrument is in opera tion Proceed according to Stop of Operation for Maintenance p 48 before opening the occlusion frames Overview A B C D Pump housing Occlusion frame closed Rotor Pump tube E F ...

Страница 60: ...the rotor C by pulling the com plete occlusion frame B out of the holder 5 Disconnect the reagent tubes from the old pump tube and con nect them to the new pump tube 6 Install the new pump tube by pushing the occlusion frame onto the holder 7 Lock the occlusion frame Check that the occlusion frame and the tube are aligned perpendicular to the axis of the rotor 8 Insert the suction lances into the ...

Страница 61: ...7 Tube No from to 1 Reagent container J 6 way valve port 1 2 Reagent container K 6 way valve port 2 3 Reagent container L 6 way valve port 3 4 Reagent container M 6 way valve port 4 5 6 way valve port 5 Photometer 6 6 way valve port 7 Peristaltic pump input 7 Peristaltic pump output Photometer reagent input ...

Страница 62: ...n the system 6 11 Longer Stop of Operation 1 Proceed according to chapter Stop of Operation for Maintenance p 48 2 Empty the measuring cell of the photometer for example with a pipette and dry it with a soft tissue 3 Relax the occlusion frame of the Peristaltic pump See Replace the Pump Tubes p 59 Press 4 x Exit 3 2 2 Fill System Verification Service Manual filling Enter 3 2 2 5 Fill System Progre...

Страница 63: ... containers to mix reagents or standard solution If the calibration factor is too high do the following 1 Check the programmed standard See chap 9 5 1 2 p 81 2 Prepare a new standard solution with demineralized water use SWAN stock solution only 3 Clean all canisters and suction lances with a mix of demineral ized water and one percent hydrochloric acid 4 Prepare new reagents with SWAN original re...

Страница 64: ...balance E and set the balance to zero 3 Unscrew and remove the tube fitting C from the photometer to disconnect tube No 7 The sample contained in the photometer will flow out 4 Put the tube into the beaker 5 Navigate to menu Maintenance Service Manual Filling and press Enter 6 Select Position and press Enter 7 Set the 6 way valve to position 1 with the or key The positions 1 to 4 of the 6 way valv...

Страница 65: ...2 3 and 4 If the reagent volume is below 2 g check the tube connections for leakage check if a tube is damaged i e kniked Replace the pump tubes of the peristaltic pump see Tube Re placement p 59 Replace the 6 way valve see enclosed installation instruction 7 2 Grab Sample The grab sample function is normally used to measure an external sample But it can be used for verification as well If the gra...

Страница 66: ...d i e Sample Flow low Such Errors are marked E0xx bold and orange Errors which indicate a hardware failure of the instrument Such Errors are marked E0xx bold and red Error or fatal Error Error not yet acknowledged Check Pending Errors 1 1 5 and take corrective action Reagent level low Indicates the remaining reagent in percent Navigate to menu Messages Pending Errors Press ENTER to acknowledge the...

Страница 67: ... value E008 Sample Temp low check process check programmed value E009 Sample Flow high check inlet pressure re adjust sample flow check programmed value 5 3 1 3 2 p 88 E010 Sample Flow low check inlet pressure re adjust sample flow clean instrument check programmed value 5 3 1 3 35 p 88 E012 Temp disconnected shut off power check wiring of photometer see Connection Diagram p 29 E013 Case Temp high...

Страница 68: ...nection E024 Input active See If Fault Yes is programmed in Menu 5 3 4 p 93 E026 IC LM75 call service E028 Signal output open check wiring on signal outputs 1 and 2 E030 I2C Rovalve call service E031 Calibration Recout call service E032 Wrong Frontend call service E033 Sample Flow 1 low Sample Sequencer See operating manual Sample Sequencer If 2nd Sample Stream option is installed see E010 E034 Sa...

Страница 69: ...e Flow 6 low Sample Sequencer See operating manual Sample Sequencer E049 Power on none normal status E050 Power down none normal status E065 Reagent low Observe the decreasing number on the screen indicating for how many hours the reagent lasts Refill reagents on time See Refill or replace Reagents p 49 Error Description Corrective action ...

Страница 70: ...according to Stop of Operation for Mainte nance p 48 2 Remove the protection cap and all pump tubes as described in Dismount pump tubes p 60 3 Unscrew the 4 screws of the peristaltic pump housing and re move the cover 4 Disconnect the motor connector A 5 Feed the cable into the housing through one of the PG7 cable glands 6 Connect the cable to the terminal block of the peristaltic pump ac cording ...

Страница 71: ...g installation relay 1 relay 2 alarm relay When a fuse has blown find out the cause and fix it before replacing it with a new one Use tweezers or needle nosed pliers to remove the defective fuse Use original fuses provided by SWAN only A B C D E F G AC variant 1 6 AT 250 V Instrument power supply DC variant 3 15 AT 250 V Instrument power supply 1 0 AT 250V Relay 1 1 0 AT 250V Relay 2 1 0 AT 250V A...

Страница 72: ...u 3 Maintenance is for service Calibration simulation of outputs and set time date Please protect with password Menu 4 Operation is for the user allowing to set limits alarm values etc The presetting is done in the menu Installation only for the System engineer Please protect with password Menu 5 Installation Defining assignment of all inputs and out puts measuring parameters interface passwords e...

Страница 73: ... Days Hours Minutes Seconds 2 1 5 1 2 1 5 Sensors FOME Sensor Current Value ppb 2 2 2 2 1 Raw value V Absorbance Cal History Number 2 2 1 4 1 2 2 1 4 Date Time Slope Ver History Number 2 2 1 5 1 2 2 1 5 Date Time Absorbance Reference value Miscellaneous Case Temp 2 2 2 1 2 2 2 State Machine Sample Sample ID 2 3 1 2 3 Temperature Sample Flow I O State Alarm Relay 2 4 1 2 4 Relay 1 2 2 4 2 Input Sig...

Страница 74: ... 3 2 3 2 Simulation Alarm Relay 3 3 1 3 3 Relay 1 3 3 2 Relay 2 3 3 3 Signal Output 1 3 3 4 Signal Output 2 3 3 5 Magnetic valve 1 3 3 6 Magnetic valve 2 3 3 7 Stirrer 3 3 8 Set Time Date Time 3 4 Grab Sample 4 1 Sensors Filter Time Const 4 2 1 4 2 Hold after Cal 4 2 2 Relay Contacts Alarm Relay Alarm Si 1 Si 2 Alarm High 4 3 1 1 1 4 3 4 3 1 4 3 1 1 Alarm Low 4 3 1 1 25 Hysteresis 4 3 1 1 35 Delay...

Страница 75: ...2 2 1 5 2 5 2 1 5 2 2 Current Loop 5 2 1 2 5 2 2 2 Function 5 2 1 3 5 2 2 3 Scaling Range Low 5 2 x 40 12 10 5 2 x 40 Range High 5 2 x 40 22 20 Signal Sequencer Parameter 5 2 4 1 5 2 4 Current Loop 5 2 4 2 Function 5 2 4 3 Scaling Range Low 5 2 4 40 10 5 2 4 40 Range High 5 2 4 40 20 Relay Contacts Alarm Relay Alarm Si 1 Si 2 Alarm High 5 3 1 1 1 5 3 5 3 1 5 3 1 1 Alarm Low 5 3 1 1 25 Hysteresis 5...

Страница 76: ...3 50 Input Active 5 3 4 1 5 3 4 Signal Outputs 5 3 4 2 Output Control 5 3 4 3 Fault 5 3 4 4 Delay 5 3 4 5 Miscellaneous Language 5 4 1 5 4 Set defaults 5 4 2 Load Firmware 5 4 3 Password Messages 5 4 4 1 5 4 4 Maintenance 5 4 4 2 Operation 5 4 4 3 Installation 5 4 4 4 Sample ID 5 4 5 Line Break Detection 5 4 6 Interface Protocol 5 5 1 only with RS485 5 5 Device Address 5 5 21 interface Baud Rate 5...

Страница 77: ... buffer 2 Diagnostics In diagnostics mode the values can only be viewed not modified 2 1 Identification Designation Designation of the instrument Version Firmware of the instrument e g V6 22 01 22 2 1 3 Peripherals 2 1 3 1 PeriClip Firmware of peristaltic pump e g 1 06 RoValve Firmware of rotary valve 6 way valve e g 1 60 2 1 4 Factory Test Test date of instrument and motherboard 2 1 5 Operating T...

Страница 78: ... 23 are assigned to the measuring cycle Number 24 is assigned to the manual filling function Number 25 31 are assigned to the calibration procedure Number 32 35 are assigned to the verifying procedure 2 3 Sample 2 3 1 Sample ID Review the programmed code The code is defined by the user to identify the sample point in the plant Temperature Shows the Actual temperature in C Sample flow Shows the act...

Страница 79: ...he instruction on the screen See Verification p 52 3 2 2 Fill System Activates the reagent pump and fills all tubes from the container to the 6 way valve 3 2 3 Manual Filling In the menu Manual filling the position of the 6 way valve can be set manually and the peristaltic pump can be switched on and off 3 2 3 1 Position Set the position of the 6 way valve 3 2 3 2 Pump Switch the peristaltic pump ...

Страница 80: ...n on the screen See Grab Sample Measurement p 47 4 2 Sensors 4 2 1 Filter Time Constant Used to damp noisy signals The higher the fil ter time constant the slower the system reacts to changes of the measured value Range 5 300 Sec 4 2 2 Hold after Cal Delay permitting the instrument to stabilize again after calibration During calibration verification or grab sample plus hold time the signal outputs...

Страница 81: ...d with yes the complete logger data is deleted A new data series is started 5 Installation 5 1 Sensors 5 1 1 Ref Verification Set absorbance value of verification kit according to label Range 0 150 0 600 5 1 2 Standard Set the value in ppb of the standard you use for calibra tion Range 50 ppb 5 ppm 5 1 3 Blank If the reagents contain a known amount of Silica Blank can be used to shift the zero poi...

Страница 82: ... are measured whereas the samples streams 1 3 and 5 are switched off Sample streams which are switched off are marked with an x behind the measuring value on the AMI Silica display Mode Fieldbus The AMI Silica is controlled via fieldbus Mode External In the mode external the AMI Silica works as a slave 2nd Sample Stream Option The 2nd Sample Stream option is switched between sample stream 1 and 2 ...

Страница 83: ...nu Signal Output 1 and Signal Output 2 is equal For reason of simplicity only the menu numbers of Signal Output 1 are used in the following 5 2 1 1 Parameter Assign one of the process values to the signal output Available values Temperature Sample Flow Si 1 5 2 1 2 Current Loop Select the current range of the signal output Make sure the connected device works with the same current range Available ...

Страница 84: ...r or logarithmic scale In addition the midpoint for the bilinear scale Parameter Temperature 5 2 1 40 10 Range low 30 C to 120 C 5 2 1 40 20 Range high 30 C to 120 C Parameter Sample Flow 5 2 1 40 11 Range low 0 600 B s 5 2 1 40 21 Range high 0 600 B s A B linear bilinear X Measured value X Measured value logarithmic 20 0 0 0 1 0 2 0 3 0 4 0 5 10 12 0 20 mA 0 4 4 20 mA mA X A B 20 1 0 1 2 3 4 10 1...

Страница 85: ...oller will minimize the steady state error If the reset time is set to zero the I controller is switched off Parameters setpoint P Band reset time PD controller The combination of a P controller with a D controller will minimize the response time to a fast change of the process value If the derivative time is set to zero the D controller is switched off Parameters setpoint P Band derivative time P...

Страница 86: ... 2 1 43 Control Parameters Si 1 5 2 1 43 12 Setpoint 0 ppb 5 ppm 5 2 1 43 22 P Band 0 ppb 5 ppm 5 2 1 43 3 Reset time The reset time is the time till the step response of a sin gle I controller will reach the same value as it will be suddenly reached by a P controller Range 0 9 000 sec 5 2 1 43 4 Derivative time The derivative time is the time till the ramp response of a single P controller will r...

Страница 87: ... like defective sensors or electronic parts High case temperature Lack of reagents Process values out of programmed ranges Program alarm levels hysteresis values and delay times for the fol lowing parameters Alarm Si 1 Sample Temp Sample Flow Case Temp high Case Temp low 5 3 1 1 Alarm Si 1 5 3 1 1 1 Alarm High If the measured value rises above the alarm high value the alarm relay is activated and ...

Страница 88: ... will always be indicated in the display pending error list saved in the message list and the logger Available values Yes or no Note Sufficient flow is essential for a correct measurement We recommend to program yes 5 3 1 3 2 Alarm High If the measuring values rises above the programmed value E009 will be issued Range 100 600 B s 5 3 1 3 35 Alarm Low If the measuring values falls below the program...

Страница 89: ... following 5 3 2 20 Parameter select a process value 5 3 2 300 Setpoint If the measured value rises above respectively falls below the set point the relay is activated 5 3 2 401 Hysteresis within the hysteresis range the relay does not switch This prevents damage of relay contacts when the measured value fluctuates around the alarm value 5 3 3 50 Delay Duration the activation of the alarm relay is...

Страница 90: ...change Range 0 600 Sec 5 3 2 32 30 Response time Minimal time the metering device needs to react Range 0 240 Sec 5 3 2 32 4 Control Parameters Range for each Parameter same as 5 2 1 43 p 86 Examples of metering devices that are pulse frequency driven are the classic membrane pumps with a potential free triggering input Dosing is controlled by the repetition speed of dosing shots 5 3 2 32 21 Pulse ...

Страница 91: ...elay stays active Range 5 32 400 Sec 5 3 2 54 Delay during run time plus the delay time the signal and control out puts are held in the operating mode programmed below Range 0 6 000 Sec 5 3 2 6 Signal Outputs Select operating mode of the signal output 5 3 2 7 Output Control Select operating mode of the controller output 5 3 2 1 Function Timer 5 3 2 24 Interval Cont Signal outputs continue to issue...

Страница 92: ...terval 5 3 2 7 Output Control see Interval The relay contact can be activated at one or several days of a week The daily starting time is valid for all days 5 3 2 342 Calendar 5 3 2 342 1 Start time The programmed start time is valid for each of the pro grammed days To set the start time see 5 3 2 341 p 92 Range 00 00 00 23 59 59 5 3 2 342 2 Monday Possible settings on or off to 5 3 2 342 8 Sunday...

Страница 93: ...am Option via an external device 5 3 4 1 Active Define when the input should be active The measurement is interrupted during the time the input is active 5 3 4 2 Signal Outputs Select the operation mode of the signal outputs when the relay is active 5 3 4 3 Output Control relay or signal output 5 3 3 1 Function End of Batch 5 3 3 1 Function Channel Selection Relay 2 inactive Channel 1 is selected ...

Страница 94: ...re kept in memory In parts Communication parameters are kept in memory All other values are set back to default values Completely Sets back all values including communication parameters 5 4 3 Load Firmware Firmware updates should be done by instructed ser vice personnel only No No message is issued in pending error list and the alarm relay does not close when input is active Message E024 is stored...

Страница 95: ...ection If activated error message E028 is shown in case of line break on signal outputs 1 and 2 5 5 Interface Select one of the following communication protocols Depending on your selection different parameters must be defined 5 5 1 Protocol Profibus 5 5 20 Device address Range 0 126 5 5 30 ID Nr Range Analyzer Manufacturer Multivariable 5 5 40 Local operation Range Enabled Disabled 5 5 1 Protocol...

Страница 96: ...N ON LINE SILICA Reagent 1b for AMI Silica Sodium hydroxide pellets Catalogue No Product name Part of Article No A 85 420 560 OXYCON ON LINE SILICA Reagent 2 for AMI Silica Sulfuric acid 25 Catalogue No Product name Part of Article No A 85 420 560 OXYCON ON LINE SILICA Reagent 3 for AMI Silica Oxalic acid dihydrate Catalogue No Product name Part of Article No A 85 420 560 OXYCON ON LINE SILICA Rea...

Страница 97: ...nterval 10 min Channels 1 Channel Selection internal Signal Output 1 Parameter Si 1 Current loop 4 20 mA Function linear Scaling Range low 0 0 ppb Scaling Range high 1 00 ppm Signal Output 2 Parameter Temperature Current loop 4 20 mA Function linear Scaling Range low 0 0 C Scaling Range high 50 0 C Alarm Relay Alarm Si 1 Alarm high 5 00 ppm Alarm low 0 0 ppb Hysteresis 10 ppb Delay 5 s Sample Temp...

Страница 98: ...vative Time 0 s Settings Control Parameters Control Timeout 0 min Settings Actuator Time proportional Cycle time 60 s Response time 10 s Settings Actuator Motor valve Run time 60 s Neutral zone 5 If Function Timer Mode Interval Interval 1 min Mode daily Start time 00 00 00 Mode weekly Calendar Start time 00 00 00 Calendar Monday to Sunday Off Run time 10 s Delay 5 s Signal output cont Output Contr...

Страница 99: ... 80 I I O State 79 Input 12 31 93 Instrument Setup 19 Interface HART 36 Interface Modbus 35 Interface Profibus DP 35 Interface RS485 35 36 Interface USB 36 L Log Interval 81 Logger 81 M Manual Filling 79 Measurement cycle 14 Measurement interval 50 Messumformer 18 Mode External 82 Mode Fieldbus 82 Mode Internal 82 Mounting requirements 20 O On site requirements 17 19 Oxalic Acid Reagent 3 49 51 P ...

Страница 100: ...51 Reagent consumption 50 Reagents 19 Relay 11 Run in period 19 S Safety Features 12 Sample Flow Establish 38 Signal Outputs 11 34 Signal Sequencer 86 Silica Measurement 11 Simulation 80 Sulfuric Acid Reagent 2 49 51 T Terminals 29 31 32 34 35 Transmitter 18 W Wire 27 ...

Страница 101: ...A 96 250 671 070222 AMI Silica Notes 101 13 Notes ...

Страница 102: ... ast e t W a e r E f u e n t s P o o l S a n i t a r y Swan Analytical Instruments CH 8340 Hinwil www swan ch swan swan ch Swan Products Analytical Instruments for Swan is represented worldwide by subsidiary companies and distributors and cooperates with independent representatives all over the world For contact in formation please scan the QR code ...

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