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Swan Analytical Instruments AMI Codes-II O3, Руководство оператора

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A-96.250.881 / 070622

AMI Codes-II O3

Troubleshooting

58

7.2. Calibration Errors

7.2.1

Process Calibration DIS

Possible error

message

Slope error:

7.3. Verification Errors

Possible error

message

Invalid zero measurement:

Verification error

Possible cause

Corrective Action

Wrong manual measure

-

ment.

Repeat the manual measurement.

Use fresh reagents.

Wrong reagent mixture

Reagents not 

completely solved in 

water.

Reagents older than 30 

days.

Make a correct mixture.

Mix long and intensively.

Possible cause

Corrective Action

Gas bubble in the pho

-

tometer.

Rinse the photometer with sample for 

1-2 minutes and repeat the verifica

-

tion.

Possible cause

Corrective Action

Deviation between mea

-

sured value and refer

-

ence value is too high

Clean the verification filters 

according to 

Cleaning, p. 48

 and 

repeat the verification.

If filter cleaning does not result in a 

successful verification, clean and 

rinse the photometer according to 

Cleaning the Photometer, p. 51

 and 

repeat the verification.

If the problem perists, call service.

Содержание AMI Codes-II O3

Страница 1: ...Operator s Manual Firmware V6 21 and higher AMI Codes II O3 A 96 250 881 070622...

Страница 2: ...y trained staff of technical specialists around the world For any technical question contact your nearest Swan representative or the manufacturer Swan Analytische Instrumente AG Studbachstrasse 13 834...

Страница 3: ...3 4 Installation of Flow Cell 21 3 5 Electrical Connections 22 3 5 1 Connection Diagram 24 3 5 2 Power Supply 25 3 5 3 Opening the peristaltic pump housing 26 3 6 Input 27 3 7 Relay Contacts 27 3 7 1...

Страница 4: ...assemble the Flow Cell 52 6 7 2 Assemble the Flow Cell 53 6 8 Tube Replacement 54 6 8 1 Replace the Pump Tubes 54 6 9 Longer Stop of Operation 56 7 Troubleshooting 57 7 1 General Instructions 57 7 2 C...

Страница 5: ...A 96 250 881 070622 AMI Codes II O3 5 10 Material Safety Data Sheets 85 10 1 Reagents 85 11 Default Values 86 12 Index 89 13 Notes 91...

Страница 6: ...structions are given throughout this manual at the re spective locations where observation is most important Strictly fol low all safety instructions in this publication Target audience Operator Quali...

Страница 7: ...ention instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the equipment min...

Страница 8: ...70622 AMI Codes II O3 Safety Instructions 8 Warning Signs The warning signs in this manual have the following meaning Electrical shock hazard Corrosive Harmful to health Flammable Warning general Atte...

Страница 9: ...ili ty for any claim resulting from unauthorized modification or alter ation WARNING Electrical Shock Hazard If proper operation is no longer possible the instrument must be disconnected from all powe...

Страница 10: ...he instrument WARNING Health hazard Some reagents are etching and can cause severe burns or eye damage For safe handling of the reagents you must read and under stand the instructions in this manual a...

Страница 11: ...ource or as a current sink selectable via switch Relays Two potential free contacts programmable as limit switches for mea suring values controllers or timer for system cleaning with automatic hold fu...

Страница 12: ...flow regulating valve D so that always a small part of the sample flows through the overflow tube B into the drain H A part of the sample flows through the photometer inlet C into the mix ing chamber...

Страница 13: ...let Flow regulating valve Mixing chamber Sample inlet Filter vessel no filter Constant head drain I J K L M N O P Photometer drain Oxycon on line DPD reagent Oxycon on line Ozone reagent Reagent level...

Страница 14: ...ents the sample which flows continuously through the photometer A short time before the measurement starts a zero point measurement is performed Then the peristaltic pump starts and a small portion of...

Страница 15: ...4X 10 to 50 C 30 to 85 C 10 90 rel non condensing backlit LCD 75 x 45 mm Sample requirements Flow rate Temperature Inlet pressure Outlet pressure min 10 l h 5 50 C 0 15 2 bar pressure free Note No oil...

Страница 16: ...I O3 Product Description 16 Dimensions Panel Dimensions Screws Weight stainless steel 400x850x200 mm 8 mm diameter 14 0 kg 13 mm 0 51 4 x dia 10 mm 0 39 850 mm 33 46 824 mm 32 44 374 mm 14 72 400 mm 1...

Страница 17: ...A B C D E F G Panel Transmitter Peristaltic pump Oxycon on line DPD reagent Oxycon on line Ozone reagent Constant head Flow regulating valve H I J K L M Sample inlet Filter vessel no filter Photometer...

Страница 18: ...e p 19 Electrical Wiring Do not switch on the Instrument until all electrical connections have been completed Connect all external devices like limit switches current loops and pumps Connect power cor...

Страница 19: ...so that the display is at eye level For the installation a kit containing the following installation ma terial is available 4 Screws 8x60 mm 4 Dowels 4 Washers 8 4 24 mm Mounting requirements The ins...

Страница 20: ...f the photometer outlet contains DPD At no means recirculate it into the water system Connect the 1 2 tubes F to the hose nozzles E and place them into a pressure free drain with sufficient capacity A...

Страница 21: ...he AMI Codes II O3 is not installed To install the constant head tube proceed as follows 1 Unpack the constant head tube C 2 Push the constant head tube into the flow cell block E 3 Put the constant h...

Страница 22: ...operate the instrument from a power outlet which has a ground connection Make sure the power specification of the instrument corre sponds to the power on site Cable thicknesses In order to comply with...

Страница 23: ...sure that the devices connected to the following contacts are disconnected from the power before resuming installation relay 1 relay 2 alarm relay WARNING To prevent from electrical shock do not conne...

Страница 24: ...lation 24 3 5 1 Connection Diagram CAUTION Use only the terminals shown in this diagram and only for the mentioned purpose Use of any other terminals will cause short circuits with possible correspond...

Страница 25: ...und has to be connected to the grounding terminal Installation requirements The installation must meet the following requirements Mains cable to comply with standards IEC 60227 or IEC 60245 flammable...

Страница 26: ...nte nance p 42 2 Remove the protection cap and all pump tubes as described in Dismount pump tubes p 55 3 Unscrew the 4 screws of the peristaltic pump housing and re move the cover 4 Disconnect the mot...

Страница 27: ...3 7 Relay Contacts 3 7 1 Alarm Relay Note Max load 1 A 250 VAC Alarm output for system errors Error codes see Troubleshooting p 57 Note With certain alarms and certain settings of the AMI transmitter...

Страница 28: ...atus of the relays described below For programming see Menu Installation 5 3 2 and 5 3 3 p 77 Relay config Terminals Jumper pos Description Relay configuration Normally Open 6 7 Relay 1 8 9 Relay 2 In...

Страница 29: ...in paral lel to the load A snubber circuit is not necessary if an AMI relaybox is used Resistive load Resistive loads max 1 A and control signals for PLC impulse pumps and so on can be connected with...

Страница 30: ...utput 1 Terminals 14 and 13 Signal output 2 Terminals 15 and 13 For programming see Program List and Explanations p 69 Menu Installation 3 9 Interface Options The slot for interfaces can be used to ex...

Страница 31: ...rresponding installation instruction Note Max burden 510 Third signal output 0 4 20 mA PCB 3 9 2 Profibus Modbus Interface Terminal 37 PB Terminal 38 PA To connect several instruments by means of a ne...

Страница 32: ...onsult the HART manual HART Interface PCB 3 9 4 USB Interface The USB Interface is used to store Logger data and for Firmware up load For detailed information see the corresponding installation in str...

Страница 33: ...ng 4 1 Prepare Reagents 1 Prepare reagents See Refill or replace Reagents p 43 2 Insert the suction lances into the canisters 4 2 Peristaltic Pump The instrument is delivered with opened occlusion fra...

Страница 34: ...en the flow regulating valve E and wait until the flow cell is completely filled 2 Adjust overflow tube to the marked level 3 Switch on power 4 Adjust the sample flow so that always a small part of th...

Страница 35: ...nuously for 1 hour 4 5 Programming Programming Program all parameters for external devices interface recorders etc Program all parameters for instrument operation disinfectant limits alarms Program th...

Страница 36: ...er to determine the sam ple disinfectant concentration Take the sample directly from the flow cell Determine the sample disinfectant value by 3 manual DPD mea surements Calculate the average value Com...

Страница 37: ...changes to move back to the previous menu level B to move DOWN in a menu list and to decrease digits C to move UP in a menu list and to increase digits D to open a selected sub menu to accept an entry...

Страница 38: ...agent low indicates remaining reagents in 17 340 ml D Keys locked transmitter control via Profibus E Time F Process value with time stamp G Sample flow in B s H Relay status upper lower limit not yet...

Страница 39: ...ameters that might need to be modified during daily routine Normally password protected and used by the process operator Subset of menu 5 Installation but process related Menu Installation 5 For initi...

Страница 40: ...s the new parameter is set 5 1 2 Sensors Sensor type FOME Temperature NT5K Standards Disinf Free chlorine 4 4 1 Logger Log interval 30 min Clear logger no 4 1 3 Logger Clear logger no Log interval 30m...

Страница 41: ...otometer with verification kit Verification p 46 Yearly Exchange reagent pump tubes see Tube Replacement p 54 By occurrence E010 Sample flow low Check sample flow see also Troubleshooting p 57 E020 FO...

Страница 42: ...into a bucket with demineralized water 2 Start Fill system The reagent tubes are flushed with water 3 Remove the suction lances from the water 4 Start Fill system again The water will be pumped out of...

Страница 43: ...cessary security measures when manipulating dangerous chemicals Read the Material Safety Data Sheets carefully Canister set up Canister almost empty Maintenance E065 Reagents low and the remaining rea...

Страница 44: ...b the canisters must be consumed within 30 days Contents of the reagent set A 85 410 210 Reagent set for the measurement of ozone Oxycon On Line DPD 3 bottles Oxycon On Line Buffer O3 3 bags Personal...

Страница 45: ...crew cover insert the suction lance A and tighten the screw cover Prepare Oxycon On line Buffer O3 1 Rinse the canister F labelled OXYCON ON LINE Ozone Re agent with demineralized water 2 Fill the can...

Страница 46: ...filters were chosen to lie in the center and at the upper limit of the measurement range of the AMI Codes II O3 The verification procedure confirms the photometric accuracy and linearity of the core c...

Страница 47: ...for visible contaminations dust or stains as these can prevent a successful verification If nec essary apply the cleaning procedure described in Cleaning p 48 To start the verification follow the dia...

Страница 48: ...erification history Can be reviewed in menu 2 2 1 5 Diagnostics Sensors Photometer Ver History Cleaning Use the provided wipes or other lint free non abrasive optical grade wipes If you choose dry wip...

Страница 49: ...l surfaces Dirt or scratches on the optical surfaces change the optical properties of the verification filters and may make recertifica tion or even replacement of the verification filters necessary R...

Страница 50: ...ion is only possible with a process value higher than 10 ppb ozone Please note that due to the low stability of the ozone a process calibration with an elevated concentration is pre ferred Use CHEMATE...

Страница 51: ...top of Opera tion for Maintenance p 42 Material Small brush Procedure 1 Close the flow regulating valve A 2 Wait until the sample flow through the photometer has stopped 3 Unscrew the screw plug B fro...

Страница 52: ...glass parts Use soft detergent and rinse well Eliminate lime deposits with a common household deliming agent in standard concentra tion Do not drop the constant head tube 6 7 1 Disassemble the Flow Ce...

Страница 53: ...er 6 Rinse well with demineralized water 6 7 2 Assemble the Flow Cell 1 Replace the gasket D before reassembling the flow cell Note A film of teflon paste e g Fomblin from Solvay Solexis on the gasket...

Страница 54: ...f reagents possible If the occlusion frames are opened during operation already mixed reagents will flow back into the reagent canisters and pol lute the reagents Never open the occlusion frames if th...

Страница 55: ...the rotor C by pulling the com plete occlusion frames B out of the holder 5 Disconnect the reagent tubes from the old pump tubes and con nect them to the new pump tubes 6 Install the new pump tubes by...

Страница 56: ...Start Fill system The reagent tubes are flushed with water 3 Remove the suction lance from the water 4 Start Fill system again The water will be pumped out of the reagent tubes 5 Stop sample flow 6 Wa...

Страница 57: ...o Diagnostic values Zero photometry 10 000 16 000 Hz mostly near 16 000 Hz Slope photometry 0 5 2 0 Frequently asked questions Problem Possible Reasons Unstable values Sample taken too close to feedin...

Страница 58: ...Reagents older than 30 days Make a correct mixture Mix long and intensively Possible cause Corrective Action Gas bubble in the pho tometer Rinse the photometer with sample for 1 2 minutes and repeat t...

Страница 59: ...vered i e Sample Flow low Such Errors are marked E0xx bold and orange Errors which indicate a hardware failure of the instrument Such Errors are marked E0xx bold and red Error or fatal Error Error not...

Страница 60: ...clean instrument see Cleaning the Photometer p 51 check programmed value in menu 5 3 1 3 x p 77 E013 Case Temp high check case environment temperature check programmed value in menu 5 3 1 5 p 77 E014...

Страница 61: ...l output open check wiring on signal outputs 1 and 2 E030 EEprom Frontend call service E031 Calibration Recout call service E032 Wrong Frontend call service E033 Power on none normal status E034 Power...

Страница 62: ...ng installation relay 1 relay 2 alarm relay When a fuse has blown find out the cause and fix it before replacing it with a new one Use tweezers or needle nosed pliers to remove the defective fuse Use...

Страница 63: ...can be modified Menu 3 Maintenance Calibration simulation of outputs and set time date Access by administrator and service Menu 4 Operation Allows to set limits alarms values etc Ac cess by administr...

Страница 64: ...es Seconds 2 1 5 1 2 1 5 Sensors Photometer Current Value 2 2 2 2 1 Raw value Absorbance Cal History Number 2 2 1 4 1 2 2 1 4 Date Time Slope Ver History Number 2 2 1 5 1 2 2 1 5 Date Time Absorbance...

Страница 65: ...u numbers 3 1 3 1 1 Slope Process Value 3 1 1 4 Service Verification Progress 3 2 1 1 3 2 3 2 1 Fill System Progress 3 2 2 5 3 2 2 Reagents Last change 3 2 3 Remaining days Change reagents 3 2 3 3 Sim...

Страница 66: ...old after Cal 4 1 3 Meas Interval 4 1 4 Relay Contacts Alarm Relay Alarm DIS Alarm High 4 2 1 1 1 4 2 4 2 1 4 2 1 1 Alarm Low 4 2 1 1 26 Hysteresis 4 2 1 1 36 Delay 4 2 1 1 46 Relay 1 2 Setpoint 4 2 x...

Страница 67: ...igh 5 2 x 40 x Relay Contacts Alarm Relay Alarm DIS Alarm High 5 3 1 1 1 5 3 5 3 1 5 3 1 1 Alarm Low 5 3 1 1 x Hysteresis 5 3 1 1 x Delay 5 3 1 1 x Sample Flow Flow Alarm 5 3 1 3 1 5 3 1 3 Alarm High...

Страница 68: ...rs 5 4 Set defaults 5 4 2 Load Firmware 5 4 3 Access Administrator Name 5 4 4 5 4 4 1 Function Password User 1 4 Name 5 4 4 x Function Password Sample ID 5 4 5 Line Break Detection 5 4 6 Interface Pro...

Страница 69: ...to save the newest error circular buffer 1 4 Audit Trail Shows the audit trail event menu date and time of issue 96 events are memorized Then the oldest event is cleared to save the newest one circula...

Страница 70: ...ion Deviation between the measured value and the reference value in 2 2 3 Miscellaneous 2 2 3 1 Case Temp Shows the current temperature in C inside the transmitter 2 3 Sample 2 3 1 Sample ID Shows the...

Страница 71: ...3 2 3 3 Change reagents Resets the counter and saves the date of the new filling 3 3 Simulation To simulate a value or a relay state select the alarm relay relay 1 or 2 signal output 1 or 2 with the...

Страница 72: ...rval Measurement interval for disinfectants Range 5 to 10 min 4 2 Relay Contacts See 5 3 Relay Contacts p 76 4 3 Logger The instrument is equipped with an internal logger The data can be copied to a P...

Страница 73: ...Note The navigation in the menu Signal Output 1 and Signal Output 2 is equal For reason of simplicity only the menu numbers of Signal Output 1 are used in the following 5 2 1 1 Parameter Assign one of...

Страница 74: ...linear or logarithmic scale In addition the midpoint for the bilinear scale Parameter DIS 5 2 1 40 10 Range low 0 0 500 0 ppb 5 2 1 40 20 Range high 0 0 500 0 ppb Parameter Sample flow 5 2 1 40 13 Ra...

Страница 75: ...controller The combination of a P controller with a D controller will minimize the response time to a fast change of the process value If the derivative time is set to zero the D controller is switch...

Страница 76: ...by a P controller Range 0 9 000 sec Derivative time The derivative time is the time till the ramp response of a single P controller will reach the same value as it will be suddenly reached by a D cont...

Страница 77: ...m Program if the alarm relay should be activated if there is a flow alarm Choose between yes or no The flow alarm will always be indicated in the display pending error list saved in the message list a...

Страница 78: ...ely falls below the set point the relay is activated 5 3 2 400 Hysteresis within the hysteresis range the relay does not switch This prevents damage of relay contacts when the measured value fluctuate...

Страница 79: ...g devices that are pulse frequency driven are the classic membrane pumps with a potential free triggering input Dosing is controlled by the repetition speed of dosing shots 5 3 2 32 21 Pulse frequency...

Страница 80: ...controller output The relay contact can be activated daily at any time of a day 5 3 2 341 Start time to set the start time proceed as follows 1 Press Enter to set the hours 2 Set the hour with the or...

Страница 81: ...y see Interval 5 3 2 6 Signal Outputs see Interval 5 3 2 7 Output Control see Interval The relay will be switched via the Profibus input No further parame ters are needed This function is only availab...

Страница 82: ...tion parameters are kept in memory All other values are set back to default values Completely Sets back all values including communication pa rameters 5 4 3 Load Firmware Firmware updates should be do...

Страница 83: ...Only an administrator can assign user rights for the users 1 to 4 5 4 4 1 3 Password The password is set to 0000 by default If an adminis trator password different from 0000 is set it is not longer p...

Страница 84: ...on protocols Depending on your selection different parameters must be defined 5 5 1 Protocol Profibus 5 5 20 Device address Range 0 126 5 5 30 ID Nr Range Analyzer Manufacturer Multivariable 5 5 40 Lo...

Страница 85: ...y Data Sheets 10 1 Reagents Catalogue No A 85 410 210 Product name OXYCON ON LINE DPD Catalogue No A 85 410 210 Product name OXYCON ON LINE Buffer O3 Download MSDS The current Material Safety Data She...

Страница 86: ...nstallation Sensors Disinf Ozone Reag expiry warning yes Signal Output 1 Parameter DIS Current loop 4 20 mA Function linear Scaling Range low 0 0 ppb Scaling Range high 500 0 ppb Signal Output 2 Param...

Страница 87: ...ntrol Parameters Setpoint 200 B s Settings Control Parameters P band 20 B s Common settings Settings Control Parameters Reset time 0 s Settings Control Parameters Derivative Time 0 s Settings Control...

Страница 88: ...88 Input Active when closed Signal Outputs hold Output Control off Fault no Delay 10 s Miscellaneous Language English Set default no Load firmware no Access Password Administrator 0000 Access Passwor...

Страница 89: ...I Input 11 27 Instrument Setup 18 Interface HART 32 Modbus 31 Profibus 31 USB 32 L Logger 72 86 M Measurement interval 44 72 86 Measuring range 15 Message List 69 Modbus 31 Mounting requirements 19 O...

Страница 90: ...AMI Codes II O3 Index A 96 250 881 070622 90 U USB Interface 32 V Ver History 70 Verification 46 71 W Wire 22 Z Zero photometry 57...

Страница 91: ...A 96 250 881 070622 AMI Codes II O3 Notes 91 13 Notes...

Страница 92: ...W ast e t W a e r E f u e n t s P o o l S a n i t a r y Swan Analytical Instruments CH 8340 Hinwil www swan ch swan swan ch Swan Products Analytical Instruments for Swan is represented worldwide by s...

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