Shodex RSpak JJ-50 2D Скачать руководство пользователя страница 1

ver.211124E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

Operation Manual 

Shodex

 RSpak

 JJ-50 2D 

 

(Please read this manual carefully to achieve the best and consistent column performance for a long time) 

 
 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

· Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 RSpak

 JJ-50 2D is a multimode (reversed phase 

and anion exchange modes) column filled with spherical porous particles of polyvinyl alcohol modified with 
quaternary ammonium group. It is an ideal column for analyzing complex samples that contain mixture of neutral 
and ionic substances.   
 

2. Column Components   

 

 
 
 

               

 

 

 
 
 
 
 
 
 

 
3. Column Specifications 

Product 

Code 

Product Name 

Column Size (mm) 

Particle Size 

(

μ

m) 

Theoretical Plate Number 

(Per Column) 

I.D. Length 

F7008220 

RSpak JJ-50 2D 

2.0 150 

 3,500   

 

Base Material 

: Spherical porous particles of polyvinyl alcohol modified with quaternary ammonium group

 

Column Housing  : SUS-316   
Screw Type 

: Internally-threaded type No.10-32 UNF 

Shipping Solvent : Water/Acetonitrile = 40/60 
 

 

 

Содержание RSpak JJ-50 2D

Страница 1: ...or any damage 2 Please check if product name and serial number written on the column package column name tag and enclosed Certificate of Analysis CoA are matching and correct 1 Introduction Thank you for purchasing the Shodex product Shodex RSpak JJ 50 2D is a multimode reversed phase and anion exchange modes column filled with spherical porous particles of polyvinyl alcohol modified with quaterna...

Страница 2: ... grade organic solvent whenever possible Solvents left in an opened bottle for a long time should not be used The content may have been changed absorbed moisture or has been contaminated Always use freshly prepared solvents Solvents stored for a long time may have changed their compositions and may influence elution patterns and or damage the column Note Use of on line degasser is recommended 6 Sa...

Страница 3: ...emperature return to room temperature before stopping the pump If the pump was stopped while the eluent inside the column was still hot as the eluent temperature decreases its volume also decreases This may result in creating an empty space in the column and deteriorates the column Note It is recommended to set the pump limiter to avoid exceeding the maximum pressure 7 3 Solvent Exchange 1 When re...

Страница 4: ...shing Solution Cleaning Time 1 H2O 6 min 2 0 1 M NaOH aq solution 75 min 3 H2O 12 min 4 Eluent 40 min Method 2 Adsorption of metal ions or in case Method 1 did not work Washing Solution Cleaning Time 1 H2O 6 min 2 0 1 M HNO3 aq solution 75 min 3 H2O 6 min 4 0 1 M NaOH aq solution 75 min 5 H2O 12 min 6 Eluent 40 min Method 3 Adsorption of hydrophobic compounds Washing Solution Cleaning Time 1 H2O 2...

Страница 5: ...late Number N 2 Asymmetry Factor Fas 10 Additional Warnings 1 Do not remove end fittings 2 Do not make a strong impact on the column Do not drop or hit the column on a hard surface Refer to the Shodex website https www shodex com for product details and their applications For additional assistance contact the distributor from whom you purchased the column or contact your regional Shodex support of...

Страница 6: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

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