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Shodex RSpak DM-614, Руководство по эксплуатации

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ver.210707E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

1 

Operation Manual 

Shodex

TM

 RSpak

TM

 DM-614 

 

（

Please read this manual carefully to achieve the best and consistent column performance for a long time

）

 

 

 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

· Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 RSpak

 DM-614 is a polymer-based reversed phase 

chromatography column. It can be used in a wide pH range from acidic to alkaline (pH 2 - 10). 
 

2. Column Components   

 

                 

 

 

 
 
 
 
 
 
 
 
 
 
3. Column Specifications 

Product 

Code 

Product Name 

Column Size (mm) 

Particle 

Size (

μ

m) 

Theoretical Plate Number 

(Per Column) 

I.D. Length 

F7001002 

RSpak DM-614 

6.0 150  10 

≥

 4,500 

F6700160 

RSpak DM-G 4A 

4.6  

10  12 

(Guard 

Column) 

 

Base Material 

: Spherical porous particles of polyhydroxymethacrylate

 

Column Housing  : SUS-316 
Screw Type 

: Internally-threaded type No.10-32 UNF 

Shipping Solvent : 5 mM Phosphoric Acid aq. Solution 
 
 
 
 
 
 
 
 

Содержание RSpak DM-614

Страница 1: ...1 Please visually inspect the package and outside of the column for any damage 2 Please check if product name and serial number written on the column package column name tag and enclosed Certificate of Analysis CoA are matching and correct 1 Introduction Thank you for purchasing the Shodex product Shodex RSpak DM 614 is a polymer based reversed phase chromatography column It can be used in a wide ...

Страница 2: ...ances may result in deterioration of the column and or they appear as noise on the chromatograms Filter the eluent with a 0 45 μm disposable filter to prevent the problems Attention Whenever water is required use ultra pure water freshly generated by a water purification system or water from a newly opened HPLC grade distilled water bottle Use HPLC grade organic solvent whenever possible Solvents ...

Страница 3: ... the end fitting and secure it with the male nut It is important that there is no extra space between the tubing and the column side of the end fitting Presence of an extra space will let the sample to spread out and may result in wide peaks 3 Set the initial flow rate at less than 0 3 mL min and start the system If using the column at an elevated temperature keep a low flow rate until the tempera...

Страница 4: ...the column If a guard column is used with the analytical column first remove the guard column and check the performance of the analytical column alone If the problem is solved most likely the cause is from the guard column In this case clean the guard column If the problem is not solved by removing the guard column clean both guard and analytical columns Make sure to clean the guard and the analyt...

Страница 5: ...late Number N 2 Asymmetry Factor Fas 10 Additional Warnings 1 Do not remove end fittings 2 Do not make a strong impact on the column Do not drop or hit the column on a hard surface Refer to the Shodex website https www shodex com for product details and their applications For additional assistance contact the distributor from whom you purchased the column or contact your regional Shodex support of...

Страница 6: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

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