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ver.220217E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

Operation Manual 

Shodex

 IC YK-421 

 

(Please read this manual carefully to achieve the best and consistent column performance for a long time) 

 

 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

·

 

Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 IC YK-421 is an ion chromatography column suitable 

for a simultaneous analysis of monovalent and divalent cations. It is applicable for non-suppressor type methods. 
It is also suitable for analysis of alkylamines as well as inorganic cations. 

 

2. Column Components   

 

 
 
 
 
 
 
 
 
 
 
 
 
3. Column Specifications 

Product 

Code 

Product Name 

Column Size (mm) 

Particle 

Size (

μ

m) 

Theoretical Plate Number 

(Per Column) 

I.D. Length 

F7120012 

IC YK-421 

4.6 125  5 

 2,800 

F6709608 

IC YK-G 

4.6  

10  5 

(Guard 

Column) 

 

Base Material 

: Spherical porous particles of silica modified with carboxyl group

 

Column Housing  : SUS-316 
Screw Type 

: Internally-threaded type No.10-32 UNF 

Shipping Solvent : Aqueous Solution containing 5 mM Tartaric Acid + 1 mM Dipicolinic Acid + 24 mM Boric Acid
 
 
 
 
 
 

Содержание IC YK-421

Страница 1: ...ease check if product name and serial number written on the column package column name tag and enclosed Certificate of Analysis CoA are matching and correct 1 Introduction Thank you for purchasing the Shodex product Shodex IC YK 421 is an ion chromatography column suitable for a simultaneous analysis of monovalent and divalent cations It is applicable for non suppressor type methods It is also sui...

Страница 2: ...rate and column temperature so that the column pressure remains below the usable maximum pressure Do not use chloric acid as it may cause corrosion of the stainless steel 5 Eluent Preparation 1 Degas the eluent fully to prevent the formation of air bubbles 2 Presence of small debris or insoluble substances may result in deterioration of the column and or they appear as noise on the chromatograms F...

Страница 3: ...ture and then gradually increase the flow rate to the desired 4 When replacing the shipping solvent with the eluent wash the column with the eluent for more than 60 minutes Caution Verify that there is no solvent leak It may cause electronic leakage rust and or chemical injury Attention Make sure not to let air bubbles enter the column while installing the column The air bubbles may damage the col...

Страница 4: ...mn outlet go directly into the waste container and not let the solution go through the detector Cleaning Method Method 1 Adsorption of hydrophobic compounds Set the flow rate at 0 3 mL min Introduce 50 mL of 5 mM aqueous tartaric acid solution acetonitrile 50 50 Method 2 Adsorption of hydrophilic compounds Set the flow rate at 0 3 mL min Introduce 50 mL of 50 mM aqueous tartaric acid solution 8 Co...

Страница 5: ...ct on the column Do not drop or hit the column on a hard surface Refer to the Shodex website https www shodex com for product details and their applications For additional assistance contact the distributor from whom you purchased the column or contact your regional Shodex support office https www shodex com en support_office list ...

Страница 6: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

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