Shodex HILICpac VG-50 4D Скачать руководство пользователя страница 1

ver.211105E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

Operation Manual 

Shodex

 HILICpak

 VG-50 4D, 4E 

 

Please read this manual carefully to achieve the best and consistent column performance for a long time

 

 

 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

· Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 HILICpak

 VG-50 series is a polymer-based HILIC     

column modified with amino group. The column is suitable for the analysis of saccharides and sugar alcohols. 
 

2. Column Components   
 
 
 

 

               

 

 

 
 
 
 
 
 
 
3. Column Specifications 

Product 

Code 

Product Name 

Column Size (mm) 

Particle 

Size (

μ

m) 

Theoretical Plate Number 

(Per Column) 

I.D. Length 

F7630200 

HILICpak VG-50 4D 

4.6 150 

 5,500   

F7630100 

HILICpak VG-50 4E 

4.6 250 

 7,500   

F6711100 

HILICpak VG-50G 4A 

4.6  

10 

(Guard 

Column) 

 

Base Material 

: Spherical porous particles of polyvinyl alcohol modified with amino group

 

Column Housing  : SUS-316   
Screw Type 

: Internally-threaded type No.10-32 UNF 

Shipping Solvent : Water/Acetonitrile = 20/80 
 
 
 
 
 
 

Содержание HILICpac VG-50 4D

Страница 1: ...nd outside of the column for any damage 2 Please check if product name and serial number written on the column package column name tag and enclosed Certificate of Analysis CoA are matching and correct 1 Introduction Thank you for purchasing the Shodex product Shodex HILICpak VG 50 series is a polymer based HILIC column modified with amino group The column is suitable for the analysis of saccharide...

Страница 2: ... μm disposable filter to prevent the problems Attention Whenever water is required use ultra pure water freshly generated by a water purification system or water from a newly opened HPLC grade distilled water bottle Use HPLC grade organic solvent whenever possible Solvents left in an opened bottle for a long time should not be used The content may have been changed absorbed moisture or has been co...

Страница 3: ...ll the way to the end fitting and secure it with the male nut It is important that there is no extra space between the tubing and the column side of the end fitting Presence of an extra space will let the sample to spread out and may result in wide peaks 3 Set the initial flow rate at less than 0 3 mL min and start the system If using the column at an elevated temperature keep a low flow rate unti...

Страница 4: ...umn Cleaning Problems in peak shapes and elution time changes or elevated column pressure etc are often caused by insoluble or adsorbing components present in the eluent and reagents being deposited inside the column These problems may be resolved by cleaning the column If a guard column is used with the analytical column first remove the guard column and check the performance of the analytical co...

Страница 5: ...and store the column at a location with stable temperature a cool and dark space is recommended Refer to section 7 3 Solvent Exchange for how to replace the eluent Attention Never allow inside of the column to dry It can damage the column 9 Column Inspection Inspection method is described in the Certificate of Analysis CoA Theoretical Plate Number N and Asymmetry Factor Fas were calculated using t...

Страница 6: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

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