Shodex GPC KD-800 Series Скачать руководство пользователя страница 1

ver.211124E

 

SHOWA DENKO K.K. (https://www.shodex.com/)

 

Operation Manual 

Shodex

 GPC KD-800 series 

 

(Please read this manual carefully to achieve the best and consistent column performance for a long time) 

 
 

Important Handling Instructions 

 

 Caution! 

 

 

· Please consult the Safety Data Sheet (SDS) of reagents and solvents used with the column 

and understand their proper handling methods to prevent potential health hazards or death 
from occurring. 

 

· Please wear appropriate personal protective equipment such as lab goggles and gloves 

when handling organic solvents and acid and alkaline reagents. Avoid any direct physical 
contact to prevent chemical injuries.   

 

Before Using the Column 

(1) Please visually inspect the package and outside of the column for any damage.   

 

(2) Please check if product name and serial number written on the column package, column name tag, and     

enclosed Certificate of Analysis (CoA) are matching and correct.   

 

1. Introduction 

Thank you for purchasing the Shodex

 product. Shodex

 GPC KD-800 series is a size exclusion 

chromatography column used with organic solvents. The column series is suitable for the separations of organic 
compounds and/or oligomers, and molecular weight distribution analysis of high molecular weight polymers. 
The columns with different exclusion limits are available. Please select columns with target molecular weight 
ranges (see below) that meet the molecular weight range of your samples.   
 

2. Column Components

       

 

         

 

 
 
 
 
 
 
 
 
 
 
 
 
 

3. Column Specifications 

 

Product 

Code 

Product Name 

Column Size 

(mm) 

Particle 

Size 

(

μ

m) 

Theoretical 

Plate Number 

(Per Column) 

Target Molecular 

Weight Range

*1

 

Exclusion 

Limit

*1

 

I.D. Length 

F6028210 

GPC KD-801 

8.0 300 

 17,000 

100 - 1,500 

    2,500 

F6028220 

GPC KD-802

 

8.0 300   

 17,000  

200 - 4,000 

    7,000 

F6028225 

GPC KD-802.5

 

8.0 300   

 17,000 

400 - 10,000 

      20,000 

F6028230 

GPC KD-803

 

8.0 300   

 17,000 

1,000 - 50,000 

      70,000 

F6028240 

GPC KD-804

 

8.0 300   

 17,000 

4,000 - 200,000 

    200,000 

F6028250 

GPC KD-805

 

8.0 300  10 

 11,000 

30,000 - (4,000,000)

*2

 

  (4,000,000)

*2

 

F6028260 

GPC KD-806

 

8.0 300  10 

 11,000 

30,000 - (40,000,000)

*2

  

(40,000,000)

*2

 

F6028290 

GPC KD-806M 

8.0 300  10 

 13,000 

1,000 - (40,000,000)

*2

  

(40,000,000)

*2

 

Содержание GPC KD-800 Series

Страница 1: ...the Shodex product Shodex GPC KD 800 series is a size exclusion chromatography column used with organic solvents The column series is suitable for the separations of organic compounds and or oligomers and molecular weight distribution analysis of high molecular weight polymers The columns with different exclusion limits are available Please select columns with target molecular weight ranges see be...

Страница 2: ...o 68 12 2 is included in the REACH Candidate List of substances of very high concern SVHC 4 Usable Conditions 4 1 System Settings 4 2 List of Applicable Solvents Product Name Flow Rate mL min Maximum Pressure MPa Per Column Temperature C Recommended Maximum Recommended Maximum GPC KD 801 to KD 807 0 5 1 0 1 5 3 5 50 60 GPC KD G 4A Solvents Product Name KD 801 to KD 802 5 KD 803 KD 804 to KD 807 Be...

Страница 3: ...tle for a long time should not be used The content may have been changed absorbed moisture or has been contaminated Always use freshly prepared solvents Solvents stored for a long time may have changed their compositions and may influence elution patterns and or damage the column Note Use of on line degasser is recommended 6 Sample Preparation 1 If possible use the eluent for analysis to dissolve ...

Страница 4: ...indicated on the column name tag If guard column is used position the guard column in front before the inlet of the analytical column 2 Make sure to insert the tubing all the way to the end fitting and secure it with the male nut It is important that there is no extra space between the tubing and the column side of the end fitting Presence of an extra space will let the sample to spread out and ma...

Страница 5: ...ents and then replace it with the new solvent e g When replacing DMF with LiBr to THF first run 100 DMF i e without LiBr and then introduce 100 THF by following step 3 above Attention Frequent solvent replacement deteriorates the column and thus not recommended 7 4 Column Cleaning Problems in peak shapes and elution timing changes or elevated column pressure etc are often caused by insoluble or ad...

Страница 6: ...late Number N 2 Asymmetry Factor Fas 10 Additional Warnings 1 Do not remove end fittings 2 Do not make a strong impact on the column Do not drop or hit the column on a hard surface Refer to the Shodex website https www shodex com for product details and their applications For additional assistance contact the distributor from whom you purchased the column or contact your regional Shodex support of...

Страница 7: ...anyone other than person or firm designated by Showa Denko K K 3 3 If the Shodex product is disposed of 3 4 If the Shodex product is resold by the user without giving prior written notice to Showa Denko K K 3 5 If the performance of the Shodex product is not conform to the specification of the attached CERTIFICATE OF ANALYSIS due to any of the reasons below a Computer virus b Impurities contained ...

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