ZEBV-5073B
Shimadzu High-Performance Liquid
Chromatograph Mass Spectrometer
LCMS-8050LCMS-8045
Pre-Installation Requirements
(Installation Preparations/Confirmation)
Страница 1: ...ZEBV 5073B Shimadzu High Performance Liquid Chromatograph Mass Spectrometer LCMS 8050 LCMS 8045 Pre Installation Requirements Installation Preparations Confirmation...
Страница 2: ...right 2018 Shimadzu Corporation 2 Information in this manual is subject to change without notice and does not represent a commitment on the part of the vendor 3 Any errors or omissions which may have...
Страница 3: ...otary Pump 7 2 7 2 Connecting to a PC 8 2 8 Required Power Supply 9 2 9 Gas 10 2 9 1 Nebulizer Gas Drying Gas and Heating Gas 11 2 9 1 1 Using a Nitrogen Gas Generator 11 2 9 1 2 Using Gas Generated f...
Страница 4: ...Contents LCMS 8045 8050 Pre Installation Requirements 2 This page is intentionally left blank...
Страница 5: ...8045 and LCMS 8050 Please make sure that the content of this document is carefully observed to ensure that the instrument functions stably providing data acquisition with a high degree of reliability...
Страница 6: ...1 Introduction LCMS 8045 8050 Pre Installation Requirements 4 This page is intentionally left blank...
Страница 7: ...tem Installation Example The working surface on which the instrument is installed should be firm stable and flat capable of withstanding the weight of the entire LCMS system including the LC hardware...
Страница 8: ...ample z When using a nitrogen gas generator prepare the space for it additionally For details please refer to the installation guide came with the generator z When using an Ar gas cylinder prepare the...
Страница 9: ...the LCMS main unit For details of Micro LC system refer to the installation manual of Micro LC unit We are assuming a micro LC system including LC Mikros and CTO Mikros Contact us for other LC system...
Страница 10: ...onnect to the PC using the USB cable Limit the length of the USB cable to 3 m USB cable is standard accessory of LCMS Standard LCMS 8045 8050 System Micro ESI 8060 LCMS 8045 8050 System Max length 3 m...
Страница 11: ...the same power source with other equipment z If the customer request UPS please contact us z Although the instrument is designed to operate properly within a voltage fluctuation range of 10 including...
Страница 12: ...tion can be prevented by using a dry air or a synthetic air as the nebulizer gas Gas Supply Pressure Gas Flow Rate 4 Type Purity Max Value Reference At normal use ESI APCI DUIS Micro ESI Nitrogen gas...
Страница 13: ...have the same source 2 9 1 1 Using a Nitrogen Gas Generator The following model of nitrogen dry air generator is available For details refer the Pre Installation Requirement of nitrogen generator Vari...
Страница 14: ...x Pressure regulator S221 35999 01 Model PPR N2 x Piping between gas cylinder and LCMS The following gas supply pipes are available from Shimadzu Please order them in advance Part Number Part Name S20...
Страница 15: ...able from Shimadzu Please order them in advance Part Number Part Name S221 35999 01 S201 48067 S201 48067 05 S221 26171 20 1 Pressure Regurator 2 Gas supply pipe Length 2 5 m 2 Gas supply pipe Length...
Страница 16: ...gas cylinders governing the installation site General Precautions When Using Gas Cylinders 1 Place gas cylinders outdoors in a well ventilated location out of direct sunlight Deliver the gas indoors...
Страница 17: ...5 meter evacuation hoses respectively for venting the rotary pump and the drain containers Connect each of the hoses from the rotary pump and the drain containers to separate evacuation facilities Le...
Страница 18: ...for DUIS x Acetophenone 100 ng ul 1 mL ampule 2 Samples for IQOQ evaluation S225 12238 04 For ESI APCI DUIS system repeatability linearity test x Papaverine 1 00 5 00 10 0 50 0 100 pg ul water 1 mL am...
Страница 19: ...me of standard installation may not satisfy the criteria under some conditions and performance history of the existing system i e when LCMS is installed to an existing HPLC or when APCI DUIS Micro ESI...
Страница 20: ......
Страница 21: ...rements 19 3 Preliminary Check List To Address The following page summarizes each of the installation conditions described so far as a check list The customer should fill in this sheet himself and han...
Страница 22: ...essure 690 to 800 kPa Heating gas Dry air Oil free Water free Gas pressure 690 to 800 kPa Hydrocarbon trap recommended CID gas Argon gas Purity 99 99 or more Pressure 500 to 800 kPa 4 Evacuation Evacu...
