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Shimadzu IRAffinity-1, Инструкция по эксплуатации

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5-4

IRAffinity-1

Chapter 5  Maintenance and Inspection

Fig. 5.2  Remove the Top Cover

Fig. 5.3  After Removing the Top Cover

5.1.1.3 Power Spectrum Check

FTIR performance is evaluated by measuring the power spectrum. The power spectrum gives the 
intensity at various wavenumbers. After ensuring that the sample chamber is empty, enter the 
following parameters in the Parameter Tab on the [Measurement] Tab Screen, and measure the 
power spectrum to verify the specifications.

In [Data] tab:

"Measuring mode":

"Power"

"Resolution":

"2 cm

−

1

"

"Range":

"4700-340 cm

−

1

"

"N scans":

"45" scans

"Apodization":

"HAPP-GENZEL"

"Detector":

"standard"

"Beam":

"internal"

In [More] tab:

"Detector speed":

"2.8 mm/sec"

Lift up to remove the Top cover.

Silica gel case
Confirm the color of the 
Silica gel inside

Содержание IRAffinity-1

Страница 1: ...INSTRUCTION MANUAL USER SYSTEM GUIDE IRAffinity 1 SHIMADZU FOURIER TRANSFORM INFRARED SPECTROPHOTOMETER Read the instruction manual thoroughly before you use the product Keep this instruction manual f...

Страница 2: ...This page is intentionally left blank...

Страница 3: ...thout written permission from Shimadzu Corporation Since Shimadzu products are frequently upgraded and improved information in this publication is subject to change without notice Any errors or omissi...

Страница 4: ...are itself for a detailed description of each command For information about your PC and printer refer to their individual product manuals This instruction manual consists of Safety Precautions Describ...

Страница 5: ...product is not an explosion proof product It ignites and causes a fire Since this instrument includes electrically active parts even if the power switch is off it ignites and causes a fire if there ar...

Страница 6: ...compounds WARNING To ensure safe operation contact your Shimadzu representative if product installation adjustment or re installation after the product is moved is required Take measures to prevent th...

Страница 7: ...gloves and protective goggles when handling solvents and samples If solvent gets into the eyes blindness could result Should solvent get into the eyes flush immediately with large amounts of water an...

Страница 8: ...he waste liquid container is virtually non conductive 10 10 S m or less it will be necessary to add properly conductive and therefore safe liquid to the tank This conductive liquid may be added before...

Страница 9: ...will prevent static Keep the room at a proper level of humidity WARNING Maximum 10 L min of the purge gas is used to purge the FTIR Take measures to prevent hypoxia in accordance with the local laws...

Страница 10: ...m the power outlet and wipe away the dust with a dry cloth If dust is allowed to accumulate fire could result Replacement parts must be of the specifications given in this manual Use of any other part...

Страница 11: ...ed obtain replacements from Shimadzu Corporation WARNING RISK OF ELECTRIC SHOCK DO NOT remove cover Contact your Shimadzu representative for service WARNING RISK OF ELECTRIC SHOCK Read instructions be...

Страница 12: ...NOTE When orange lamp is lighting interferometer is kept in low humid If this orange lamp is not lighting refer to Instruction manual User s System Guide Troubleshooting immediately Notice label Part...

Страница 13: ...eon laser with an output of 0 5 mW maximum in it When the IRAffinity 1 is on the laser is emitted continuously It has two purposes in the system sampling signal generation and optical axis adjustment...

Страница 14: ...xii IRAffinity 1 Symbol Definition Current AC Symbols Found on the IRAffinity 1...

Страница 15: ...or example the service life of an LCD display panel depends on the actual operating conditions 8 combination uses with hardware or software other than our specification 9 damages of instrument data an...

Страница 16: ...ware upgrades for the SOFTWARE that SMZ will release as deemed necessary by SMZ An upgrade means certain supplemental program modules and or information for bug fixing and or updates to the defects an...

Страница 17: ...oying all copies of SOFTWARE including any documentation This License will terminate immediately without notice from SMZ if you fail to comply with any provision of this License Upon termination you m...

Страница 18: ...e Fourier Transform Infrared Spectrophotometer Model Name IRAffinity 1 Manufacturer SHIMADZU CORPORATION ANALYTICAL MEASURING INSTRUMENTS DIVISION Address 1 NISHINOKYO KUWABARA CHO NAKAGYO KU KYOTO 60...

Страница 19: ...strial professional use only Contact Shimadzu service representative when the equipment has reached the end of its life They will advise you regarding the equipment take back With your co operation we...

Страница 20: ...10 1 5 3 Optical System 1 11 1 5 4 Light Source 1 12 1 5 5 Beam Splitter 1 13 1 5 6 Detector 1 13 1 5 7 Dry Unit 1 13 1 6 Electrical System 1 15 1 7 S N Ratio 1 16 Chapter 2 Specifications 2 1 IRAffin...

Страница 21: ...hapter 5 Maintenance and Inspection 5 1 Start Up Inspection and Periodic Inspection 5 2 5 1 1 Start Up Inspection 5 2 5 1 1 1 Dry Indicator Check 5 2 5 1 1 2 Silica Gel Check 5 3 5 1 1 3 Power Spectru...

Страница 22: ...aterials for Infrared Analysis 7 1 Materials for Infrared Analysis 7 2 7 2 Characteristics of Materials 7 3 7 3 Optical Materials in IRAffinity 1 7 5 7 4 Material Safety Data Sheet 7 6 7 4 1 KRS 5 7 6...

Страница 23: ...d Functions of the IRAffinity 1 CONTENTS 1 1 Principle and Construction 1 2 1 2 Resolution and Apodization 1 5 1 3 The FTIR Advantage 1 7 1 4 System Configuration of IRAffinity 1 1 8 1 5 Interferomete...

Страница 24: ...eposited on a potassium bromide substrate via evaporation comprises the beam splitter it splits the single beam into two reflecting one to the fixed mirror and transmitting the other to the moving mir...

Страница 25: ...nterference Equation 1 1 extrapolated from the above principles calculates the intensity I of light wavelength incident to the detector where R energy reflected by the beam splitter T energy transmitt...

Страница 26: ...ine transform of spectrum B Thus an inverse Fourier cosine transform of I recovers the original spectrum B While the conventional dispersive spectrometer directly determines the intensity of B at cert...

Страница 27: ...1 8 first becomes zero at 1 2L where the half width value is 0 605 L The greater the optical path difference L the smaller the half value width when the moving mirror is driven further the resolution...

Страница 28: ...rameter for samples requiring high resolution such as gas and the Happ Happ Genzel Function or Sqr Triaug Sqr Triaug Function parameter which has fewer submaxima peaks when high resolution is unnecess...

Страница 29: ...ated by the large FTIR aperture FTIR results depend on the aperture area and the incident angle of light When a large aperture is used more of the light source is available to maintain a high throughp...

Страница 30: ...te data processing Two types of personal computers the desktop type and the notebook type are available However when using the infrared microscope which handles image data the notebook type is not ava...

Страница 31: ...3 Dry indicator orange Lights up while humidity in the interferometer is low Contact Shimadzu representative if it does not light even though the power cord is connected correctly 4 Sample compartment...

Страница 32: ...interferometer or the sample compartment with dry air etc 1 5 2 Inside of Sample Compartment Fig 1 7 Inside View of Sample Compartment 1 Cassette When using a liquid cell or 5 cm gas cell slide it in...

Страница 33: ...t through this terminal so that the option type can be recognized Take care not to touch this terminal or spill liquid on it 4 Auto sample changer connector To use an option with the auto sample chang...

Страница 34: ...o the Help document included in the software The image size in the sample compartment in each resolution is as follows when the standard light source is used When 1 thin films are measured by transmit...

Страница 35: ...the IRAffinity 1 be connected to the AC power supply to keep power supply Confirm that the orange LED dry indicator in the lower right portion of the front face is lit If it is expected that the main...

Страница 36: ...hen discharged Fig 1 9 Principle of ROSAHL The dry unit is located the inside of the cover on the back side of IRAffinity 1 The following attentions should be paid when use Please avoid using this pro...

Страница 37: ...digitized by the 20 bit A D converter After the signal is digitized into the interferometer memory it travels through the USB 2 0 interface to the PC where IRsolution transforms the interferogram int...

Страница 38: ...s used 2250 2050 cm 1 The S N ratio is therefore measured and calculated by the following method with IRAffinity 1 series 1 BKG scan and Sample scan is sequentially measured at 4 cm 1 resolution and 2...

Страница 39: ...2 1 IRAffinity 1 Chapter 2 Specifications CONTENTS 2 1 IRAffinity 1 Specifications 2 2...

Страница 40: ...egrated for 1 minute Mirror speed 4 step 2 0 2 8 5 9 mm sec One time integration at 4 cm 1 resolution and 2 8 mm sec mirror speed take about 2 to 3 sec Data sampling He Ne laser used guaranteed for 30...

Страница 41: ...alysis program PharmaReport program Quantitative analysis Peak height Peak area Multi point calibration curve method using ratio Multi linear regression MLR method Spectrum search Spectral search peak...

Страница 42: ...her Power for the computer is required separately Installation site Temperature 15 to 30 C Must be controlled with an Air conditioner Humidity 70 or less No dewing condensation Utility AC 100 120 220...

Страница 43: ...ting Standard Accessories 3 2 3 2 Installation Environment for Equipment 3 3 3 3 Wiring the Cables 3 5 3 4 Installing the Software 3 6 3 5 User Management 3 14 3 6 Uninstallation of the IRsolution 3 1...

Страница 44: ...erferometer then unpack the interferometer especially in winter NOTE 1 The personal computer and the printer are not included in standard accessories Separately prepare them We can offer the preinstal...

Страница 45: ...a flat table that can withstand this weight 7 For the IRAffinity 1 the internal dry unit is operating even while the power switch on the front is OFF Accordingly when the power should be completely t...

Страница 46: ...afety reasons Shimadzu recommends the use of the oxygen indicator along with the product introduced in this manual The following is the recommended portable oxygen indicator XO 2000 Oxygen Indicator N...

Страница 47: ...PPLY Fluctuation of supply voltage and capacity of power supply for IRAffinity 1 is 100 120 220 230 240 V 10 150 VA 50 60 Hz Confirm the capacity of power supply including the power for personal compu...

Страница 48: ...he Instruction Manual User s System Guide 2 Turn them ON and then Windows will automatically recognize the IRAffinity 1 with Plug Play function In this case Windows should be run as Administrator 3 Wi...

Страница 49: ...her software is running close it Insert the CD ROM into the CD ROM drive The setup program automatically starts up Execute setup exe if setup program does not run automatically 4 Preparing Setup dialo...

Страница 50: ...prey 100 If the microscope is not used or another kind of video capture device is used select the radio button Normal video capture device Click Next button after this selection 7 Installation starts...

Страница 51: ...the destination folder to be installed The default folder is usually used Click the Browse button to change the destination Fig 3 6 Chose Destination Location Dialog Box 11 Click the Next button to pr...

Страница 52: ...gram The IRsolution main body Help Help message file of the IRsolution GLP mode Installs the IRsolution on the GLP mode to support the GLP GMP Electric Signature function is available on the GLP mode...

Страница 53: ...rrectly 16 Click the Finish button to install the Alternation Check Program and Sample Files 17 When all selected components are installed the Install Shield Wizard Complete dialog box opens Click Fin...

Страница 54: ...m the installation program of IRsolution creates a data folder C Program Files Shimadzu IRsolution data where C represents the drive Windows was installed to which security settings are modified so th...

Страница 55: ...IRsolution menu on the Start menu 2 Set up the model of instrument to connect with the IRsolution Select the Environment Instrument Preferences Instruments menu before initializing the FTIR Select IR...

Страница 56: ...og Box Click the OK button to open the message There is no active user xxxxxx The application has to be closed Do you want to continue and close the application Click the Yes button to close IRsolutio...

Страница 57: ...ompts on the screen 5 Next select IRsolution x xx then click the Modify Remove button Select Automatic on the window then follow the prompts on the screen Fig 3 15 Select Uninstall Method 6 Finally se...

Страница 58: ...al Operation Guide Execute Auto Adjust from the IRsolution window measure the power spectrum then confirm that the intensity of the power spectrum satisfies the standard value shown in Chapter 5 WARNI...

Страница 59: ...ducted Susceptibility IEC61000 4 6 1996 3 Vrms 0 15 MHz 80 MHz e Power Frequency Magnetic Field Measurement IEC61000 4 8 1993 Field Strength 30 A m f Voltage dips short interruptions and Voltage varia...

Страница 60: ...Chapter 3 Installation 3 18 This page is intentionally left blank IRAffinity 1...

Страница 61: ...tware refer to Instruction manual Operation guide for detail operation CONTENTS 4 1 Activation and Shutdown of IRAffinity 1 and PC 4 2 4 2 Initialization of IRAffinity 1 and Self Diagnostics 4 3 4 3 S...

Страница 62: ...the PC and turn off the PC 5 Turn off the power switch at the front right side of the IRAffinity 1 The power indicator green should turn off 6 Keep a power supply cable connected to IRAffinity 1 to r...

Страница 63: ...the log window 4 Failed item is indicated as Failure on the log window 5 After all items are inspected a message INIT SUCCESS is recorded on the log window the condition of IRAffinity 1 is displayed o...

Страница 64: ...es higher and exceeds the capacity of the A D converter Set auto or smaller aperture On the other hand when samples are measured with Open aperture using an ATR or Diffuse reflectance accessory the qu...

Страница 65: ...ning The raw spectrum and corrected spectrum are stored in a file Atmosphere correction parameters are set on Environment Instruments Preferences Atmosphere Correction Fig 4 3 Atmosphere Correction Pa...

Страница 66: ...automatically After that a macro program can also be executed automatically macro program is option The scan parameter for the Automatic recognition function is configured with the following steps 1...

Страница 67: ...er this setting when an accessory with an Automatic Recognition Function is installed the following dialog box is displayed Fig 4 6 QuickStart Accessories Recognized 7 Clicking OK button sets the spec...

Страница 68: ...surement Initialize 7 Select Measurement Auto Sampler The Sampler dialog box is displayed Fig 4 7 Sampler 8 Select either ASC A 9 Select your accessory on the Accessory section Selecting following acc...

Страница 69: ...ckground sample 4 Put a check mark on the BKG when the first sample position is a background sample 5 Input the file name for data 6 When you want to save the obtained spectra in a file put a check ma...

Страница 70: ...ion is the last sample position of the ASC the Next button moves to the first position initialized position When the current position is the first sample position initialized position of the ASC the P...

Страница 71: ...cher Otherwise samples might be dropped by the vibration during moving the position 4 7 4 Accessories Which Are Mounted to the Cassette Sample Holder When mounting accessories such as liquid cells in...

Страница 72: ...Chapter 4 Operations Unplug the power cord of IRAffinity 1 instead of turning off the power switch on the front panel if IRAffinity 1 must be completely turned off in case of rising smoke etc 4 8 In...

Страница 73: ...Inspection 5 2 5 2 When Not Using IRAffinity 1 for a Long Term Over a Month 5 7 5 3 For Brownout 5 8 5 4 Procedure to Replace Silica Gel 5 9 5 5 Dry Indicator 5 10 5 6 Self Diagnostics 5 11 5 7 Cleani...

Страница 74: ...ower cord immediately and do not use your IRAffinity 1 2 Remove the Top cover and replace the silica gel packages 3 Please contact your SHIMADZU representative Start up inspection Is an inspection bef...

Страница 75: ...n the interferometer becomes high and the optical elements will be damaged In this case 1 Disconnect the power cord immediately and do not use your IRAffinity 1 2 Remove the Top cover and replace the...

Страница 76: ...bers After ensuring that the sample chamber is empty enter the following parameters in the Parameter Tab on the Measurement Tab Screen and measure the power spectrum to verify the specifications In Da...

Страница 77: ...Auto adjustment on the Instrument Menu and reanalyze the spectrum If the power spectrum does not improve after the auto adjustment the system may be damaged contact your SHIMADZU representative If the...

Страница 78: ...umber accuracy wavenumber reproducibility and transmittance absorbance reproducibility The performance of the FTIR 8400S is validated through comparison between the measurement result and the standard...

Страница 79: ...d for long term AC power must still be supplied The Dry unit works desiccating the inside of the interferometer and protecting the optical elements against humidity Inspection according to the section...

Страница 80: ...Maintenance and Inspection When AC power cannot be supplied because of periodic inspection of utilities etc the Dry unit does not desiccate Replace Silica gel packages in the FTIR once a week during...

Страница 81: ...5 6 to fix the lid of the Silica gel case and then take off the lid of the Silica gel case 2 in Fig 5 6 3 Take all Silica gel out and then put new 4 Silica gel packages in 4 Put the Silica gel case wi...

Страница 82: ...power plug of the IRAffinity 1 be connected to the AC power supply to keep the power supply Confirm that the orange Dry indicator is lit If the Dry indicator is not lit please confirm following check...

Страница 83: ...lighting 3 Humidity level inside the interferometer 4 Status of the beam switching kit 5 Presence of Auto sampler 6 Presence of QuickStart accessory and its information 5 6 1 Self Diagnostics during I...

Страница 84: ...les and accessories from the sample compartment If this test was failed by interrupting the beam you can execute Self diagnostics after initialization If this test was failed with empty sample compart...

Страница 85: ...can parameters first Then execute Measurement Auto Adjust If the test is still failed after auto adjustment the Beam splitter might be damaged Please contact your SHIMADZU representative Laser Laser l...

Страница 86: ...en The humidity in the interferometer is low enough Red The humidity in the interferometer is high The dry unit might break down 1 Disconnect the power cord immediately and do not use your IRAffinity...

Страница 87: ...er is not installed Yellow Auto sampler is not initialized Green Auto sampler was initialized and is ready to be used Accessory Indicates presence and information of the installed accessory None Acces...

Страница 88: ...a soft cloth or tissue soak the cloth in water or detergent and wring it out Do not use organic solvents such as thinner or benzene and avoid contact with mirrors and other internal components NOTE Do...

Страница 89: ...e System 5 17 IRAffinity 1 WARNING To ensure safe operation contact your SHIMADZU representative for installation adjustment or re installation after moving the instrument to a different site 5 8 Tran...

Страница 90: ...10 Laser Assy 1 206 73369 91 11 Laser Power Supply Assy 1 206 72343 91 12 Piezo Assy 1 206 17317 13 Moving Mirror Assy 1 206 17331 05 14 Fixed Mirror Assy 1 206 70012 91 15 ASC cable 1 206 73433 91 16...

Страница 91: ...IRAffinity 1 Chapter 6 Troubleshooting CONTENTS 6 1 Error Message Table 6 2 6 2 Error Message Shown in the Status Window 6 3 6 3 What s Happening 6 6 6 4 Confirming the Power Selector Switch and Fuse...

Страница 92: ...ches the sample measurement T or Abs When you change parameters such as Resolution background data must be measured then sample measurement becomes available Can t open the File File to be loaded migh...

Страница 93: ...is set to Option2 liquid nitrogen sensor is active and if there is no liquid N2 in the MCT dewer this error message is shown Confirm that MCT dewer is filled with liquid N2 and that cable is connecte...

Страница 94: ...asurement Auto Adjust Optim vertical value beyond the limit after Auto Adjust The parameters of fixed mirror adjustment beyond the software limit Execute Measurement Auto Adjust Optim horizontal value...

Страница 95: ...zation communication between interferometer and PC is not active Check if interferometer power is not ON or USB cable is disconnected Instrument Timeout Error Communication between interferometer and...

Страница 96: ...ative 6 3 2 The Signal Intensity of the Power Spectrum Remains Zero Phenomena 1 The Signal intensity of the power spectrum remains zero Reason 1 The light source is disconnected 2 The fuse blew 3 Sele...

Страница 97: ...r has several mirrors inside Never wipe the mirror surface with cloth or cleaner even if these mirrors are contaminated with dust It may damage the mirror surface and lower the intensity of the infrar...

Страница 98: ...ard 3 Trouble with the detector Solution 1 Deterioration because of long term use Execute the Measurement Auto Adjust When power spectrum does not fluctuate in short term execute a Japanese or Europea...

Страница 99: ...voltage or replacing the fuse CAUTION Rating and type of fuse Be sure to replace the fuse specified as below Part No 072 02004 22 250 V 4 0 AT Fig 6 1 a 1 Be sure to disconnect AC cable Insert the Fi...

Страница 100: ...6 10 IRAffinity 1 Chapter 6 Troubleshooting Fig 6 1 e 5 Close the lid of the AC inlet Place the interferometer so that the front face is placed toward you after the works above are completed...

Страница 101: ...ity 1 Chapter 7 Materials for Infrared Analysis CONTENTS 7 1 Materials for Infrared Analysis 7 2 7 2 Characteristics of Materials 7 3 7 3 Optical Materials in IRAffinity 1 7 5 7 4 Material Safety Data...

Страница 102: ...er solubility at 20 C g 100 gH2O transmission thickness Max Temp Melting point Knoop hardness KBr 40000 340 0 25 29 4 1 52 65 90 5 mm 300 730 7 0 100 g NaCl 50000 600 0 2 16 6 1 49 36 90 5 mm 400 801...

Страница 103: ...humidity conditions lower than 50 chloroform carbon tetrachloride aqueous solution lower alcohol KCl Potassium chloride Similar characteristics as NaCl and KBr Not popularly used chloroform carbon tet...

Страница 104: ...dely used as the material for semiconductors Rarely used as window material Ge can substitute Si as window material acetone water HF HNO3 Ge Germanium Widely used as the material for semiconductors Ea...

Страница 105: ...IRAffinity 1 Fig 7 1 shows optical materials in the IRAffinity 1 Fig 7 1 Optical Materials in IRAffinity 1 7 3 Optical Materials in IRAffinity 1 Beam splitter Ge on KBr window Window KRS 5 window Comp...

Страница 106: ...ing apparatus only after soiled clothing has been completely removed In case of irregular breathing or respiratory arrest provide artificial respiration After inhalation Supply fresh air If required p...

Страница 107: ...Handling Information for safe handling Keep containers tightly sealed Store in cool dry place in tightly closed containers Ensure good ventilation exhaustion at the workplace Open and handle containe...

Страница 108: ...France VME 0 1 Germany MAK 0 1 Ireland TWA 0 1 skin Korea TLV 0 1 skin Netherlands MAC TGG 0 1 skin Norway TWA 0 1 Poland TWA 0 1 0 3 STEL Switzerland MAK W 0 1 skin United Kingdom LTEL 0 1 skin USA P...

Страница 109: ...Water Insoluble 10 Stability and reactivity Thermal decomposition conditions to be avoided No decomposition if used and stored according to specifications Materials to be avoided Oxidizing agents Alka...

Страница 110: ...state local or national regulations for proper disposal Hand over to disposers of hazardous waste Must be specially treated under adherence to official regulations Uncleaned packagings Recommendation...

Страница 111: ...possible 61 Avoid release to the environment Refer to special instructions safety data sheets National regulations Information about limitation of use Employment restrictions concerning young persons...

Страница 112: ...soiled clothing has been completely removed In case of irregular breathing or respiratory arrest provide artificial respiration After inhalation Supply fresh air If required provide artificial respir...

Страница 113: ...See item 13 for information on disposal 7 Handling and storage Handling Information for safe handling Keep containers tightly sealed Store in cool dry place in tightly closed containers Ensure good v...

Страница 114: ...France VME 0 1 Germany MAK 0 1 Ireland TWA 0 1 skin Korea TLV 0 1 skin Netherlands MAC TGG 0 1 skin Norway TWA 0 1 Poland TWA 0 1 0 3 STEL Switzerland MAK W 0 1 skin United Kingdom LTEL 0 1 skin USA...

Страница 115: ...Dangerous products of decomposition Toxic metal oxide smoke Hydrogen iodide HI 11 Toxicological information Acute toxicity Primary irritant effect on the skin Irritant for skin and mucous membranes o...

Страница 116: ...gulations 14 Transport information Land transport ADR RID and GGVS GGVE cross border domestic ADR RID GGVS E Class 6 1 T5 Toxic substances Kemler Number 60 UN Number 1707 Packaging group II Label 6 1...

Страница 117: ...possible 61 Avoid release to the environment Refer to special instructions safety data sheets National regulations Information about limitation of use Employment restrictions concerning young persons...

Страница 118: ...ate medical advice After eye contact Rinse opened eye for several minutes under running water Then consult doctor After swallowing Seek medical treatment 5 Fire fighting measures Suitable extinguishin...

Страница 119: ...ure controls and personal protection Additional information about design of technical systems Properly operating chemical fume hood designed for hazardous chemicals and having an average face velocity...

Страница 120: ...ording to specifications Materials to be avoided Water moisture Dangerous reactions No dangerous reactions known Dangerous products of decomposition Hydrogen bromide Metal oxide 11 Toxicological infor...

Страница 121: ...ifications 15 Regulatory information Designation according to EC guidelines Observe the normal safety regulations when handling chemicals The product is not subject to identification regulations under...

Страница 122: ...ce After eye contact Rinse opened eye for several minutes under running water Then consult doctor After swallowing Seek medical treatment 5 Fire fighting measures Suitable extinguishing agents Use fir...

Страница 123: ...itions Protect from humidity and keep away from water Keep container tightly sealed Store in cool dry conditions in well sealed containers 8 Exposure controls and personal protection Additional inform...

Страница 124: ...0 1 Germany TWA 0 15 respirable fraction of the aerosol Ireland TWA 0 4 respirable USA PEL See quartz Silica amorphous diatomaceous earth mg m3 ACGIH TLV 10 inhalable particulate 3 respirable particul...

Страница 125: ...tective work clothing 9 Physical and chemical properties General Information Form Powder Colour White Smell Odourless Change in condition Melting point Melting range 1610 1728 C Boiling point Boiling...

Страница 126: ...inogenic to humans sufficient evidence of carcinogenicity NTP 2 Reasonably anticipated to be a carcinogen limited evidence from studies in humans or sufficient evidence from studies in experimental an...

Страница 127: ...s concerning young persons must be observed For use only by technically qualified individuals Water hazard class Generally not hazardous for water 16 Other information Employers should use this inform...

Страница 128: ...Chapter 7 Materials for Infrared Analysis 7 28 This page is intentionally left blank IRAffinity 1...

Страница 129: ...Class 1 xi collimator mirror 1 2 Compensator 7 5 Continuous Scan 4 5 D detector 1 12 2 2 5 18 7 5 DLATGS detector 1 13 DRS 8010ASC 4 8 dry indicator 1 9 1 13 5 2 5 10 dry unit 1 13 5 18 DuraSamplIR I...

Страница 130: ...ic inspection 5 2 5 6 phase 1 3 Polystyrene 5 18 power indicator 1 9 5 10 Power spectrum 5 2 5 4 power switch 1 9 4 2 4 12 purge 1 10 3 4 Q QuickStart 4 6 R resolution 1 12 2 2 4 4 S S N ratio 1 7 1 1...

Страница 131: ...3 IRAffinity 1 Z ZnSe 7 2 7 4...

Страница 132: ...4 This page is intentionally left blank IRAffinity 1...

Страница 133: ...1 Record of Revision Note A Added Page No D Deleted Page No Date Revision Changed Page Description 2009 01 B Windows Vista Business was added on Specification P N of IRsolution and Supplemental Disk w...

Страница 134: ...This page is intentionally left blank IRPrestige 21...

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