320
Troubleshooting
If the above checks fail to make an improvement, turn off the plasma, then check
the following:
•
Check that the nebulizer end cap is connected tightly.
•
Check the nebulizer spray pattern: run deionized water for several minutes,
then remove the nebulizer end cap. If the nebulizer spray is sputtering or
uneven, inspect the nebulizer tips for clogging and clean or replace them as
necessary.
Note: For a clogged Meinhard K1 nebulizer, try soaking in low acid solution for several
hours or over night. Alternatively, direct a flow of gas (air, nitrogen or argon)
through the nebulizer tip (this can sometimes dislodge a clog in the Ar capillary).
•
Check that the injector is not clogged. You will need to remove the Quick-
Change Torch Module and disassemble the torch as described in
Change Adjustable Torch Module on page 205
.
Performance Problems
Checking the Sample Introduction System
Many performance problems (such as poor precision or loss of signal) can be traced
to the setup and condition of the sample introduction system.
The following list describes general checks for the sample introduction system,
which should be done on a regular basis. Typical symptoms of problems are listed
to help you determine whether maintenance is required.
If you have already done performance checks, refer to the Syngistix Software
Guide on the Syngistix Document Pack CD for details
.
If the plasma has been on, allow one minute for the Quick-Change Torch
Module to cool and an additional two minutes for the torch to cool before
checking the following.
Avertissement:
Si le plasma a été allumée, laissez une minute pour le
changement rapide Module Torch refroidir et deux minutes
supplémentaires pour la torche pour refroidir avant de vérifier le suivant
.
!
Warning
Содержание AVIO 500
Страница 1: ...AVIO 500 Customer Hardware and Service Guide ICP OPTICAL EMISSION ...
Страница 2: ......
Страница 3: ...Avio 500 Customer Hardware and Service Guide ...
Страница 12: ...Contents 10 ...
Страница 30: ...28 ...
Страница 31: ...C h a p t e r 1 ...
Страница 32: ......
Страница 33: ...Safety Practices 1 ...
Страница 58: ...56 Safety Practices ...
Страница 59: ...C h a p t e r 2 ...
Страница 60: ......
Страница 76: ...74 Preparing Your Laboratory ...
Страница 77: ...C h a p t e r 3 ...
Страница 78: ......
Страница 79: ...System Description 3 ...
Страница 94: ...92 System Description Figure 3 7 GemCone nebulizer and end cap N0680504 also shown in cross sectional view ...
Страница 115: ...C h a p t e r 4 ...
Страница 116: ......
Страница 137: ...135 Installing the Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 152: ...150 Installation Figure 4 22 Scott Spray Chamber Clip Assembly in Place ...
Страница 195: ...193 Shipping Lists 09290798 USB Cable Table 4 6 Spares Available Continued ...
Страница 196: ...194 Installation ...
Страница 197: ...C h a p t e r 5 ...
Страница 198: ......
Страница 209: ...207 Quick Change Adjustable Torch Module Figure 5 1 Quartz Torch Item Description 1 Plasma Induction Plates 2 Torch 2 1 ...
Страница 217: ...215 Quick Change Adjustable Torch Module 1 2 10 8 9 3 4 7 6 5 ...
Страница 316: ...314 Maintenance ...
Страница 317: ...C h a p t e r 6 ...
Страница 318: ......
Страница 339: ...337 RF Generator Sample Introduction System Troubleshooting Form Figure 6 2 Normal plasma at 3mm position ...
Страница 340: ...338 Troubleshooting Figure 6 3 Rounded Plasma due to sample or air getting around the outside typically subtle air leak ...
Страница 342: ...340 Troubleshooting Figure 6 5 Injector too far forward ...
Страница 343: ...341 RF Generator Sample Introduction System Troubleshooting Form Figure 6 6 No Aux Gas torch may be glowing ...
Страница 344: ...342 Troubleshooting Figure 6 7 Air leak or spray chamber temperature too high ...
Страница 345: ...343 RF Generator Sample Introduction System Troubleshooting Form Figure 6 8 Thin plasma due to leak in plasma gas line ...
Страница 346: ...344 Troubleshooting ...
Страница 354: ......