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Parr Instrument Company

No. 394M

Operating Instruction Manual for 

4540

Pressure Reactors

 

Содержание 4540

Страница 1: ...Parr Instrument Company No 394M Operating Instruction Manual for 4540 Pressure Reactors...

Страница 2: ...odic Pressure Tests 15 General Maintenance Notes 16 Parts Lists 17 Reaction Vessel Parts List 17 Overarm Parts List 19 Cooling Coil Parts List 21 Vessel Heater Parts List 22 Diagrams 23 Related Instru...

Страница 3: ...ngs are found in the Operating Instructions for the controller supplied with your reactor Before connecting a controller to an electrical outlet the user must be certain that the electrical outlet has...

Страница 4: ...be bonded to Protective Earth at the source of supply in accordance with national and local electrical code requirements Earth Ground Functional earth connection NOTE This connection shall be bonded...

Страница 5: ...re readily apparent but the penalties that must be paid for over designed apparatus are often overlooked Recognizing these criteria Parr reactors and pressure vessels are offered in several different...

Страница 6: ...lterations or by substituting components which are not recommended by the Parr Instrument Company It must also be understood that lower pressure and temperature limits may be required for modified rea...

Страница 7: ...the top of the beltguard This knob is attached to the upper drive shaft and the universal coupling Lifting the knob will allow the alignment of the universal coupling and the drive adapter attached t...

Страница 8: ...de of the bomb head Gas released from this valve will be drawn from the top of the reactor Liquid Sampling Valve The liquid sampling valve is attached to the same fitting as the gas inlet valve and co...

Страница 9: ...ler using the A470E2 extension wire furnished with the controller Pressure Gage A pressure gage usually 0 7500 psi with a T316 stainless steel Bourdon tube is mounted on the head using attachment fitt...

Страница 10: ...nd head For vessels on a stationary stand loosen the panel screw holding the vessel retainer remove the vessel from the stand and set it on a table To Open the Vessel Remove the split rings For vessel...

Страница 11: ...and into the gas tank when the inlet valve is opened If there is any possibility that the tank pressure might not be high enough to force gas into the reactor install a one way check valve optional in...

Страница 12: ...ller ACCESSORIES Internal Cooling Loop A cooling loop can be installed in any of these reactors The reactors are not drilled for a cooling loop unless so ordered Reactors purchased without a loop can...

Страница 13: ...exhaust If the muffler felts are dirty wash them in solvent or replace them Relubricate the motor with a squirt of oil into the chamber and reassemble If it becomes necessary to disassemble the motor...

Страница 14: ...zard associated with these units can be resolved by installing the controller in a remote location outside of the hazardous area or by enclosing it in an approved explosion proof housing If enclosed w...

Страница 15: ...ure vessels must be tested at regular intervals Records are kept of deflections at specific test pressures so that any increase in deflection becomes a warning that the metal has lost strength Any cyl...

Страница 16: ...ion ring be sure that it is in place on the head before attaching any head fittings The compression ring cannot be installed after fittings have been screwed into the head 8 Clean all threads and gas...

Страница 17: ...shaft coupling 447HC Shaft bushing PTFE 448HC16 Shaft with bushing 600 mL 448HC17 Shaft with bushing 1200 mL A2308HC Impeller with set screws 358HC2F Set screws for impeller For parts made from altern...

Страница 18: ...13HC Drop Band RV A2315HC Split Ring Assembly w bolts rings latches FH 1278HC4F Bolts split ring 5 8 18 1 2 Hex 1368HC Torque Wrench 3 8 drive 1369HC2 Torque Adapter 3 8 drive x 1 2 hex Gages 56HCPF P...

Страница 19: ...732HC Snap Ring External 1 HD 2429HC Bushing PTFE HD Upper Drive Shafts A860HC Upper Drive Shaft RV A742HC13 Upper Drive Shaft standard Calrod heater only RV A2562HC Upper Drive Shaft FH A2564HC Upper...

Страница 20: ...20 4540 Pressure Reactors Parr Instrument Company Overarm Plate Drive Pulley Motor Belt Tach Sensor Assembly Upper Drive Shaft Release Knob Driven Pulley Optical Wheel Hub Coupling Collar...

Страница 21: ...op 600 mL RV 2306HC2 Cooling Loop 1200 mL RV 2306HC3 Cooling Loop 600 mL FH 2306HC4 Cooling Loop 1200 mL FH Cooling Loop Fittings 511HC Elbow Tube Connector T 122HW Ferrule for 511HC 123HW Cap Nut for...

Страница 22: ...1500W 230V for use with 600 mL w o BDV or 1200 mL w or w o BDV For Bench Top and Floor Stand Vessels A2256HC10EB Heater Assembly 1000W 115V 600 mL A2256HC10EE Heater Assembly 1000W 230V 600 mL A2256HC...

Страница 23: ...23 4540 Pressure Reactors Parr Instrument Company DIAGRAMS Diagram of Overarm for 4544A 4545A 4546A 4547A...

Страница 24: ...24 4540 Pressure Reactors Parr Instrument Company Diagram of Overarm for 4544A 4545A 4546A 4547A...

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Страница 35: ...Revision 02 21 08 PARR INSTRUMENT COMPANY 211 Fifty Third Street Moline Illinois 61265 USA 309 762 7716 800 872 7720 Fax 309 762 9453 http www parrinst com E Mail parr parrinst com...

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