CH-9101 Herisau/Switzerland
E-Mail
[email protected]
Internet www.metrohm.com
Titrando
Installation Instructions
8.840.1133 06.2006
/
jb
Страница 1: ...CH 9101 Herisau Switzerland E Mail info metrohm com Internet www metrohm com Titrando Installation Instructions 8 840 1133 06 2006 jb...
Страница 2: ...m These instructions are protected by copyright All rights reserved Although all the information given in these Instructions has been checked with great care errors cannot be entirely excluded Should...
Страница 3: ...Connecting an external dosing device 18 2 4 4 Connecting a remote box 20 2 5 Device connection at the USB 21 2 5 1 Connecting a printer 21 2 5 2 Connecting a balance 22 2 5 3 Connecting a USB Sample P...
Страница 4: ...titration stands 47 4 3 3 Titration equipment 47 4 3 4 Karl Fischer titration equipment 6 5609 000 48 4 3 5 Dosing devices 49 4 3 6 Combined pH electrodes 50 4 3 7 Combined metal electrodes 50 4 3 8 I...
Страница 5: ...ng the exchange unit to the Titrando 16 Fig 11 Example for connecting a dosing device Titrando 800 Dosino 18 Fig 12 Example for connecting a dosing device Titrando 805 Dosimat 19 Fig 13 Titrando Remot...
Страница 6: ...Contents IV Titrando Installation Instructions...
Страница 7: ...ces Titrandos Dosing Interfaces USB Sample Processors etc can be controlled via USB connection The tiamo software allows to expand the system with prac tically any number of control devices The contro...
Страница 8: ...nit type 806 or previous or for the use of external dosing devices 700 and 800 Dosinos with 807 dosing units Common features of the Titrando A connection for Touch Control or for a computer with PC so...
Страница 9: ...the Titrandos provide you with a com prehensive overview of the installation startup troubleshooting and technical specifications of the instruments The Installation Instructions are arranged as foll...
Страница 10: ...nue Button on the user interface Danger This symbol indicates a possible risk of death or injury to the user and possible damage to the instrument or its compo nents by electricity Warning This symbol...
Страница 11: ...tering the exchange unit 4 Coupling for switching the flat cock 2 Push rod of the dosing drive 5 On LED Lights up when the Titrando is con nected to the mains supply and a con troller Touch Control or...
Страница 12: ...ront view of a Titrando for the use of external dosing devices 7 Bottle holder with holding clips for two reagent bot tles 8 On LED Lights up when the Titrando is con nected to the mains supply and a...
Страница 13: ...connection Connection for Touch Control or PC with installed PC software 15 Connection for reference electrode Ref e g Ag AgCl reference electrode 11 MSB connections MSB 1 to MSB 4 Metrohm Serial Bus...
Страница 14: ...ando housing This could destroy the Titrando Inside the housing there are no components that the user can ser vice or exchange Electrical safety when handling the Titrando is guaranteed within the fra...
Страница 15: ...Titrando It also informs you about how a com plete titration system from a simple system with stirrer and printer up to a complicated system with additional dosing devices sample changer and balance...
Страница 16: ...system with stirrer external dosing device printer and balance More detailed information can be found in the given sections Setup Section 2 2 Touch Control Computer connection Section 2 3 Stirrer Tit...
Страница 17: ...l laboratory use it should not be used in explosion endangered locations Place the instrument on a suitable vibration free laboratory bench pro tected as much as possible from corrosive atmospheres an...
Страница 18: ...he Touch Control After switch on automatic system tests are carried out on both the Ti trando and the Touch Control The On LED on the Titrando lights up when the system test is finished and the instru...
Страница 19: ...nish PC Control Connect the USB dongle authorization plug supplied with the full version of the PC Control software to any USB socket type A of the computer or Titrando Windows 2000 The USB dongle wil...
Страница 20: ...ch have an MSB output so that the devices can be switched sequentially daisy chain The following illustration provides an overview of the devices that can be connected to an MSB Fig 8 Overview of MSB...
Страница 21: ...9 Titrando Stirrer You can connect a maximum of one 801 Stirrer one 804 Titration Stand with 802 Rod Stirrer or one 803 Titration Stand to each MSB socket The 801 Stirrer as well as the 804 and 803 T...
Страница 22: ...e exchange unit Fig 10 Attaching the exchange unit to the Titrando Slide the exchange unit onto the Titrando so that it snaps into posi tion and the Status LED slowly blinks If the exchange unit has b...
Страница 23: ...has been attached correctly and recognized and is now in the change position i e the ex change unit can be removed blinks slowly The Titrando is currently dosing or filling or the exchange unit is no...
Страница 24: ...osimat or 800 or 700 Dosino can be connected to Titrandos with an internal dosing drive and four of them to Titrandos without internal dosing drive MSB 1 is occupied by the built in dosing drive on th...
Страница 25: ...itrando without in ternal dosing drive then we recommend that the stirrer is connected to MSB 1 and the dosing device to the MSB connection of the stirrer as this corresponds to the standard settings...
Страница 26: ...ditional instrument e g a dosing device or stirrer can be connected During a method run remote output lines are set automatically and the setting of input lines by a peripheral device can automaticall...
Страница 27: ...itrando with the PC software end the program before setting up or breaking USB connections 2 5 1 Connecting a printer Printers to be connected to the Titrando operated by Touch Control must meet the f...
Страница 28: ...ER 60 120 180 182 FR 200 300 FX 200 300 320 with RS232 interface OP 03 6 2125 020 6 2125 010 Mettler AB AG PR LC RS9 Supplied with balance Mettler AM PM PE with interface option 016 or Mettler AJ PJ...
Страница 29: ...the balance Configure the RS232 interface of the balance Configure the RS232 interface of the USB RS232 box in the device manager of the Touch Control see Instructions for Use for PC Con trol Touch C...
Страница 30: ...e USB Sample Processor Robotic Titrosampler in the device manager or the configuration dialog as described in the In structions for Use for PC Control Touch Control or tiamo respec tively 2 5 4 Connec...
Страница 31: ...in the device manager Configure the keyboard in the device manager of the Touch Control as described in the Instructions for Use for PC Control Touch Con trol 2 5 6 Connecting a barcode reader The bar...
Страница 32: ...de 2 5 7 Connecting a USB hub If you would like to connect more than two devices to the USB connec tion of the Titrando then you can use an additional commercially avail able USB hub distributor If yo...
Страница 33: ...a 840 Touch Control as control unit The version 5 840 0130 or higher of the Touch Control software is required The Metrohm Bluetooth USB adapter guarantees wireless data transfer over a distance of up...
Страница 34: ...dapter Bluetooth serial adapters must be configured on the PC using the utility program supplied by the manufacturer The data transfer parameters of instrument and adapter must agree with each other T...
Страница 35: ...necting an 854 iConnect One or two external 854 iConnect measuring interfaces can be con nected to an 857 Titrando depending on the Titrando s version Connect the iConnect plug of the 854 iConnect to...
Страница 36: ...portant that the solution is thoroughly mixed The stir ring rate should be high enough for a small vortex to be formed If the stirring rate is too high then air bubbles will be entrained This results...
Страница 37: ...Installation Instructions 31 2 6 4 Assembly of the Karl Fischer titration cell Install the titration cell for volumetric KF titrations according to the fol lowing figures Fig 21 Drawing of the KF tit...
Страница 38: ...uret tip and draw off tip 1 Position of the transport tip for sol vent 3 Position of the draw off tip 2 Position of the buret tip for KF re agent 2 7 Update of the instrument software The Update of th...
Страница 39: ...links while the data is being read out from an intel ligent exchange unit 806 and is on continuously when the exchange unit has been recognized correctly The exchange unit flat cock is not in the chan...
Страница 40: ...is indi cated by the software Touch Control or PC Control tiamo Switch the control device off and then on again The dosing device is initialized when switching on Re move the exchange unit and clean...
Страница 41: ...Titration to one or two predefined endpoints KFT Karl Fischer titration STAT Endpoint titration while holding the measured value constant MEAS Measurement pH potential temperature current Upol poten...
Страница 42: ...1000 NTC 150 C 250 C 20 C 250 C 4 0 1 C 0 1 C 0 2 C Pt1000 20 C 150 C 1 1 digit without sensor error under reference conditions 2 potentiometric and voltametric 3 amperometric 4 for a NTC Sensor with...
Страница 43: ...rol the Titrando Touch Control connection With built in Touch Control cable Computer connection With 6 2151 000 cable MSB connections MSB Metrohm Serial Bus Dosing device Connection of max 3 external...
Страница 44: ...lity EMC Emission Standards complied with EN IEC 61326 EN 55022 CISPR 22 Immunity Standards complied with EN IEC 61326 EN IEC 61000 4 2 EN IEC 61000 4 3 EN IEC 61000 4 4 EN IEC 61000 4 5 EN IEC 61000...
Страница 45: ...e Housing material Polybutylene terephthalate PBT Width Height Depth 142 mm 227 mm 231 mm Weight 2817 g 4 1 13 Recycling and disposal This product is covered by European Directive 2002 96 EC WEEE Wast...
Страница 46: ...to 2 808 0020 No Order No Description 1 1 808 0010 or 1 808 0020 808 Titrando with one measuring interface or 808 Titrando with two galvanically separated measuring interfaces 1 6 0262 100 Ecotrode P...
Страница 47: ...ring interface or 809 Titrando with two galvanically separated measuring interfaces 1 6 0262 100 Ecotrode Plus Combined LL pH glass electrode with fixed ground joint diaphragm 1 6 2104 020 Connection...
Страница 48: ...measuring interface or 835 Titrando with two galvanically separated measuring interfaces 1 6 0262 100 Ecotrode Plus Combined LL pH glass electrode with fixed ground joint diaphragm 1 6 2104 020 Conne...
Страница 49: ...ring interface or 836 Titrando with two galvanically separated measuring interfaces 1 6 0262 100 Ecotrode Plus Combined LL pH glass electrode with fixed ground joint diaphragm 1 6 2104 020 Connection...
Страница 50: ...o with one measuring interface 1 6 5609 000 Karl Fischer titration equipment see Section 4 3 4 and Fig 21 2 6 2043 005 Holding clip for bottle 1 1 6 2103 130 6 2103 140 Adapter red Adapter black for t...
Страница 51: ...lus Combined LL pH glass electrode with fixed ground joint diaphragm 1 6 2104 020 Connection cable for Metrohm electrodes with plug head length 1 m 2 6 2043 005 Holding clip for bottle 1 1 6 2103 130...
Страница 52: ...kets refers to 2 857 0020 No Order no Description 1 1 857 0010 or 1 857 0020 857 Titrando with one measuring interface or 857 Titrando with two galvanically separated measuring interfaces 1 1 854 0010...
Страница 53: ...c stirrer without stand 2 804 0040 804 Titration stand for 802 Rod stirrer with stand and electrode holder for mounting on Titrando 2 804 0010 804 Titration stand for 802 Rod stirrer without stand 2 8...
Страница 54: ...013 010 Clamping ring for 10 mm diameter support rods 6 1602 190 Bottle adapter for tandem dosing 1 x NS14 4 x M6 4 3 4 Karl Fischer titration equipment 6 5609 000 Order no Description 6 0338 100 Doub...
Страница 55: ...ass cylinder 6 3026 150 806 Exchange unit with 5 mL glass cylinder 6 3026 210 806 Exchange unit with 10 mL glass cylinder 6 3026 220 806 Exchange unit with 20 mL glass cylinder 6 3026 250 806 Exchange...
Страница 56: ...ed LL pH glass electrode 6 0255 100 Profitrode Combined LL pH glass electrode with ground diaphragm double junction 6 0258 010 Unitrode with Pt1000 temperature sensor 2 mm plug plug F 6 0259 100 Unitr...
Страница 57: ...0726 100 Ag AgCl reference electrode with ground joint diaphragm 6 0726 107 Ag AgCl reference electrode filled with c KCl 3 mol L with ground joint diaphragm 6 0726 108 Ag AgCl reference electrode fi...
Страница 58: ...for measurements in poorly conducting solutions 6 5104 040 Differential amplifier 115 V USA for measurements in poorly conducting solutions 4 3 13 Communication Order no Description 6 2151 000 Cable...
Страница 59: ...nk for connecting the Touch Control to a computer network 4 3 14 Cables for balances Order no Description 6 2125 010 Adapter cable 25 pin to 9 pin 9 p f 25 p m 30 cm 6 2125 020 Cable for Mettler balan...
Страница 60: ...ll as the absence of guaranteed features the purchaser has no rights or claims except those mentioned above If damage of the packaging is evident on receipt of a consignment or if the goods show signs...
Страница 61: ...IEC 61000 4 5 EN IEC 61000 4 6 EN IEC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the Int...
Страница 62: ...4 6 EN IEC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Bod...
Страница 63: ...IEC 61000 4 5 EN IEC 61000 4 6 EN IEC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the Int...
Страница 64: ...4 6 EN IEC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Bod...
Страница 65: ...EC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Body CB IEC...
Страница 66: ...4 6 EN IEC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Bod...
Страница 67: ...EC 61000 4 11 Safety specifications EN IEC UL 61010 1 CSA C22 2 No 61010 1 protection class I It has also been certified by ElectroSuisse which is member of the International Certification Body CB IEC...
Страница 68: ...e Laboratory testing accompanies all phases of instrument development Software development Software development occurs in terms of the software life cycle Tests are per formed to detect programming er...
Страница 69: ...ument setup 11 Instrument software Update 32 Instrument type 7 Interface 37 Internal dosing device 37 Operating status 16 Internal dosing drive 2 Introduction 1 Ion sensitive electrodes 50 K Karl Fisc...
Страница 70: ...Titration modes 35 Titration stand 14 47 Connection 15 Titration vessel 47 Setup 30 Touch Control 25 Connection 12 Transport damage 54 Troubleshooting 33 U Update Instrument software 32 USB 37 connec...
