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859 Titrotherm

Manual

8.859.8001EN / 2019-12-02

Содержание 859 Titrotherm

Страница 1: ...859 Titrotherm Manual 8 859 8001EN 2019 12 02...

Страница 2: ......

Страница 3: ...Metrohm AG CH 9100 Herisau Switzerland Phone 41 71 353 85 85 Fax 41 71 353 89 01 info metrohm com www metrohm com 859 Titrotherm Manual 8 859 8001EN 2019 12 02...

Страница 4: ...echcom metrohm com This documentation is protected by copyright All rights reserved This documentation has been prepared with great care However errors can never be entirely ruled out Please send comm...

Страница 5: ...6 1 4 4 Recycling and disposal 6 2 Overview of the instrument 7 3 Installation 9 3 1 Setting up the instrument 9 3 1 1 Packaging 9 3 1 2 Checks 9 3 1 3 Location 9 3 2 Connecting the instrument to the...

Страница 6: ...ximum dosing and filling rate 23 6 3 Remote interface 24 6 3 1 Pin assignment of the remote interfaces 24 7 Technical specifications 26 7 1 Measuring interface NTC 10 kOhm 26 7 2 Interfaces and connec...

Страница 7: ...computer 11 Figure 6 MSB connections 13 Figure 7 Connecting a dosing device 14 Figure 8 Connecting an MSB stirrer 15 Figure 9 Propeller stirrer and titration stand 15 Figure 10 Connecting a Remote Bo...

Страница 8: ......

Страница 9: ...ic titration we recommend the monograph Thomas Smith Practical thermometric titrimetry Metrohm AG 2006 Order No 8 036 5003 1 1 The 859 Titrotherm in the Titrando system The 859 Titrotherm is a compone...

Страница 10: ...ay Box Remote Box 859 Titrotherm Stirrer Ti Stand Dosino Dosimat U S B R S 2 3 2 C o n v e r t e r 867 pH Module Titrando On Figure 1 The 859 Titrotherm in the Titrando system You can request informat...

Страница 11: ...nd other commands TET Thermometric endpoint titration The reagent addition takes place con tinuously at a constant dosing rate Dosing commands The following commands for dosing can be selected ADD add...

Страница 12: ...ing symbols and formatting may appear in this documentation Cross reference to figure legend The first number refers to the figure number the sec ond to the instrument part in the figure Instruction s...

Страница 13: ...maintain this state and ensure non hazardous operation of the instrument the following instructions must be observed carefully 1 4 2 Electrical safety The electrical safety when working with the inst...

Страница 14: ...ctrical plug connections at the rear of the instrument 1 4 3 Working with liquids CAUTION Periodically check all system connections for leaks Observe the relevant regulations in respect to working wit...

Страница 15: ...ermoprobes 2 USB connector USB 1 and USB 2 USB ports type A for connecting printer keyboard barcode reader additional Titran dos USB Sample Processor etc 3 Controller connector Controller Connector fo...

Страница 16: ...itrotherm with titration accessories 1 800 Dosino Dosing drive for the titrant 2 Dosing unit 6 3032 XXX With cylinder sizes 2 5 10 20 50 mL 3 Bottle 6 1608 XXX 4 Bottle holder for Dosinos 6 2061 010 5...

Страница 17: ...table for operation and free of vibrations and which provides protection against corrosive atmosphere and contamination by chemicals The instrument should be protected against excessive temperature fl...

Страница 18: ...n order to be able to be controlled by a computer software Using a 6 2151 000 controller cable the instrument can be connected directly either to a USB socket on a computer to a connected USB hub or t...

Страница 19: ...iver installation proceeds differ ently afterwards Either the necessary driver software is installed automatically or an installation wizard is started 3 Follow the instructions of the installation wi...

Страница 20: ...of the instrument can be found in the documentation for the respective computer software 3 4 Connecting MSB devices In order to connect MSB devices e g stirrers or dosing devices Metrohm instruments...

Страница 21: ...or at one time Type 700 Dosino dosing devices cannot be connected together with other MSB instruments on a shared connector These dosing devices must be connected separately CAUTION Exit the control s...

Страница 22: ...on the rear of the 859 Titrotherm Start the control software Figure 7 Connecting a dosing device 3 4 2 Connecting a stirrer or titration stand You can use the magnetic stirrers 801 Stirrer or 803 Ti...

Страница 23: ...emote Box In addition to Metrohm other instrument manufacturers also use similar connectors that make it possible to connect different instruments together These interfaces are also frequently given t...

Страница 24: ...urrent outlets The Remote Box also has an MSB socket at which a further MSB device e g a dosing device or a stirrer can be connected You will find precise information concerning the pin assignment of...

Страница 25: ...d simultaneously from one PC software 3 6 Connecting a sensor Connect the Thermoprobe as follows 1 Plug the Thermoprobe plug into the T Port 1 or T Port 2 socket of the 859 Titrotherm Note the orienta...

Страница 26: ...on stand 2 Sensor Thermoprobe 6 9011 020 or 6 9011 040 Connect the sensor at T Port 1 or T Port 2 to the rear side of the 859 Titrotherm 3 SGJ sleeve 6 1236 050 SGJ 14 12 mm Material PE 4 SGJ intermed...

Страница 27: ...hould be installed in accordance with the above figure A high stirring rate is very important Please ensure that there is a sufficient amount of liquid in the vessel so that the sensor is immersed at...

Страница 28: ...is is extensively prevented by design measures the mains plug should be unplugged immediately if aggressive media has penetra ted the inside of the instrument so as to avoid serious damage to the inst...

Страница 29: ...can be read from the dosing unit or be saved on it anymore The dosing drive is overloa ded because the piston or the valve disc is jammed Exit tiamo and then restart it The dosing device will be initi...

Страница 30: ...itration In contrast to potentiometric electrodes Thermoprobes need not be cali brated 6 9011 020 6 9011 040 Figure 13 Thermoprobes two models Thermoprobe with glass shaft 6 9011 020 For titrations in...

Страница 31: ...ensor with water or other cleaning solutions 6 2 Maximum dosing and filling rate The maximum dosing rate and maximum filling rate for the dosing unit depend on the cylinder volume Cylinder volume Maxi...

Страница 32: ...ector Metrohm Serial Bus For connecting external dosing devices or stirrers 3 Remote connector For connecting instruments with a remote interface 6 3 1 Pin assignment of the remote interfaces 13 1 14...

Страница 33: ...be set with the CTRL command Table 1 Inputs and outputs of the remote interface Assignment Pin no Assignment Pin no Input 0 21 Output 0 5 Input 1 9 Output 1 18 Input 2 22 Output 2 4 Input 3 10 Output...

Страница 34: ...SB Upstream port 9 pin Mini DIN socket for connecting a computer for controlling the instrument MSB connectors MSB1 MSB4 Four 9 pin Mini DIN sockets for connecting dosing devices Dosino Dosimat stirre...

Страница 35: ...60 C Transport 40 60 C 7 5 Reference conditions Ambient tempera ture 25 C 3 C Relative humidity 60 Instrument status Instrument in operation at least 30 min Validity of the data After adjustment 7 6...

Страница 36: ...r Internet browser 2 Enter the article number e g 859 into the search field The search result is displayed 3 Click on the product Detailed information regarding the product is shown on various tabs 4...

Страница 37: ...nstallation Driver software 10 Instrument description 3 Instrument type 7 Intended use 3 Intermediate cone 18 L LED On 7 21 Status 21 Link stopper 18 M Magnetic stirrer Connect 14 Mains connection 7 M...

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