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882 Compact IC plus

882 Compact IC plus – Anion

Manual

8.882.8012EN

Содержание 1.882.0020

Страница 1: ...882 Compact IC plus 882 Compact IC plus Anion Manual 8 882 8012EN...

Страница 2: ......

Страница 3: ...etrohm AG CH 9101 Herisau Switzerland Phone 41 71 353 85 85 Fax 41 71 353 89 01 info metrohm com www metrohm com 882 Compact IC plus 882 Compact IC plus Anion 2 882 0020 Manual 8 882 8012EN 05 2011 zs...

Страница 4: ...gh all the information given in this documentation has been checked with great care errors cannot be entirely excluded Should you notice any mistakes please send us your comments using the address giv...

Страница 5: ...ear 8 3 Installation 10 3 1 About this chapter 10 3 2 Initial installation 10 3 3 Installation diagram 13 3 4 Setting up the instrument 15 3 4 1 Packaging 15 3 4 2 Checks 15 3 4 3 Location 16 3 5 Capi...

Страница 6: ...Connecting the instrument to mains supply 45 3 16 Guard column 46 3 17 Separation column 47 4 Start up 50 4 1 Initial start up 50 4 2 Conditioning 51 5 Handling and maintenance 53 5 1 General notes 53...

Страница 7: ...d their solutions 82 7 Technical specifications 86 7 1 Reference conditions 86 7 2 Instrument 86 7 3 Leak sensor 86 7 4 Ambient conditions 86 7 5 Housing 87 7 6 High pressure pump 87 7 7 Injection val...

Страница 8: ...Table of contents VI 882 Compact IC plus Anion Index 107...

Страница 9: ...igh pressure pump 31 Figure 16 Connecting the inline filter 33 Figure 17 Pulsation absorber Connection 34 Figure 18 Injection valve connected 35 Figure 19 Injection valve Positions 36 Figure 20 Perist...

Страница 10: ......

Страница 11: ...on which MagIC Net is installed The soft ware automatically recognizes the instrument and checks its functional readiness MagIC Net controls and monitors the instrument evaluates the measured data and...

Страница 12: ...the heart of the ion chromatographic analysis It separates the different components corresponding to their interactions with the column Metrohm separation columns are equipped with a chip on which the...

Страница 13: ...ry out these steps in the sequence shown Warning This symbol draws attention to a possible life hazard or risk of injury Warning This symbol draws attention to a possible hazard due to electrical curr...

Страница 14: ...fety The electrical safety when working with the instrument is ensured as part of the international standard IEC 61010 Warning Only personnel qualified by Metrohm are authorized to carry out service w...

Страница 15: ...be used to loosen connections Check the connections regularly for leakage If the instrument is used mainly in unattended operation then weekly inspections are manda tory 1 4 4 Flammable solvents and c...

Страница 16: ...Safety instructions 6 882 Compact IC plus Anion More details about the disposal of your old equipment can be obtained from your local authorities from waste disposal companies or from your local deal...

Страница 17: ...ont 1 2 3 4 5 6 7 8 9 10 Figure 1 Front 882 Compact IC plus Anion 1 High pressure pump 2 Purge valve 3 Inline filter 4 Pulsation absorber 5 Injection valve 6 Column chamber 7 Column holder With column...

Страница 18: ...2 2 Rear 8 882 Compact IC plus Anion 2 2 Rear 21 1 20 1 18 17 19 15 14 12 11 10 9 8 13 7 6 5 4 3 1 1 2 16 Type Made by Metrohm Herisau Switzerland Figure 2 Rear 882 Compact IC plus Anion...

Страница 19: ...g 10 Leak sensor connection cable Extractable For connecting the leak sensor 11 Drainage tubing connector For supplying escaped liquid through the connected drainage tubing to the leak sen sor 12 Devi...

Страница 20: ...uding those that are already installed at the time the instrument is delivered 3 2 Initial installation Note A number of the capillaries is already connected at the time the instru ment is delivered I...

Страница 21: ...the Sample Processor if applicable see Sample Processor manual Guide the sample outlet capillary connected to the sample output of the injection valve out of the instrument through a capillary feed th...

Страница 22: ...Connecting the MSM see Chapter 3 14 page 42 Connect the capillary of the MSM labeled with regenerant to the pump tubing connection of the pump tubing for the regeneration solution using a short pressu...

Страница 23: ...using a short pressures screw 6 2744 070 OR Connect the inlet of the separation column with the guard column if used see leaflets to the separation column and the guard column Connect the MSM capilla...

Страница 24: ...3 3 Installation diagram 14 882 Compact IC plus Anion 1 2 6 17 17 16 7 8 9 10 11 12 13 14 3 17 18 19 17 15 4 5 20 17 17 Figure 3 Installation diagram 882 Compact IC plus Anion...

Страница 25: ...ing solution inlet capillary Labeled with rinsing solution 14 MSM rinsing solution outlet capillary Labeled with waste rins 15 Sample aspirating capillary 6 1803 040 Connected to the injection valve 1...

Страница 26: ...l information concerning the capillary con nections in the IC instruments and systems Generally speaking capillary connections between two components of an IC system are made up of one connection capi...

Страница 27: ...internal diameter of 0 25 mm for the entire high pressure range PEEK capillaries 6 1831 030 with an internal diameter of 0 75 mm for sample handling in the ultra trace range Caution For the capillary...

Страница 28: ...ry connections To create dead volume free capillary connections proceed as follows 1 Slide the pressure screw over the capillary Ensure that the capillary protrudes 1 2 mm from the tip of the pressure...

Страница 29: ...arning In order to avoid damage to the high pressure pump the transport locking screws must be remounted each time the instrument undergoes major transport 3 6 2 Leak sensor The leak sensor detects es...

Страница 30: ...r 2 Leak sensor connector plug 3 Leak sensor connection cable Extractable Coiled up in the base tray 3 6 3 Drainage tubings Fluid that escapes in the covering plate or in the detector chamber flows th...

Страница 31: ...the detector chamber 4 Drainage tubing Section of the 6 1816 020 silicon tubing For draining escaped fluid from the detector chamber 5 Y connector 6 1807 010 For connecting the two drainage tubings 6...

Страница 32: ...6 2 and drainage tubing 6 4 to the Y connector 6 5 4 Connect drainage tubing 6 6 to the Y connector 6 5 shorten to the required length and connect the other end of the drainage tub ing to the drainage...

Страница 33: ...onnector For connecting a 6 2816 020 syringe For manual sample feeding 5 Capillary feed through At the door of the instrument For feeding capillaries out of the instrument 6 Capillary feed through At...

Страница 34: ...following accessories for equipping the eluent aspiration tubing 6 1602 160 Eluent bottle attachment GL 45 6 2744 210 tubing adapter for aspiration filter 6 2821 090 aspiration filter To equip the el...

Страница 35: ...and screw tight 1 2 Figure 9 Mounting aspiration filter 1 Filter holder From accessories set 6 2744 210 2 Aspiration filter 6 2821 090 4 Install tubing weighting and aspiration filter 1 2 3 4 5 Figure...

Страница 36: ...ation tubing into the eluent bottle 12 10 Fasten the completely equipped bottle attachment 10 2 on the eluent bottle 12 10 The aspiration filter 12 6 must rest on the base of the eluent bottle Close t...

Страница 37: ...609 000 3 Cotton 4 CO2 adsorber Adsorbs CO2 from the air e g Merck soda lime with indicator no 6839 10 5 Eluent 6 Aspiration filter 6 2821 090 7 Filter holder From accessories set 6 2744 210 8 Clampin...

Страница 38: ...history operating hours service data are saved The purge valve is used for deaerating see Chapter 3 9 2 page 30 the high pressure pump 3 9 1 Capillary connections high pressure pump purge valve Note A...

Страница 39: ...er with the pressure screw 13 8 under the number 6 2744 230 10 Deaerating capillary For aspirating the eluent when deaerating the high pressure pump see Chapter 3 9 2 page 30 11 Purge valve For deaera...

Страница 40: ...ion The clamping screws must be tightened carefully To tighten grip the coupling 14 2 with the key 6 2739 000 and grip the clamp ing screw 14 3 with the wrench 6 2621 050 Plug the eluent aspiration tu...

Страница 41: ...valve rotary knob 1 Connecting the purging needle Push the end of the purging needle 15 3 over the end of the deaerating capillary 15 4 on the purge valve 2 Connecting the syringe Insert syringe 15 1...

Страница 42: ...t the separation column securely against possible con tamination from the eluent Inline filters can however also just as well be used for the purpose of protecting the suppressor against contamination...

Страница 43: ...unning to the pulsation absorber to the output side of the inline filter using a pressure screw 6 2744 070 3 11 Pulsation absorber Note The pulsation absorber is already installed in the newly deliver...

Страница 44: ...on valve connects the eluent and sample path Through rapid and precise valve switchover a precise amount of sample solution defined by the size of the sample loop is injected and rinsed with eluent on...

Страница 45: ...sample to the waste container 7 PEEK pressure screw 6 2744 010 Replacing the sample loop The sample loop can be replaced depending on requirements For addi tional information concerning selection of t...

Страница 46: ...nt input Capillary coming from the high pressure pump 2 Eluent output Capillary to the column 3 Sample input Sample aspirating capillary 4 Sample output Capillary to waste container 5 Sample loop Posi...

Страница 47: ...on without suppression 100 L 3 13 Peristaltic pump 3 13 1 Principle of the peristaltic pump The Peristaltic pump is used for pumping sample and auxiliary solutions It can rotate in both directions The...

Страница 48: ...sure screws short 6 2744 070 2 Tubing olive 6 2744 034 3 Stopper The colors of the stopper indicate the inner diameter of the pump tubing 4 Tubing cartridge 6 2755 000 5 Contact pressure lever 6 Union...

Страница 49: ...or pumping the auxiliary solutions to the MSM or to the SPM a 6 2744 180 pump tubing connection with filter must be used Case A 6 2744 180 pump tubing connection with filter 1 2 3 Figure 22 Install pu...

Страница 50: ...ting the pump tubing Press the contact pressure lever all the way down Place the pump tubing in the tubing cartridge The stoppers 21 3 must snap into the corresponding holders of the tubing cartridge...

Страница 51: ...e press it all the way down Switch on the peristaltic pump Raise the contact pressure lever one step at a time until liquid flows When liquid starts flowing raise the contact pressure lever by an addi...

Страница 52: ...for suppression regenerated with 100 mmol L sulfuric acid rinsed with ultrapure water Suppression reaction in the MSM When using a carbonate eluent the following reaction amongst others occurs in the...

Страница 53: ...er 6 2744 180 22 3 must be mounted between the peristaltic pump and the inlet capillaries of the suppressor Connect the PTFE capillaries firmly mounted on the connecting piece to the other components...

Страница 54: ...he end of the inlet capillary labeled with rinsing solution to the pump tub ing connection of the pump tubing which carries the rinsing solu tion 4 Connecting the rinsing the solution outlet capillary...

Страница 55: ...itzerland 6 2122 040 with plug CEE 7 VII Germany 6 2122 070 with plug NEMA 5 15 USA The mains cable is three core and provided with a plug with grounding If another plug has to be mounted the yellow g...

Страница 56: ...ch is available from your Metrohm agent the leaflet provided along with your separation column the product information on the separation column at http www metrohm com product area Ion Chromatography...

Страница 57: ...utlet capillary of the guard column Set the flow rate of the high pressure pump according to the data given in the leaflet of the separation column Start the high pressure pump and rinse the guard col...

Страница 58: ...ttp www metrohm com in the Applications area or via the Metrohm agent responsible free of charge Note The separation column may only be installed after the initial start up see Chapter 4 1 page 50 of...

Страница 59: ...the separation column approx 10 minutes with eluent Switch off the high pressure pump again 3 Mounting the separation column Fasten the column output capillary to the output of the separation column...

Страница 60: ...t be installed for the initial start up Make sure that the coupling 6 2744 040 is being used instead of the columns Perform the following steps during the initial start up 1 Preparing the software Sta...

Страница 61: ...umns with eluent for 5 minutes The instrument is now ready for the installation of the columns see Chap ter 3 16 page 46 4 2 Conditioning After the installation and after switching on the instrument t...

Страница 62: ...espective solutions and that the is enough solution in the bottles 3 Checking leak tightness In MagIC Net start the equilibration Check all capillaries and their connections from the high pressure pum...

Страница 63: ...cs In such cases the Metrohm Service must be informed On the rear of the instrument the drainage tubings must be mounted and the leak sensor must be plugged in and activated as protection against esca...

Страница 64: ...follows 1 Remove the separation column from the eluent path Connect the connection capillaries directly with each other using a coupling 6 2744 040 2 Rinse the IC system with methanol ultrapure water...

Страница 65: ...y applies for reagents which are used in ion chromatography Newly produced eluents should always be microfiltered filter 0 45 m The composition of the eluent has a crucial effect on the chromatographi...

Страница 66: ...4 2 3 Changing the eluent When changing the eluent it must be ensured that no precipitates can occur Solutions following one another in direct succession must therefore be miscible If the system has t...

Страница 67: ...leaning contami nated valves and or replacing worn parts such as pistons piston seal and valves This maintenance work should be carried out at least once a year Removing the pump head 1 Switch off hig...

Страница 68: ...idge 2 Dismantling the piston Caution On the inside of the piston cartridge there is a taut spring than can jump out of the piston cartridge if suddenly loosing tension When opening the piston cartrid...

Страница 69: ...rasion or deposits with fine abrasive cleaning powder rinse particle free with ultrapure water and dry Replace highly contaminated or scratched zirconium oxide pistons spare part 6 2824 070 zirconium...

Страница 70: ...n seal 2 Sleeve Sleeve for inserting the new piston seal Caution Screwing the special tool for the piston seal 6 2617 010 into the pis ton seal destroys this completely 1 Removing the piston seal Caut...

Страница 71: ...piston seal 27 2 The sealing springs must be visible from the outside 1 2 Figure 29 Inserting the piston seal into the tool 1 Tool for piston seal 6 2617 010 Sleeve for inserting the new piston seal...

Страница 72: ...ridge back into the pump head and tighten first by hand then additionally by approx 15 with a wrench Cleaning the inlet valve and outlet valve 1 Removing valves Unscrew the connection capillary for th...

Страница 73: ...solution or acetone The rinsing effect is further increased through a short treatment lasting for a maximum of 20 s in an ultrasonic bath Note Longer lasting ultrasonic baths can damage the ruby ball...

Страница 74: ...2 valve 3 Recess For collecting the valve components 4 Holder The components of the valve are collected in the recess of the holder Note The components of the valve are very small In order not to los...

Страница 75: ...must point to ruby ball 8 Ruby ball 9 Ceramic holder for ruby ball 10 Seal The larger opening must point outwards 4 Cleaning the components of the valve Rinse the valve components with ultrapure wate...

Страница 76: ...7 Inserting the valves back into the pump head Caution If by mistake the inlet valve is mounted instead of the outlet valve an extreme pressure builds up within the working cylinder which can destroy...

Страница 77: ...6 2621 030 2 Screw connection capillaries 13 1 13 7 and 13 13 onto the pump head again 5 6 Inline filter 5 6 1 Maintenance The inline filter 6 2821 120 comprises the filter housing 34 2 the filter scr...

Страница 78: ...he filter Remove the old filter 34 3 using tweezers Place the new filter 34 3 flat in the filter housing 34 2 using tweezers 4 Mounting filter screw Screw the filter screw 34 4 back into the filter ho...

Страница 79: ...aly sis If the concentration of the sample is too high the sample should be dilu ted before feeding see documentation on the IC Equipment for Sample Dilution For an overview of all Metrohm inline samp...

Страница 80: ...oceed as follows 1 Preparing two samples Sample A A typical sample for the application Sample sample B Ultrapure water 2 Determining Sample A Let Sample A pass through the sample path for the duration...

Страница 81: ...r rinsing with solutions containing acetone In this case use other pump tubings or use another pump for rinsing 5 10 2 Maintenance 5 10 2 1 Pump tubing The pump tubing used in the peristaltic pump is...

Страница 82: ...ine ultrafiltration 6 1826 330 Pump tubing LFL orange white 3 stopper PVC Tygon 0 64 mm No special applications 6 1826 340 Pump tubing LFL black black 3 stop per PVC Tygon 0 76 mm For the sample solut...

Страница 83: ...11 Metrohm Suppressor Module MSM 5 11 1 Protection To protect the suppressor against foreign particles or bacterial growth a pump tubing connection with filter 6 2744 180 see Figure 22 page 39 must b...

Страница 84: ...must be regenerated see Chapter 5 11 3 2 page 74 cleaned see Chapter 5 11 3 3 page 76 or replaced see Chapter 5 11 3 4 page 78 5 11 3 Maintenance 5 11 3 1 Parts of the suppressor 1 2 3 4 5 Figure 36 P...

Страница 85: ...ng the suppressor from the IC system Disconnect the capillaries of the suppressor labeled with regener ant and rinsing solution from the IC system 2 Connecting the suppressor to the high pressure pump...

Страница 86: ...lowing cases it may be necessary to clean the suppressor Increased backpressure onto the connection tubings of the suppres sor Blockage of the suppressor which cannot be eliminated solutions can no lo...

Страница 87: ...the corre sponding recesses inside the housing and one of the three holes of the rotor is visible from below in the slot of the housing 36 5 If the rotor is correctly inserted its sealing surface will...

Страница 88: ...the suppressor from the IC system 2 Dismantling the suppressor Unscrew union nut 36 1 from the housing 36 4 Pull the connecting piece 36 2 and the rotor 36 3 out of the housing The connecting piece an...

Страница 89: ...e first time rinse the three suppressor units with solution for 5 minutes 5 12 Separation column 5 12 1 Separating efficiency Which analysis quality can be attained depends to a great extent on the se...

Страница 90: ...your separation column the product information on the separation column at http www metrohm com product area Ion Chromatography or obtained directly from your agent The pulsation absorber see Chapter...

Страница 91: ...tional Qualification OQ IQ and OQ are also offered as a service by the Metrohm agents In addition various application bulletins are also available on the subject which also contain Standard Operat ing...

Страница 92: ...tion column blocked Regenerate separation column see Chap ter 5 12 4 page 80 Replace separation column see Connect ing and rinsing the separation column page 48 Note Samples should always be microfilt...

Страница 93: ...age 57 piston seals Pulsation absorber not connected Connect pulsation absorber see Chapter 3 11 page 33 Pulsation absorber not connected or defective Connect pulsation absorber see Chapter 3 11 page...

Страница 94: ...altic pump pump tubing defective Replace pump tubing Chromatograms have poor resolution Separation column diminished separating effi ciency Regenerate separation column see Chap ter 5 12 4 page 80 Rep...

Страница 95: ...ple rinsing volume too low Increase rinsing time see Chapter 5 9 page 69 Injection valve defective Request Metrohm Service Unexpected change to the retention times in the chroma tograms Separation col...

Страница 96: ...C system Compact system with modular design Material Painted polyurethane hard foam without CFCs fire class V0 Operating pres sure range 0 50 MPa 500 bar high pressure pump 0 35 MPa 350 bar standard P...

Страница 97: ...pe Serial dual piston pump Intelligent pump head recognition Chemically inert Metal free pump heads Materials in contact with eluent PEEK ZrO2 PTFE PE Self optimizing flow and pressure Flow rate Adjus...

Страница 98: ...own after 3 piston strokes below the minimum pressure limit 7 7 Injection valve Actuator time typ 100 ms Max operating pressure 35 MPa 350 bar Material PEEK 7 8 Peristaltic pump Type 2 channel perista...

Страница 99: ...ctronically monitored internal fuse 3 15 A 7 11 Interfaces USB Input 1 USB upstream type B for connection to the PC Output 2 USB downstream type A MSB 2 MSB MiniDin 8 pin female for Dosino stirrer rem...

Страница 100: ...13 Electromagnetic compatibility EMC Emission EN IEC 61326 1 EN IEC 61000 6 3 EN 55022 CISPR 22 EN IEC 61000 3 2 EN IEC 61000 3 3 Immunity EN IEC 61326 1 EN IEC 61000 6 2 EN IEC 61000 4 2 EN IEC 61000...

Страница 101: ...compatibility Emission EN IEC 61326 1 2006 EN IEC 61000 6 3 2004 EN 55022 CISPR 22 2006 EN IEC 61000 3 2 2006 EN IEC 61000 3 3 2005 Immunity EN IEC 61326 1 2006 EN IEC 61000 6 2 2005 EN IEC 61000 4 2...

Страница 102: ...d by SQS Swiss Association for Quality and Management Systems Internal and external audits are carried out periodically to assure that the standards defined by Metrohm s QM Manual are maintained The s...

Страница 103: ...equipped to support customers in imple menting standards such as GLP GMP ISO 900X in performing Opera tional Qualification and Performance Verification of the system compo nents or in carrying out the...

Страница 104: ...ranty guarantee 94 882 Compact IC plus Anion Faults arising from circumstances that are not the responsibility of Metrohm such as improper storage or improper use etc are expressly excluded from the w...

Страница 105: ...60320 C13 Cable plug according to customer requirements Switzerland Type SEV 12 6 2122 020 Germany Type CEE 7 VII 6 2122 040 USA Type NEMA ASA 6 2122 070 2 6 1602 150 Bottle attachment GL 45 3 x UNF 1...

Страница 106: ...e mL 1000 1 6 1608 070 Eluent bottle 2 L GL 45 Material Clear glass Height mm 262 Volume mL 2000 1 6 1609 000 Adsorber tube large and bent For filling with adsorber material Material Glass Height mm 1...

Страница 107: ...ry 0 5 mm i d 1 m Capillary for sample handling in IC Material PTFE Outer diameter inches 1 16 Inner diameter mm 0 5 Length m 1 1 6 1807 010 Y connector for tubing i d 6 9 mm Connector for waste tubin...

Страница 108: ...6 320 Pump tubing LFL orange yellow 3 stop per For suppressor solutions acceptor solutions for inline dialysis and for inline ultrafiltration 1 6 2023 020 Clip for SGJ 14 15 Clip for SGJ 14 15 Materia...

Страница 109: ...0 PRIMUS multi anion standard solution Promo 1 6 2617 010 Tool for piston seal For removing and assembling the piston seal for all standard pump heads 2 6 2621 000 Adjustable wrench Maximum opening 20...

Страница 110: ...o Description 1 6 2621 050 1 4 in wrench For 1 4 in screws For IC instruments Length mm 73 1 6 2621 080 Capillary cutter For plastic capillaries For IC instruments Length mm 118 1 6 2621 100 Hexagon k...

Страница 111: ...sional IC instruments to be mounted on the front of the instrument 2 6 2739 000 Wrench For tightening connectors Length mm 68 1 6 2743 080 Stoppers for overflow 5 pieces For Professional IC instrument...

Страница 112: ...ve UNF 10 32 2x Connection of pressure screw and pump tubing 2 pieces For IC instruments with peristaltic pumps 2 6 2744 040 2 x UNF 10 32 coupling For connecting 1 16 in capillaries For IC instrument...

Страница 113: ...p tubing and a capillary with built in fil ter Material PEEK 1 6 2744 210 Tubing adapter for aspiration filter For Professional IC instruments 1 6 2816 020 Syringe 10 mL with Luer connection For diffe...

Страница 114: ...IC plus Anion Order no Description 2 850 9010 850 Professional IC Detector iDetector Compact and intelligent High Performance Conductivity Detector for intelligent IC Instruments Outstanding temperat...

Страница 115: ...exible user administration efficient database operations extensive data export functions individually configurable report generator control and monitoring of all system components and the chromatograp...

Страница 116: ...ftware permits control data acquisition eval uation and monitoring as well as report generation of ion chromatographic analyses Graphics user interface for routine operations extensive database pro gr...

Страница 117: ...Electrostatic charge 5 Eluent Aspiration 24 Production 55 Eluent bottle Figure 27 Installation 24 Operation 56 EMC 90 Emission 90 Equilibration 50 52 F Feed throughs Capillaries 22 Fill Injection val...

Страница 118: ...stalling 38 Service life 71 Purge valve 28 Q Quality Management 81 R Reference conditions 86 Regeneration 53 Suppressor 74 Rinsing Guard column 47 Pump tubings 71 Sample path 69 Separation column 49 R...

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